CEN ISO/TR 19402:2020

Paints and varnishes - Adhesion of coatings (ISO/TR 19402:2018)

This document summarises the common methods for evaluating the adhesive strength of coatings on a substrate, which can be another coating beneath or the substrate itself. The test methods and evaluation methods are described in Clauses 4, 5, and 6. In the case of standardized test methods the respective standard is referenced in regard to procedure and evaluation. Annex A compares the methods in the synoptic Tables A.1, A.2, and A.3.
Often the adhesive strength cannot be sufficiently evaluated by means of a single method.
The purely physical methods for measuring the adhesive strength are such in which mechanical quantities (e.g. force or torsion moment) are measured directly.
All other methods are based on the evaluation of behaviour under mechanic stress according to practical conditions. For these methods the viscoelastic properties have a wide influence on the evaluation of the adhesive strength, so that it can only be tested comparatively within one method.
Each method has its specific application. An unsuitable method can lead to false information. All of the test methods for the evaluation of the adhesive strength require a certain routine of the test person, especially in regard to identifying the separation line. For most of the test methods the test results, among other things, depend on the film thickness of the coating to be tested. In addition, for several methods differences between tests on a test sheet and in practice can occur, due to different roughness of the substrate.
Effects of delamination caused by weathering or corrosion influences are not subject of this document.
In case cohesion failures predominantly occur during an adhesive strength test, this is no measure for the adhesive strength. However, information can be given on the protective effect of the coating against corrosion.

Beschichtungsstoffe - Haftfestigkeit von Beschichtungen (ISO/TR 19402:2018)

Dieses Dokument fasst die gebräuchlichen Verfahren zum Beurteilen der Haftfestigkeit von Beschichtungen auf einem Untergrund, wobei dieser eine darunterliegende Beschichtung oder das Substrat sein kann, zusammen. Die Prüf- und Auswerteverfahren werden im Abschnitt 4, Abschnitt 5 und Abschnitt 6 beschrieben. Im Fall von genormten Prüfverfahren wird für die Durchführung und Auswertung auf die entsprechenden Normen verwiesen. Im Anhang A werden die Verfahren in Übersichtstabelle A.1, Übersichtstabelle A.2 und Übersichtstabelle A.3 vergleichend gegenübergestellt.
Die Haftfestigkeit lässt sich meistens nicht ausreichend mit nur einem Verfahren beurteilen.
Die rein physikalischen Verfahren zum Messen der Haftfestigkeit sind solche, bei denen direkt mechanische Größen (z. B. Kraft oder Drehmoment) gemessen werden.
Alle übrigen Verfahren beruhen auf der Beurteilung des Verhaltens bei mechanischer Beanspruchung in Anlehnung an praktische Bedingungen. Bei diesen Verfahren haben die viskoelastischen Eigenschaften einen großen Einfluss auf die Beurteilung der Haftfestigkeit, so dass nur vergleichend innerhalb eines Verfahrens geprüft werden kann.
Jedes Verfahren hat seine spezifische Anwendung. Ein ungeeignetes Verfahren kann zu einer falschen Aussage führen. Alle Prüfverfahren zum Beurteilen der Haftfestigkeit erfordern eine gewisse Übung des Prüfers, insbesondere beim Erkennen der Trennebene. Bei den meisten Prüfverfahren sind die Prüf-ergebnisse u. a. von der Schichtdicke der zu untersuchenden Beschichtung abhängig. Außerdem können bei einigen Verfahren auf Grund der unterschiedlichen Rauheit des Untergrundes Unterschiede zwischen Prüfungen auf einem Probenblech und der Praxis auftreten.
Enthaftungseffekte, die durch Bewitterungs- und Korrosionseinflüsse hervorgerufen werden, sind nicht Gegenstand dieses Dokumentes.
Wenn bei einer Haftfestigkeitsprüfung vorwiegend Kohäsionsbrüche auftreten, ist dies kein Maß für die Haftfestigkeit, es kann jedoch eine Aussage über die Schutzwirkung der Beschichtung gegen Korrosion getroffen werden.

