EN ISO 3405:2019
(Main)Petroleum and related products from natural or synthetic sources - Determination of distillation characteristics at atmospheric pressure (ISO 3405:2019)
Petroleum and related products from natural or synthetic sources - Determination of distillation characteristics at atmospheric pressure (ISO 3405:2019)
This document specifies a laboratory method for the determination of the distillation characteristics of light and middle distillates derived from petroleum and related products of synthetic or biological origin with initial boiling points above 0 °C and end-points below approximately 400 °C, utilizing either manual or automated equipment. Light distillates are typically automotive engine petrol, automotive engine ethanol fuel blends with up to 85 % (V/V) ethanol, and aviation petrol. Middle distillates are typically aviation turbine fuel, kerosene, diesel, diesel with up to 30 % (V/V) FAME, burner fuel, and marine fuels that have no appreciable quantities of residua.
NOTE For the purposes of this document, the term "% (V/V)" is used to represent the volume fraction of a material.
The distillation (volatility) characteristics of hydrocarbons and related products of synthetic or biological origin have an important effect on their safety and performance, especially in the case of fuels and solvents. The boiling range gives important information on composition and behaviour during storage and use, and the rate of evaporation is an important factor in the application of many solvents. Limiting values to specified distillation characteristics are applied to most distillate petroleum product and liquid fuel specifications in order to control end-use performance and to regulate the formation of vapours which may form explosive mixtures with air, or otherwise escape into the atmosphere as emissions (VOC).
Mineralölerzeugnisse und verwandte Produkte mit natürlichem oder synthetischem Ursprung - Bestimmung des Destillationsverlaufes bei Atmosphärendruck (ISO 3405:2019)
Dieses Dokument legt ein Laborprüfverfahren mittels manuellen als auch automatisierten Prüfgeräten zur Bestimmung des Destillationsverlaufes von aus Erdöl gewonnenen niedrig siedenden Fraktionen und Mitteldestillaten und verwandten synthetischen oder biologischen Produkten fest, die einen Destillationsbeginn über 0 °C und einen Destillationsendpunkt unter etwa 400 °C aufweisen. Niedrig siedende Fraktionen sind üblicherweise Ottokraftstoffe, Benzin Ethanol Gemische mit einem Ethanolgehalt von bis zu 85 % (V/V) und Flugzeugbenzine. Mitteldestillate sind üblicherweise Flugturbinenkraftstoffe, Kerosin, Diesel, Diesel mit Gehalten an Fettsäuremethylester (FAME) bis zu 30 % (V/V), Heizöl und Schifffahrtsbrennstoffe, die keine nennenswerten Rückstandsanteile aufweisen.
ANMERKUNG Für die Zwecke dieses Dokumentes wird zur Angabe des Volumenanteiles einer Substanz der Aus-druck „% (V/V)“ verwendet.
Der Destillationsverlauf (die Flüchtigkeit) von Kohlenwasserstoffen und verwandten Produkten mit natür-lichem oder synthetischem Ursprung hat eine große Bedeutung hinsichtlich der Sicherheit und Gebrauchs-fähigkeit, vor allem bei Kraftstoffen und Lösemitteln. Der Siedebereich gibt wichtige Informatio¬nen über die Zusammensetzung und das Verhalten bei Lagerung und Gebrauch, und die Verdampfungsrate ist ein wichtiger Faktor bei der Verwendung vieler Lösemittel. In den meisten Anforderungen für Destillate auf Mineralölbasis und flüssige Brennstoffe werden Grenzwerte für den Destillationsverlauf festgelegt, um die Endgebrauchsfähigkeit zu kontrollieren und die Bildung von Dämpfen zu begrenzen, die möglicherweise mit Luft explosionsfähige Gemische bilden oder auch als Emissionen (en: volatile organic compounds, VOC) in die Atmosphäre entweichen.
