Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)

ISO 6498:2012 specifies guidelines for the preparation of test samples from laboratory samples of animal feeding stuffs, including pet foods.
The guidelines are overruled by special instructions and regulations for sample preparation demanded by specific analysis methods.

Futtermittel - Leitfaden für die Probenvorbereitung (ISO 6498:2012)

Diese Internationale Norm legt einen Leitfaden zur Herstellung von Untersuchungsproben aus Laboratoriums-proben von Tierfuttermitteln, einschließlich Futtermitteln für Heimtiere fest.
ANMERKUNG 1   Der Leitfaden leitet sich am häufigsten von den Richtlinien des AAFCO (en: Association of American Feed Control Officials) (Verband amerikanischer Kontrollbehörden für Futtermittel) ab (siehe Literaturhinweis [7]).
Der Leitfaden wird von speziellen Anweisungen und Vorschriften zur Probenvorbereitung aufgehoben, die durch spezifische Analysenverfahren gefordert werden.
ANMERKUNG 2   Solche Analyseverfahren werden von ISO und CEN entwickelt.
ANMERKUNG 3   Diese Internationale Norm enthält keinen speziellen Leitfaden zur Probenvorbereitung für die mikrobiologische Analyse von Mikroorganismen, wie z. B. Hefen, Bakterien und Schimmelpilze. Trotzdem sind für Mikroorganismen, die als Futtermittelzusätze (Probiotika) verwendet werden, einige wichtige Gesichtspunkte zur Proben¬vorbereitung genannt.

Aliments des animaux - Lignes directrices pour la préparation des échantillons (ISO 6498:2012)

L'ISO 6498:2012 spécifie des lignes directrices pour la préparation des échantillons pour essai d'aliments pour animaux, y compris les animaux domestiques, à partir des échantillons pour laboratoire.
Les lignes directrices sont annulées par des instructions et des règlements particuliers pour la préparation des échantillons exigés par les méthodes d'analyse spécifiques des aliments pour animaux.

Krma - Smernice za pripravo vzorca (ISO 6498:2012)

Ta mednarodni standard določa smernice za pripravo preskusnih vzorcev iz laboratorijskih vzorcev krme, vključno s hrano za hišne ljubljenčke. Posebne analizne metode vključujejo posebna navodila in predpise, ki se uporabljajo namesto teh smernic.

General Information

Status
Published
Publication Date
31-May-2012
Withdrawal Date
30-Dec-2012
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
01-Jun-2012
Due Date
07-Nov-2011
Completion Date
01-Jun-2012

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Standards Content (Sample)


SLOVENSKI STANDARD
01-oktober-2012
Krma - Smernice za pripravo vzorca (ISO 6498:2012)
Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)
Futtermittel - Leitfaden für die Probenvorbereitung (ISO 6498:2012)
Aliments des animaux - Lignes directrices pour la préparation d'échantillons (ISO
6498:2012)
Ta slovenski standard je istoveten z: EN ISO 6498:2012
ICS:
65.120 Krmila Animal feeding stuffs
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EUROPEAN STANDARD
EN ISO 6498
NORME EUROPÉENNE
EUROPÄISCHE NORM
June 2012
ICS 65.120
English Version
Animal feeding stuffs - Guidelines for sample preparation (ISO
6498:2012)
Aliments des animaux - Lignes directrices pour la Futtermittel - Leitfaden für die Probenvorbereitung (ISO
préparation des échantillons (ISO 6498:2012) 6498:2012)
This European Standard was approved by CEN on 31 May 2012.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same
status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2012 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 6498:2012: E
worldwide for CEN national Members.

Contents Page
Foreword .3
Foreword
This document (EN ISO 6498:2012) has been prepared by Technical Committee CEN/TC 327 “Animal feeding
stuffs - Methods of sampling and analysis", the secretariat of which is held by NEN, in collaboration with
Technical Committee ISO/TC 34 "Food products".
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by December 2012, and conflicting national standards shall be withdrawn
at the latest by December 2012.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
According to the CEN/CENELEC Internal Regulations, the national standards organisations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
Sweden, Switzerland, Turkey and the United Kingdom.
INTERNATIONAL ISO
STANDARD 6498
Third edition
2012-06-01
Corrected version
2012-07-15
Animal feeding stuffs — Guidelines for
sample preparation
Aliments des animaux — Lignes directrices pour la préparation des
échantillons
Reference number
ISO 6498:2012(E)
©
ISO 2012
ISO 6498:2012(E)
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means,
electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO’s
member body in the country of the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2012 – All rights reserved

ISO 6498:2012(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Terms and definitions . 1
2.1 Definitions concerning “sample” . 1
2.2 Definitions concerning “parameters” . 2
2.3 Examples of animal feeding stuffs characteristics . 3
2.4 Definitions concerning “sample preparation procedure” . 5
3 Principle . 6
4 Consideration of sample preparation errors . 7
4.1 Subsampling and other errors . 7
4.2 Minimum mass . 8
4.3 Errors associated with division techniques . 9
5 Safety precautions .10
6 Apparatus .10
7 Procedure .12
7.1 General .12
7.2 Sample check .12
7.3 Mass reduction .14
7.4 Particle size reduction .17
7.5 Partial drying .20
7.6 Coarse grinding .22
7.7 Special sample preparation procedures .22
7.8 Storage .22
8 Performance tests (quality control) .22
8.1 General .22
8.2 Performance test for mass reduction (division) .23
8.3 Performance test for particle size reduction (grinding) .24
8.4 Performance test for mixing .25
9 Categories of feeds — Special remarks and flow charts .25
9.1 General .25
9.2 Birdseed .26
9.3 Whole cottonseed .27
9.4 Mineral mix .29
9.5 Dry feeds .29
9.6 Forages including silage, hay, haylage, TMR and byproducts .30
9.7 Oilseeds and high-fat feeds .32
9.8 Large block and molasses block feeds .33
9.9 Liquid feeds .35
9.10 Canned pet food .35
9.11 Semi-moist pet food and dog chews.36
9.12 Premixtures .37
9.13 Range and alfalfa hay pellets .38
9.14 Texturized and sticky feed .39
9.15 Aquatic feeds .40
Annex A (informative) Calculations, examples and tables for minimum mass .42
Bibliography .46
ISO 6498:2012(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International
Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 6498 was prepared by the European Committee for Standardization (CEN) Technical Committee TC 327,
Animal feeding stuffs — Methods of sampling and analysis, in collaboration with ISO Technical Committee
TC 34, Food products, Subcommittee SC 10, Animal feeding stuffs, in accordance with the Agreement on
technical cooperation between ISO and CEN (Vienna Agreement).
This third edition cancels and replaces the second edition (ISO 6498:1998), which has been technically revised.
This corrected version of ISO 6498:2012 incorporates the following correction: in 7.1, paragraph 4, the phrase
“particle sizes below 4 mm ± 2 mm (4 mm to 6 mm) can be” has been substituted by “particle sizes of 4 mm to
6 mm can be”.
iv © ISO 2012 – All rights reserved

INTERNATIONAL STANDA
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