Peintures et vernis - Adhérence des revêtements (ISO/TR 19402:2018)

Barve in laki - Oprijemljivost premazov (ISO/TR 19402:2018)

General Information

• Status: Published
• Publication Date: 06-Oct-2020
• ICS: 87.040 - Paints and varnishes
• Technical Committee: CEN/TC 139 - Paints and varnishes
• Drafting Committee: CEN/TC 139 - Paints and varnishes
• Current Stage: 6060 - Definitive text made available (DAV) - Publishing
• Start Date: 07-Oct-2020
• Due Date: 25-Nov-2021
• Completion Date: 07-Oct-2020
• Ref Project: SIST-TP CEN ISO/TR 19402:2020 - Paints and varnishes - Adhesion of coatings (ISO/TR 19402:2018)

Overview

CEN ISO/TR 19402:2020 (identical to ISO/TR 19402:2018) is a technical report for paints and varnishes that summarises commonly used methods to assess the adhesion of coatings and the adhesive strength between a coating and its substrate (or between coating layers). The document describes test procedures and evaluation approaches (Clauses 4–6) and provides synoptic comparison tables (Annex A, Tables A.1–A.3) to help users select the most appropriate paint adhesion test for their situation.

Key technical topics and requirements

• Scope and purpose: Guidance on selecting and interpreting adhesion test methods for coatings, not a single prescriptive test.
• Test families covered: Mechanical stress tests (e.g. pull-off, twist-off, peel), deformation tests (bend, cupping, T-bend, three-point bend), impact tests (single- and multi-impact, falling‑weight), and scratch / cross-cut methods.
• Evaluation methods: Visual assessment, failure pattern analysis, area comparison, and instrumental techniques including digital image evaluation and contrasting methods.
• Practical limitations:
  • Many methods are influenced by the viscoelastic properties of the coating and therefore are generally comparative within a given method.
  • Test results often depend on film thickness, substrate roughness and operator routine (especially in identifying the separation line).
  • Cohesion failures (coating breaks within itself) do not directly indicate adhesive strength but can give information on protective performance.
  • Effects of weathering or corrosion-induced delamination are outside the scope of this report.
• Selection guidance: Annex A’s synoptic tables compare applicability, sensitivity and typical outcomes to reduce the risk of using an unsuitable method.

Practical applications and who uses this standard

• Quality control laboratories in paint and coating manufacturing use the guidance to choose appropriate adhesion tests for production batches.
• R&D teams developing new coatings apply the report to select complementary tests that characterize adhesion under intended service stresses.
• Specifiers and coating applicators (architects, industrial coating contractors) use it to verify field performance correlations and select suitable test methods for acceptance criteria.
• Failure analysts and corrosion engineers use the evaluation guidance to interpret test outcomes and distinguish adhesion vs cohesion issues.

Keywords: CEN ISO/TR 19402:2020, ISO/TR 19402:2018, paints and varnishes, adhesion of coatings, adhesive strength, pull-off test, cross‑cut test, scratch test, peel test, impact test, evaluation methods.

Related standards

The report references respective standardized test methods for detailed procedures and evaluation criteria; users should consult the referenced standards for specific test apparatus, calibration and pass/fail criteria.

Standards Content (Sample)

SLOVENSKI STANDARD
01-december-2020
Barve in laki - Oprijemljivost premazov (ISO/TR 19402:2018)
Paints and varnishes - Adhesion of coatings (ISO/TR 19402:2018)
Beschichtungsstoffe - Haftfestigkeit von Beschichtungen (ISO/TR 19402:2018)
Peintures et vernis - Adhérence des revêtements (ISO/TR 19402:2018)
Ta slovenski standard je istoveten z: CEN ISO/TR 19402:2020
ICS:
87.040 Barve in laki Paints and varnishes
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

CEN ISO/TR 19402
TECHNICAL REPORT
RAPPORT TECHNIQUE
October 2020
TECHNISCHER BERICHT
ICS 87.040
English Version
Paints and varnishes - Adhesion of coatings (ISO/TR
19402:2018)
Peintures et vernis - Adhérence des revêtements Beschichtungsstoffe - Haftfestigkeit von
(ISO/TR 19402:2018) Beschichtungen (ISO/TR 19402:2018)