Produits pétroliers et connexes d'origine naturelle ou synthétique - Détermination des caractéristiques de distillation à pression atmosphérique (ISO 3405:2019)
Le présent document spécifie une méthode de laboratoire pour la détermination des caractéristiques de distillation des distillats pétroliers légers et moyens, ainsi que des produits connexes d'origine biologique ou synthétique, ayant un point initial de distillation supérieur à 0 °C et un point final inférieur à environ 400 °C, utilisant un équipement manuel ou automatisé. Les distillats légers habituels sont les essences pour moteur automobiles, les essences pour moteurs automobiles contenant jusqu'à 85 % (V/V) d'éthanol et l'essence aviation. Les distillats moyens habituels sont le carburéacteur, le kérosène, le gazole, le gazole contenant jusqu'à 30 % (V/V) d'EMAG, le combustible de chauffe et les combustibles pour la marine qui n'ont pas une quantité de résidus appréciable.
NOTE Pour les besoins du présent document, l'expression "% (V/V)" est utilisée pour désigner la fraction volumique des produits.
Les caractéristiques de distillation (volatilité) des hydrocarbures et des produits connexes d'origine synthétique ou biologique sont importantes en matière de sécurité et de performances, en particulier dans le cas des carburants et des solvants. L'intervalle de distillation donne des renseignements importants sur la composition et le comportement pendant le stockage et l'utilisation, et la vitesse d'évaporation est une caractéristique essentielle dans l'utilisation de nombreux solvants. La plupart des spécifications applicables aux distillats pétroliers et aux carburants liquides fixent des valeurs limites pour certaines caractéristiques de distillation, afin de mieux maîtriser les performances en utilisation et pour contrôler la formation de vapeurs qui pourraient devenir explosives en présence d'air ou s'échapper dans l'atmosphère (COV).
Naftni in sorodni proizvodi iz naravnih ali sintetičnih virov - Določevanje destilacijskih značilnosti pri atmosferskem tlaku (ISO 3405:2019)
Ta dokument določa laboratorijsko metodo za določanje destilacijskih značilnosti lahkih in srednjih destilatov iz naftnih in sorodnih proizvodov iz naravnih ali sintetičnih virov z začetnim vreliščem nad 0 °C in končno točko pod približno 400 °C pri uporabi ročne ali avtomatske opreme. Lahki destilati so običajno bencin za avtomobilski motor, mešanice z etanolom za avtomobilski motor z do 85-odstotno (V/V) vsebnostjo etanola in letalsko gorivo. Srednji destilati so običajno gorivo za letalske turbine, kerozin, dizel, dizel z do 30-odstotno (V/V) vsebnostjo metilnih estrov maščobnih kislin, kurilno olje in ladijska goriva, ki nimajo znatne količine ostankov.
OPOMBA: Za namene tega dokumenta se termin »% (V/V)« uporablja za prostorninski delež snovi.
Destilacijske značilnosti (hlapnost) ogljikovodikov in sorodnih proizvodov iz sintetičnih ali naravnih virov imajo pomemben učinek na njihovo varnost in lastnosti, predvsem v primeru goriv in topil. Območje vrelišča je pomembna informacija o sestavi in vedenju med skladiščenjem in uporabo, stopnja izhlapevanja pa je pomemben dejavnik pri uporabi številnih topil. Mejne vrednosti določenih destilacijskih značilnosti se uporabljajo za večino destiliranih naftnih proizvodov in specifikacij tekočih goriv, da bi nadzorovali končne lastnosti in nastajanje hlapov, ki lahko z zrakom tvorijo eksplozivne zmesi, ali kako drugače preidejo v atmosfero kot emisije (VOC).
