EN 15510:2007

Animal feeding stuffs - Determination of calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum, arsenic, lead and cadmium by ICP-AES

This European Standard specifies inductively coupled plasma atomic emission spectroscopy (ICP-AES) method for the determination of:
-   minerals calcium, sodium, phosphorus, magnesium and potassium and the elements iron, zinc, copper, manganese, cobalt, molybdenum in animal feeding stuffs,
-   elements arsenic, lead and cadmium in minerals on their own, in pre-mixtures or mixtures for use in animal nutrition.
The method detection limit for each element is dependent on the sample matrix as well as of the instrument. The method is not applicable for determination of low concentrations of elements. The limit of quantification should be 3 mg/kg or lower.
NOTE   This method can also be used for the determination of minerals in products with high mineral content (> 5%), yet for this purpose, other more precise analytical techniques are available.

Futtermittel - Bestimmung von Calcium, Natrium, Phosphor, Magnesium, Kalium, Eisen, Zink, Kupfer, Mangan, Cobalt, Molybdän, Arsen, Blei und Cadmium mittels ICP-AES

Diese Europäische Norm legt ein Verfahren mittels Atomemissionsspektrometrie mit induktiv gekoppeltem Plasma (ICP AES) zur Bestimmung von
   den Mineralstoffen Calcium, Natrium, Phosphor, Magnesium und Kalium und den Elementen Eisen, Zink, Kupfer, Mangan, Cobalt und Molybdän in Futtermitteln,
   den Elementen Arsen, Blei und Cadmium in Mineralien für sich allein, in Vormischungen und Mischungen für die Anwendung in Tiernahrung
fest.
Die Nachweisgrenze des Verfahrens hängt bei jedem Element sowohl von der Probenmatrix als auch von dem Gerät ab. Das Verfahren ist nicht für die Bestimmung von geringen Elementkonzentrationen anwendbar. Die Bestimmungsgrenze sollte bei 3 mg/kg oder niedriger liegen.
ANMERKUNG   Dieses Verfahren kann für die Bestimmung von Mineralstoffen in Produkten mit einem hohen Mineral¬stoffgehalt (> 5 %) eingesetzt werden, für diesen Zweck stehen aber auch andere genauere Analysenverfahren zur Verfügung.

Aliments des animaux - Détermination des teneurs en calcium, sodium, phosphore, magnésium, potassium, fer, zinc, cuivre, manganèse, cobalt, molybdène, arsenic, plomb et cadmium par ICP-AES

La présente Norme européenne spécifie une méthode de spectrométrie d'émission atomique à plasma à couplage inductif (ICP-AES) pour la détermination de la teneur en :
   minéraux (calcium, sodium, phosphore, magnésium et potassium) et en éléments (fer, zinc, cuivre, manganèse, cobalt, molybdène) dans les aliments pour animaux ;
   éléments (arsenic, plomb et cadmium) dans des minéraux purs, dans des pré-mélanges ou des mélanges utilisés pour nourrir des animaux.
La limite de détection de la méthode pour chacun des éléments est fonction de la matrice de l'échantillon et de l'instrument. Cette méthode ne permet pas la détermination des éléments en faibles concentrations. Il convient que la limite de quantification soit de 3 mg/kg ou moins.
NOTE   La présente méthode peut être utilisée pour la détermination de la teneur en minéraux dans les produits à forte concentration minérale ( 5 %). D'autres techniques d’analyse plus précises sont néanmoins applicables pour ce genre de détermination.

Krma - Določevanje kalcija, natrija, fosforja, magnezija, kalija, železa, cinka, bakra, mangana, kobalta, molibdena, arzena, svinca in kadmija z ICP-AES

General Information

• Status: Withdrawn
• Publication Date: 31-Jul-2007
• Withdrawal Date: 08-Aug-2017
• ICS: 65.120 - Animal feeding stuffs
• Technical Committee: CEN/TC 327 - Animal feeding stuffs - Methods of sampling and analysis
• Drafting Committee: CEN/TC 327/WG 1 - Minerals and Contaminants
• Current Stage: 9960 - Withdrawal effective - Withdrawal
• Completion Date: 09-Aug-2017
• Directive: 1999/29/EC - Council Directive 1999/29/EC of 22 April 1999 on the undesirable substances and products in animal nutrition
• Directive: 70/373/EC - Council Directive 70/373/EEC of 20 July 1970 on the introduction of Community methods of sampling and analysis for the official control of feeding-stuffs
• Mandate: M/315 - Mandate to CEN for standardization in the field of methods of analysis for animal feedingstuffs
• Ref Project: SIST EN 15510:2007 - Animal feeding stuffs - Determination of calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum, arsenic, lead and cadmium by ICP-AES

Relations

• Replaced By: EN 15510:2017 - Animal feeding stuffs: Methods of sampling and analysis - Determination of calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum and lead by ICP-AES
• Effective Date: 16-Aug-2017

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Animal feeding stuffs - Determination of calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum, arsenic, lead and cadmium by ICP-AESAliments des animaux - Détermination des teneurs en calcium, sodium, phosphore, magnésium, potassium, fer, zinc, cuivre, manganese, cobalt, molybdene, arsenic, plomb et cadmium par ICP-AESFuttermittel - Bestimmung von Calcium, Natrium, Phosphor, Magnesium, Kalium, Eisen, Zink, Kupfer, Mangan, Cobalt, Molybdän, Arsen, Blei und Cadmium mittels ICP-AESTa slovenski standard je istoveten z:EN 15510:2007SIST EN 15510:2007en,fr,de65.120KrmilaAnimal feeding stuffsICS:SLOVENSKI
STANDARDSIST EN 15510:200701-november-2007







EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 15510August 2007ICS 65.120 English VersionAnimal feeding stuffs - Determination of calcium, sodium,phosphorus, magnesium, potassium, iron, zinc, copper,manganese, cobalt, molybdenum, arsenic, lead and cadmium byICP-AESAliments des animaux - Détermination des teneurs encalcium, sodium, phosphore, magnésium, potassium, fer,zinc, cuivre, manganèse, cobalt, molybdène, arsenic,plomb et cadmium par ICP-AESFuttermittel - Bestimmung von Calcium, Natrium,Phosphor, Magnesium, Kalium, Eisen, Zink, Kupfer,Mangan, Cobalt, Molybdän, Arsen, Blei und Cadmiummittels ICP-AESThis European Standard was approved by CEN on 30 June 2007.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2007 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 15510:2007: E



EN 15510:2007 (E) 2 Contents Page Foreword.3 1 Scope.4 2 Normative references.4 3 Terms and definitions.4 4 Principle.5 5 Reagents.5 6 Apparatus, usual laboratory apparatus and, in particular, the following.7 7 Sampling.7 8 Preparation of the test sample.8 9 Procedure.9 10 Calculation and expression of the result.13 11 Precision.15 12 Test report.20 Annex A (informative)
Results of the interlaboratory test.21 Annex B (informative)
Notes on the detection technique, interferences and quantification.26 Bib
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