This Technical Report was approved by CEN on 4 October 2020. It has been drawn up by the Technical Committee CEN/TC 139.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2020 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN ISO/TR 19402:2020 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
The text of ISO/TR 19402:2018 has been prepared by Technical Committee ISO/TC 35 "Paints and
varnishes” of the International Organization for Standardization (ISO) and has been taken over as
which is held by DIN.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
Endorsement notice
The text of ISO/TR 19402:2018 has been approved by CEN as CEN ISO/TR 19402:2020 without any
modification.
TECHNICAL ISO/TR
REPORT 19402
First edition
2018-08
Paints and varnishes — Adhesion of
coatings
Peintures et vernis — Adhérence des revêtements
Reference number
ISO/TR 19402:2018(E)
©
ISO 2018
ISO/TR 19402:2018(E)
© ISO 2018
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: [phone]
Fax: [phone]
Email: [e-mail]
Website: www.iso.org
Published in Switzerland
ii © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
Contents Page
Foreword .v
Introduction .vi
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Adhesive strength tests without scratch/cut . 3
4.1 Tests with mechanical stress application on the coating . 3
4.1.1 Pull-off test . 3
4.1.2 Twist-off test . 5
4.1.3 Peel-off test 1 . 6
4.1.4 Peel-off test 2 . 8
4.2 Tests with continuous deformation of test specimens . 9
4.2.1 Bend test with a wedge-shaped conical mandrel . 9
4.2.2 Bend test with a conical mandrel .11
4.2.3 Bend test with a cylindrical mandrel 1 .12
4.2.4 Bend test with a cylindrical mandrel 2 .14
4.2.5 Three point bending method .15
4.2.6 T-bend test 1 .17
4.2.7 T-bend test 2 .19
4.2.8 Cupping test 1 .20
4.3 Test with impact stress application .22
4.3.1 Single-impact test 1 .22
4.3.2 Single-impact test 2 .25
4.3.3 Single-impact test 3 .27
4.3.4 Single-impact test 4 .28
4.3.5 Falling-weight test 1 .30
4.3.6 Falling-weight test 2 .33
4.3.7 Falling-weight test 3 .35
4.3.8 Multi-impact test 1 .36
4.3.9 Multi-impact test 2 .38
4.3.10 Multi-impact test 3 .41
4.3.11 Multi-impact test 4 .43
4.3.12 Impact-bend test .44
5 Adhesive strength tests with scratch/cut .45
5.1 Tests with single scratch .45
5.1.1 Scratch test 1 .45
5.1.2 Scratch test 2 .46
5.1.3 Scratch test 3 (Scrape-adhesion test) .47
5.2 Test with multiple scratch (without deformation of test specimens) .49
5.2.1 Pressure-water jetting test .49
5.2.2 Cross-cut test 1 .53
5.2.3 Cross-cut test 2 .56
5.2.4 Cross-cut test 3 .57
5.2.5 X-cut test 1 .58
5.2.6 X-cut test 2 .58
5.2.7 X-cut test 3 .59
5.2.8 X-cut test 4 .59
5.2.9 Scribe test with a square-diagonal grid .60
5.2.10 Scribe test with a rhombus grid .61
5.3 Test with multiple scratch (with deformation of test specimens) .62
5.3.1 Cupping test 2 .62
6 Evaluation methods for adhesive strength .63
ISO/TR 19402:2018(E)
6.1 Auxiliary methods .63
6.1.1 Contrasting 1 .63
6.1.2 Contrasting 2 .64
6.2 Visual methods.64
6.2.1 Failure pattern analysis.64
6.2.2 Comparison of areas .65
6.2.3 General assessment .66
6.3 Instrumental methods .67
6.3.1 Digital image evaluation 1 .67
6.3.2 Digital image evaluation 2 .67
Annex A Synoptical tables for the methods.69
Bibliography .76
iv © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to the
World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following
URL: www .iso .org/iso/foreword .html.
This document was prepared by Technical Committee ISO/TC 35, Paints and varnishes, Subcommittee
SC 9, General test methods for paints and varnishes.
ISO/TR 19402:2018(E)
Introduction
The determination of the adhesive strength is one of the most important preconditions for evaluating
the protective function of coatings.
This document offers a helpful overview for the selection of the test method most suitable for each
individual case in regard to the evaluation of the adhesive strength.
vi © ISO 2018 – All rights reserved