General Information
Relations
Standards Content (Sample)
SLOVENSKI STANDARD
01-julij-2019
Nadomešča:
SIST EN ISO 3405:2011
Naftni in sorodni proizvodi iz naravnih ali sintetičnih virov - Določevanje
destilacijskih značilnosti pri atmosferskem tlaku (ISO 3405:2019)
Petroleum and related products from natural or synthetic sources - Determination of
distillation characteristics at atmospheric pressure (ISO 3405:2019)
Mineralölerzeugnisse und verwandte Produkte mit natürlichem oder synthetischem
Ursprung - Bestimmung des Destillationsverlaufes bei Atmosphärendruck (ISO
3405:2019)
Produits pétroliers et connexes d'origine naturelle ou synthétique - Détermination des
caractéristiques de distillation à pression atmosphérique (ISO 3405:2019)
Ta slovenski standard je istoveten z: EN ISO 3405:2019
ICS:
75.080 Naftni proizvodi na splošno Petroleum products in
general
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EN ISO 3405
EUROPEAN STANDARD
NORME EUROPÉENNE
May 2019
EUROPÄISCHE NORM
ICS 75.080 Supersedes EN ISO 3405:2011
English Version
Petroleum and related products from natural or synthetic
sources - Determination of distillation characteristics at
atmospheric pressure (ISO 3405:2019)
Produits pétroliers et connexes d'origine naturelle ou Mineralölerzeugnisse und verwandte Produkte mit
synthétique - Détermination des caractéristiques de natürlichem oder synthetischem Ursprung -
distillation à pression atmosphérique (ISO 3405:2019) Bestimmung des Destillationsverlaufes bei
Atmosphärendruck (ISO 3405:2019)
This European Standard was approved by CEN on 7 March 2019.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2019 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 3405:2019 E
worldwide for CEN national Members.
Contents Page
European foreword . 3
European foreword
This document (EN ISO 3405:2019) has been prepared by Technical Committee ISO/TC 28 "Petroleum
and related products, fuels and lubricants from natural or synthetic sources" in collaboration with
Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related products of
petroleum, synthetic and biological origin.” the secretariat of which is held by NEN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by November 2019, and conflicting national standards
shall be withdrawn at the latest by November 2019.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 3405:2011.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 3405:2019 has been approved by CEN as EN ISO 3405:2019 without any modification.
INTERNATIONAL ISO
STANDARD 3405
Fifth edition
2019-03
Petroleum and related products
from natural or synthetic sources —
Determination of distillation
characteristics at atmospheric
pressure
Produits pétroliers et connexes d'origine naturelle ou synthétique —
Détermination des caractéristiques de distillation à pression
atmosphérique
Reference number
ISO 3405:2019(E)
©
ISO 2019
ISO 3405:2019(E)
© ISO 2019
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ii © ISO 2019 – All rights reserved
ISO 3405:2019(E)
Contents Page
Foreword .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 3
5 Apparatus . 3
5.1 General . 3
5.2 Distillation flasks . 4
5.3 Condenser tube and cooling bath . 4
5.4 Metal shield or enclosure for flask (manual apparatus only) . 4
5.5 Heat source(s) . 8
5.6 Flask-support . 8
5.7 Graduated cylinders . 9
5.8 Temperature measurement system .10
5.9 Centring device .10
5.10 Barometer .10
6 Samples and sampling .12
6.1 Sample grouping .12
6.2 Sample maintenance prior to testing .12
6.2.1 General.12
6.2.2 Groups 1 and 2 .13
6.2.3 Groups 3 and 4 .13
6.3 Removing water from sample .13
6.3.1 General.13
6.3.2 Groups 1 and 2 .14
6.3.3 Groups 3 and 4 .14
7 Preparation of apparatus .14
8 Apparatus verification .16
8.1 Level follower .16
8.2 Electronic temperature-measurement devices .16
8.3 Electronic pressure measuring device .17
9 Procedure — Manual apparatus .17
10 Procedure — Automated apparatus .20
11 Calculations.21
12 Expression of results .24
13 Precision (Manual Apparatus) .25
13.1 General .25
13.2 Repeatability .26
13.3 Reproducibility .26
14 Precision (automated apparatus).27
14.1 General .27
14.2 Repeatability .
...
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