TECHNICAL REPORT ISO/TR 19402:2018(E)
Paints and varnishes — Adhesion of coatings
1 Scope
This document summarises the common methods for evaluating the adhesive strength of coatings on a
substrate, which can be another coating beneath or the substrate itself. The test methods and evaluation
methods are described in Clauses 4, 5, and 6. In the case of standardized test methods the respective
standard is referenced in regard to procedure and evaluation. Annex A compares the methods in the
synoptic Tables A.1, A.2, and A.3.
Often the adhesive strength cannot be sufficiently evaluated by means of a single method.
The purely physical methods for measuring the adhesive strength are such in which mechanical
quantities (e.g. force or torsion moment) are measured directly.
All other methods are based on the evaluation of behaviour under mechanic stress according to practical
conditions. For these methods the viscoelastic properties have a wide influence on the evaluation of the
adhesive strength, so that it can only be tested comparatively within one method.
Each method has its specific application. An unsuitable method can lead to false information. All of the
test methods for the evaluation of the adhesive strength require a certain routine of the test person,
especially in regard to identifying the separation line. For most of the test methods the test results,
among other things, depend on the film thickness of the coating to be tested. In addition, for several
methods differences between tests on a test sheet and in practice can occur, due to different roughness
of the substrate.
Effects of delamination caused by weathering or corrosion influences are not subject of this document.
In case cohesion failures predominantly occur during an adhesive strength test, this is no measure for
the adhesive strength. However, information can be given on the protective effect of the coating against
corrosion.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 4618, Paints and varnishes — Terms and definitions
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO 4618 and the following apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https: //www .iso .org/obp
— IEC Electropedia: available at http: //www .electropedia .org/
3.1
adhesion
phenomenon of attachment at the interface between a solid surface and another material caused by
molecular forces
Note 1 to entry: Adhesion should not be confused with cohesion.
ISO/TR 19402:2018(E)
[SOURCE: ISO 4618:2014, 2.7]
3.2
cohesion
forces that bind a film or coat into an integral entity
Note 1 to entry: Cohesion should not be confused with adhesion.
[SOURCE: ISO 4618:2014, 2.55]
3.3
adhesion failure
detachment of a coating from the substrate caused by external forces
Note 1 to entry: The substrate can be another coating beneath or the working material.
3.4
cohesion failure
loss of coherence within a coating caused by external forces
3.5
adhesive strength
force required to detach a coating from a substrate or another coating
[SOURCE: ISO 4618:2014, 2.8]
3.6
wet adhesive strength
adhesive strength (3.5) immediately after previous exposure to moisture
3.7
separation line
interface in which adhesion failure (3.3) occurs
3.8
failure pattern
entirety of the visual coating defects, which are caused by an adhesive strength (3.5) test
3.9
failure pattern assessment
classification of a failure pattern (3.8) by means of criteria or reference patterns
3.10
failure pattern analysis
quantitative evaluation of a failure pattern (3.8) with specification of the relative percentages of area
for adhesion failure (3.3) and cohesion failure (3.4) as well as the separation line(s)
3.11
main separation line
separation line with the largest area
3.12
repeatability conditions
conditions where independent test results are obtained with the same method on identical test items
in the same laboratory by the same operator using the same equipment within short intervals of time
[SOURCE: ISO 5725-1:1994, 3.14]
2 © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
3.13
repeatability limit
r
the value less than or equal to which the absolute difference between two test results obtained under
repeatability conditions (3.12) may be expected to be with a probability of 95 %
[SOURCE: ISO 5725-1:1994, 3.16]
3.14
reproducibility conditions
conditions where independent test results are obtained with the same method on identical test items in
different laboratories with different operators using different equipment
[SOURCE: ISO 5725-1:1994, 3.18]
3.15
reproducibility limit
R
the value less than or equal to which the absolute difference between two test results obtained under
reproducibility conditions (3.14) may be expected to be with a probability of 95 %
[SOURCE: ISO 5725-1:1994, 3.20]
4 Adhesive strength tests without scratch/cut
4.1 Tests with mechanical stress application on the coating
4.1.1 Pull-off test
— Principle
A uniformly increasing tensile force is applied to a test cylinder (metal cylinder of diameter
20 mm), which is adhered to the coating, until the test cylinder is pulled off. The pull-off strength
is determined by calculating the tensile force to pull off the test cylinder and the area of the test
cylinder.
The principle of the pull-off test is illustrated schematically in Figure 1.
ISO/TR 19402:2018(E)
Key
1 substrate
2 coating
3 adhesive film
4 free punch
5 test cylinder
6 outer ring to support the test panel
a
The pull-off direction.
Figure 1 — Principle of the pull-off test
— Application
The pull-off test is generally applicable.
— Procedure
— Attach the test cylinder to the coating by means of a previously tested adhesive.
— Cut the coating around the circumference of the test cylinder using a suitable tool through to
the substrate (see Figure 1).
— Attach the test specimen to the test apparatus so that it is supported and the test cylinder is
connected to the pulling unit, centred and without being wedged.
— Carry out the pull-off process with a uniformly increasing tensile force and measure when the
test cylinder is pulled off.
— Evaluation
The test result is the pull-off strength (MPa) = the tensile force when pulling off the test cylinder
divided by the area of the test cylinder.
Specify the result of the failure pattern analysis (see the procedure specified in 6.2.1).
— Precision
Precision data are not available at present.
— Reference
The pull-off test is specified in ISO 4624 and ISO 16276-1.
4 © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
4.1.2 Twist-off test
— Principle
By means of a motor-driven test apparatus a uniformly increasing torsion moment is introduced to
a test cylinder (a metal cylinder of a 12 mm or 15 mm diameter and a 6 mm drill), which is adhered
to the coating, until it is twisted off. The adhesive strength (“shear strength”) can be read directly
from the test apparatus as shear stress (N/mm = MPa).
Figure 2 illustrates the principle of the twist-off test in a schematic diagram. Figure 3 shows the
minimum distance between the test cylinders for repeated tests.
Key
1 substrate
2 coating
3 adhesive
4 test cylinder
a
The axis of rotation.
Figure 2 — Principle of the twist-off test
Figure 3 — Minimum distance between the test cylinders
— Application
The twist-off test is generally applicable.
— Procedure
— Use a sufficiently thick substrate (minimum 0,7 mm) or a substrate with reinforcement adhered
to the backside in order to avoid deformation during testing.
— Adhere the test cylinder to the coating using a previously tested adhesive. For repeated tests
observe a minimum distance between the test cylinders (see Figure 3).
ISO/TR 19402:2018(E)
— Attach the test apparatus at the hexagon bolt of the test cylinder (see Figure 2) and secure the
test panel against twisting.
— Start torsional stress and read the shear stress from the apparatus when the test cylinder is
twisted off.
— Evaluation
The test result is the shear stress (N/mm = MPa), which is read from the apparatus and interpreted
as the twist-off strength.
Specify the result of the failure pattern analysis (see the procedure specified in 6.2.1).
— Precision
Precision data are not available at present.
— Reference
The twist-off test is specified in Reference [50].
4.1.3 Peel-off test 1
— Principle
A fabric specified by material, thread size, and mesh size is bedded into a newly applied coating
material. After curing of the coating a tensile tester grabs the overlapping fabric, and due to
continuous tensile force at 90° the coating is peeled off from the substrate. The peel strength is
determined as the force required for peeling off and referring to the width of the test specimen.
Figure 4 schematically shows the peel-off process and the function of a 90°-peel-off apparatus.
6 © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
Key
1 substrate
2 coating
3 fabric
4 tape (uncoated end of the test panel)
a
The direction of movement of the test panel.
b
The direction of rotation of the pressing roller on the coating.
c
The direction of rotation of the pressing roller on the uncoated test panel.
d
The direction of peel-off (tensile tester).
Figure 4 — Principle of the peel-off test 1
— Application
The peel-off test 1 is preferably carried out on automotive coatings.
— Procedure
— Coat the test panel (dimensions 15 mm × 100 mm) sparing a 10 mm wide strip at the edge of
the narrow side. Subsequently bed the fabric so that it remains for about 50 mm uncoated and
overlaps at the uncoated end of the test panel (see Figure 5).
ISO/TR 19402:2018(E)
Key
1 substrate
2 coating
3 fabric
4 tape (uncoated end of the test panel)
Figure 5 — Test panel with coating and fabric
— After drying/hardening of the coating mount the test panel into a tensile tester equipped with
a 90°-peel-off apparatus (see Figure 4) and clamp the free end of the fabric.
— Start the peel-off process and record the tensile force (peel strength) required for peeling off.
— Evaluation
Determine the mean peel strength over a peel-off distance of at least 50 mm for five test specimens,
disregard the beginning and the end of the test.
The test result is the mean value (with standard deviation) from the five individual determinations,
which is designated as the peel strength (N/15 mm width of test specimen).
Specify the result of the failure pattern analysis (see the procedure specified in 6.2.1).
— Precision
Precision data are not available at present.
— Reference
The peel-off test 1 is specified in Reference [47].
4.1.4 Peel-off test 2
— Principle
The coating is peeled off from the substrate under specified conditions by means of an electrically
driven test apparatus. The force is determined which is required for peeling off and which refers to
the width of peeling off. Figure 6 illustrates the peel-off process in a schematic diagram.
8 © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
Key
1 substrate
2 coating
3 peel-off tool
a
The peel strength.
Figure 6 — Principle of the peel-off test 2
— Application
The peel-off test 2 is generally applicable.
— Procedure
— Specify the peel-off tool (cutting angle/width), setting angle, peel-off speed and peel-off
distance.
— Mount the test panel into the peel-off apparatus and start the peel-off process.
— During testing record the force (peel strength) required for peeling off.
— Evaluation
Determine the mean peel strength over the peel-off distance, disregard the beginning and the end
of the peel-off process.
The test result is the mean peel strength divided by the width of the peel-off tool (N/mm).
— Precision
Precision data are not available at present.
— Reference
The peel-off test 2 is specified in Reference [35].
4.2 Tests with continuous deformation of test specimens
4.2.1 Bend test with a wedge-shaped conical mandrel
— Principle
The test panel is deformed from the direction of the substrate side by pressing in a wedge-shaped
conical mandrel of specified geometry. The smallest radius of the mandrel is determined for which
no defect of delamination in the deformed area is detectable.
ISO/TR 19402:2018(E)
Figure 7 shows the test principle in a schematic diagram. Figure 8 illustrates the dimensions of the
wedge-shaped conical mandrel.
Key
1 wedge-shaped conical mandrel
2 test panel (after deformation)
3 elastic pad
Figure 7 — Principle of the bend test with a wedge-shaped conical mandrel
Key
R radius – the number specifies the bending radius in mm
Figure 8 — Measures of the wedge-shaped conical mandrel
— Application
The bend test with a wedge-shaped conical mandrel is preferably carried out on coil coatings.
— Procedure
— Put the test panel with the coated side onto an elastomer panel.
— From the direction of the substrate side press the mandrel by hand (with lever transmission)
or by means of a pneumatic apparatus into the panel until the deformation results in a V-shape.
10 © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
Doing so, the longitudinal axis of the mandrel shall be parallel to the direction of rolling of the
substrate.
— Evaluation
Examine the coating in the deformed area for delamination using a magnifier and determine the
smallest bending radius for which no defect can be detected.
The test result is this bend radius (mm) divided by the thickness of the substrate (mm).
— Precision
Precision data are not available at present.
— Reference
The bend test with a wedge-shaped conical mandrel is specified in EN 13523-7.
4.2.2 Bend test with a conical mandrel
— Principle
The test panel is bent around a conical mandrel of specified dimensions and is deformed accordingly.
The length (mm) of the produced defect is determined.
Figure 9 shows the principle of the bend test with a conical mandrel. Figure 10 shows the bent
test panel.
Key
1 conical mandrel
2 test panel
3 clamping element
l length of the mandrel (203 mm)
d smallest diameter of the mandrel (3,1 mm)
d largest diameter of the mandrel (38 mm)
Figure 9 — Test arrangement of the bend test with a conical mandrel
ISO/TR 19402:2018(E)
Key
1 test panel
2 end of the crack in the coating
a
The small radius of the bent test panel.
b
The large radius of the bent test panel.
Figure 10 — Bent test panel with delamination
— Application
The bend test with a conical mandrel is generally applicable for coatings on deformable substrates.
— Procedure
— Mount the test panel into the test apparatus, coating facing outwards, and bend uniformly
around the mandrel.
— Evaluation
Visually examine the delaminated area of the coating (10× magnifier).
The test result is the length (mm) of the delamination (the mean value rounded to whole numbers
of the three single values).
— Precision
The repeatability limit r is 23 mm.
The reproducibility limit R is 46 mm.
— Reference
The bend test with a conical mandrel is specified in ISO 6860.
4.2.3 Bend test with a cylindrical mandrel 1
— Principle
The test panel is bent around a cylindrical mandrel and is deformed accordingly. The exchangeable
mandrels in the bending apparatus have diameters of 2 mm, 3 mm, 4 mm, 5 mm, 6 mm, 8 mm,
10 mm, 12 mm, 16 mm, 20 mm, 25 mm, and 32 mm. The largest diameter of the mandrel (mm)
is determined for which a defect of the coating is visible after bending around that mandrel. The
method can also be carried out as a “pass/fail” test.
12 © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
Figure 11 shows the principle of bending around a cylindrical mandrel. Figure 12 shows the bent
test panel.
Key
1 cylindrical mandrel
2 test panel
3 clamping element
Figure 11 — Test arrangement of the bend test with a cylindrical mandrel 1
Key
1 test panel
2 crack in the coating
a
The radius of the bent test panel.
Figure 12 — Bent test panel with delamination
— Application
The bend test with a cylindrical mandrel 1 is generally applicable for coatings on deformable
substrates.
— Procedure
— Insert a mandrel of medium diameter into the bending apparatus.
— Mount the test panel into the test apparatus, coating facing outwards, and bend uniformly
around the mandrel.
— Visually examine the coating on the deformed test panel for defects and specify the diameter of
the mandrel for the next bend test:
a) when the coating has been damaged select the next larger mandrel;
b) when the coating has not been damaged select the next smaller mandrel.
ISO/TR 19402:2018(E)
— Continue bend tests until the final result has been determined.
— When carrying out the test as a “pass/fail” test bend the test specimen around the mandrel of
the agreed diameter and visually examine the coating for defects.
— Evaluation
The test result is the largest diameter of the mandrel (mm) for which a defect of the coating is
visible after bending around that mandrel or the information that for all mandrels no defect can be
detected after bending.
When carried out as a “pass/fail” test specify if the coating has been damaged (“fail”) or not (“pass”)
for the agreed diameter of the mandrel.
— Precision
The method should only be considered as an approximation test and not as one giving precise
results. The reproducibility limit R, determined in a round-robin test with six participants and
two coating systems, has been set at 50 %, and is only specified here in order to convey a rough
impression of the precision.
— Reference
The bend test with a cylindrical mandrel 1 is specified in ISO 1519.
4.2.4 Bend test with a cylindrical mandrel 2
— Principle
The test panel is bent around a cylindrical mandrel and deformed accordingly. The exchangeable
mandrels in the bending apparatus have diameters in the range of 0,5 mm to 5,0 mm, in steps
of 0,5 mm. The smallest diameter of the mandrel (mm) is determined for which no defect of the
coating is visible after bending around that mandrel.
Figure 13 shows a typical mandrel bending apparatus for exchangeable cylindrical mandrels.
Figure 13 — Mandrel bending apparatus for exchangeable cylindrical mandrels
— Application
The bend test with a cylindrical mandrel 2 is preferably carried out on coil coatings.
14 © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
— Procedure
— Insert a mandrel of medium diameter into the bending apparatus.
— Mount the test panel into the test apparatus so that the uncoated side faces the mandrel.
— Bend the test panel uniformly around the mandrel.
— Examine the coating on the deformed test panel for defects and specify the diameter of the
mandrel for the next bend test:
a) when the coating has been damaged select the next larger mandrel;
b) when the coating has not been damaged select the next smaller mandrel.
— Continue bend tests until the final result has been determined.
— Evaluation
Visually examine the delaminated area of the coating using a magnifier and determine the smallest
bending radius for which delamination is not yet detectable.
The test result is the bending radius (mm) divided by the thickness of the substrate (mm).
— Precision
Precision data are not available at present.
— Reference
The bend test with a cylindrical mandrel 2 is specified in EN 13523-7.
4.2.5 Three point bending method
— Principle
The coating is applied as specified to a substrate of specified dimensions. The test specimen is
continuously bent by means of a bending apparatus at a speed of 0,5 mm/s. From the recorded
force-distance graph information in regard to the adhesion of the coating is taken.
Figure 14 illustrates the test principle.
ISO/TR 19402:2018(E)
a)  Test specimen prior to stress application b)  Test specimen after stress application
Key
1 struts (diameter 6 mm, length >15 mm, centre distance 33 mm)
2 coating (25 mm × 5 mm)
3 substrate (30 mm × 10 mm)
4 compression bar (diameter 12 mm, length >15 mm)
a
The direction of stress application.
Figure 14 — Principle of the three point bending test
— Application
The three point bending method is applicable for coatings on flexible substrates.
— Procedure
— Coat the substrate panels by means of a template.
— Dry/harden the coating and determine the dry film thickness.
— Mount the specimen in accordance with Figure 14 into the test apparatus and start the bending
process.
— During the bending process record the force-distance graph (see Figure 15).
16 © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
Key
X bending distance
Y bending force
1 maximum bending distance
2 maximum bending force
3 linear range
4 failure extent
Figure 15 — Force-distance graph
— Evaluation
Read from the force-distance graph (see Figure 15):
— the gradient of the curve (N/mm) in the linear range,
— the maximum bending force (N) and the maximum bending distance (mm), and
— a qualitative description of the failure extent.
— Precision
Precision data are not available at present.
— Reference
The three point bending method is specified in NF T 30-010.
A similar method is specified in EN 1966.
4.2.6 T-bend test 1
— Principle
The test panel is successively bent around itself. Doing so the coating shall be facing outwards. The
smallest radius is determined around which the test panel can be bent without any loss of adhesion.
Figure 16 shows a common bending apparatus and explains the bending process. Figure 17
illustrates the individual stages of the bending process.
ISO/TR 19402:2018(E)
Figure 16 — Common bending apparatus
1 1
0 T T 1 T 1 T 2 T
2 2
Figure 17 — Stages of the bending process from 0 T to 2 T
— Application
The T-bend test 1 is preferably carried out on coil coatings.
— Procedure
— Mount the test panel into the bending test apparatus with the coated side facing down and
swivel the bending plate as far as it goes.
— Take out the bent test panel and then complete the 180° bending by means of the bending
apparatus, resulting in the bent condition illustrated in Figure 16.
— Continue bending the bent test panel in the same way.
— After each bending examine the bent area for delamination using a magnifier.
— The test is completed when no delamination is detectable for the first time.
— Evaluation
The smallest radius is determined around which the test panel can be bent without delamination,
expressed in “T units” (see Figure 17).
— Precision
Precision data are not available at present.
18 © ISO 2018 – All rights reserved

ISO/TR 19402:2018(E)
— Reference
The T-bend test 1 is specified in EN 13523-7.
4.2.7 T-bend test 2
— Principle
The test panel is bent around a distance piece with the coating facing outwards. The distance piece
can be a solid bending piece or consist of a pile of substrate panels. Alternatively, the test panel
can also be bent around itself. The smallest bending distance is determined for which no loss of
adhesion is detectable. The method can also be carried out as a “pass/fail” test.
Figure 18 shows the process of the T-bend test around a solid bending piece using a bench vice.
Figure 19 illustrates representative examples for both of the other types of the process.
Figure 18 — Bending around a bending piece
a)  Bending with panels as distance pieces (ex- b)  Bending method with a bench vice (exam-
ample 2T) ple 2T)
Figure 19 — Further types of the process
— Application
The T-bend test 2 is generally applicable for coatings on deformable metal substrates.
— Procedure
— Specify the type of the process:
a) bending around solid bending pieces,
b) bending around bending pieces consisting of substrate panels,
c) bending procedure.
— Carry out the bend test in accordance with Figure 18 or Figure 19 and examine the bent area for
delamination using a magnifier.
ISO/TR 19402:2018(E)
— Carry out further bend tests with increasing bending distance until no loss of adhesion is
detected.
— When car
...