IEC 60475:2011

Method of sampling insulating liquids

IEC 60475:2011 is applicable to the procedure to be used for insulating liquids in delivery containers and in electrical equipment such as power and instrument transformers, reactors, bushings, oil-filled cables, oil-filled tank-type capacitors, switchgear and load tap changers. The main changes with respect to the previous edition are as follows:
- withdrawal of askarels;
- addition of recommendations concerning general health, safety and environmental protection;
- additional details regarding the sampling of oil from electrical equipment, using various types of sampling devices appropriate for the different types of oil tests to be performed in the laboratory.

Méthode d'échantillonnage des liquides isolants

La CEI 60475:2011 décrit le mode opératoire d'échantillonnage à utiliser dans des liquides isolants dans les récipients de livraison et les appareils électriques tels que les transformateurs de puissance et de mesure, les réacteurs, les traversées de transformateurs, les câbles à huile fluide, les condensateurs de puissance, l'appareillage de connexion et les changeurs de prise en charge. Les modifications principales par rapport à l'édition précédente sont les suivantes:
- retrait des askarels;
- ajout de recommandations en matière de protection générale de la santé, de la sécurité et de l'environnement on été ajoutées en tant qu'Introduction; détails supplémentaires concernant l'échantillonnage de l'huile dans les appareils électriques, à l'aide de différents types de matériels d'échantillonnage correspondant aux différents types d'essais à l'huile à réaliser en laboratoire.

General Information

• Status: Published
• Publication Date: 19-Oct-2011
• ICS: 01 - GENERALITIES. TERMINOLOGY. STANDARDIZATION. DOCUMENTATION
• ICS: 29.040.10 - Insulating oils
• Technical Committee: TC 10 - Fluids for electrotechnical applications
• Current Stage: DELPUB - Deleted Publication
• Start Date: 30-Jul-2021
• Completion Date: 25-May-2022

Relations

• Revised: IEC 60475:2022 - Method of sampling insulating liquids
• Effective Date: 05-Sep-2023

Standards Content (Sample)

IEC 60475 ®
Edition 2.0 2011-10
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
Method of sampling insulating liquids

Méthode d'échantillonnage des liquides isolants

All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by
any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from either IEC or
IEC's member National Committee in the country of the requester.
If you have any questions about IEC copyright or have an enquiry about obtaining additional rights to this publication,
please contact the address below or your local IEC member National Committee for further information.

Droits de reproduction réservés. Sauf indication contraire, aucune partie de cette publication ne peut être reproduite
ni utilisée sous quelque forme que ce soit et par aucun procédé, électronique ou mécanique, y compris la photocopie
et les microfilms, sans l'accord écrit de la CEI ou du Comité national de la CEI du pays du demandeur.
Si vous avez des questions sur le copyright de la CEI ou si vous désirez obtenir des droits supplémentaires sur cette
publication, utilisez les coordonnées ci-après ou contactez le Comité national de la CEI de votre pays de résidence.

IEC Central Office
3, rue de Varembé
CH-1211 Geneva 20
Switzerland
Email: [e-mail]
Web: www.iec.ch
About the IEC
The International Electrotechnical Commission (IEC) is the leading global organization that prepares and publishes
International Standards for all electrical, electronic and related technologies.

About IEC publications
The technical content of IEC publications is kept under constant review by the IEC. Please make sure that you have the
latest edition, a corrigenda or an amendment might have been published.
 Catalogue of IEC publications: www.iec.ch/searchpub
The IEC on-line Catalogue enables you to search by a variety of criteria (reference number, text, technical committee,…).
It also gives information on projects, withdrawn and replaced publications.
 IEC Just Published: www.iec.ch/online_news/justpub
Stay up to date on all new IEC publications. Just Published details twice a month all new publications released. Available
on-line and also by email.
 Electropedia: www.electropedia.org
The world's leading online dictionary of electronic and electrical terms containing more than 20 000 terms and definitions
in English and French, with equivalent terms in additional languages. Also known as the International Electrotechnical
Vocabulary online.
 Customer Service Centre: www.iec.ch/webstore/custserv
If you wish to give us your feedback on this publication or need further assistance, please visit the Customer Service
Centre FAQ or contact us:
Email: [e-mail]
Tel.: [phone]
Fax: [phone]
A propos de la CEI
La Commission Electrotechnique Internationale (CEI) est la première organisation mondiale qui élabore et publie des
normes internationales pour tout ce qui a trait à l'électricité, à l'électronique et aux technologies apparentées.

A propos des publications CEI
Le contenu technique des publications de la CEI est constamment revu. Veuillez vous assurer que vous possédez
l’édition la plus récente, un corrigendum ou amendement peut avoir été publié.
 Catalogue des publications de la CEI: www.iec.ch/searchpub/cur_fut-f.htm
Le Catalogue en-ligne de la CEI vous permet d’effectuer des recherches en utilisant différents critères (numéro de référence,
texte, comité d’études,…). Il donne aussi des informations sur les projets et les publications retirées ou remplacées.
 Just Published CEI: www.iec.ch/online_news/justpub
Restez informé sur les nouvelles publications de la CEI. Just Published détaille deux fois par mois les nouvelles
publications parues. Disponible en-ligne et aussi par email.
 Electropedia: www.electropedia.org
Le premier dictionnaire en ligne au monde de termes électroniques et électriques. Il contient plus de 20 000 termes et
définitions en anglais et en français, ainsi que les termes équivalents dans les langues additionnelles. Egalement appelé
Vocabulaire Electrotechnique International en ligne.
 Service Clients: www.iec.ch/webstore/custserv/custserv_entry-f.htm
Si vous désirez nous donner des commentaires sur cette publication ou si vous avez des questions, visitez le FAQ du
Service clients ou contactez-nous:
Email: [e-mail]
Tél.: [phone]
Fax: [phone]
IEC 60475 ®
Edition 2.0 2011-10
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
Method of sampling insulating liquids

Méthode d'échantillonnage des liquides isolants

INTERNATIONAL
ELECTROTECHNICAL
COMMISSION
COMMISSION
ELECTROTECHNIQUE
PRICE CODE
INTERNATIONALE
CODE PRIX U
ICS 29.040 ISBN 978-2-88912-767-2

– 2 – 60475 © IEC:2011
CONTENTS
FOREWORD . 3
INTRODUCTION . 5
1 Scope . 6
2 Normative references . 6
3 Terms and definitions . 6
4 General principles for the sampling of insulating liquids . 7
4.1 New insulating liquids in delivery containers . 7
4.1.1 Place of sampling . 7
4.1.2 Quantity of sample to be taken . 7
4.1.3 Sampling equipment . 7
4.1.4 Sampling procedure. 11
4.2 Sampling of oil from oil-filled equipment . 13
4.2.1 General remarks . 13
4.2.2 Sampling of oil by syringe . 19
4.2.3 Sampling of oil by ampoule . 20
4.2.4 Sampling of oil by flexible metal bottles . 21
4.2.5 Sampling of oil by glass and rigid metal bottles . 22
4.2.6 Sampling of oil by plastic bottles . 23
4.3 Storage and transportation of samples . 23
4.4 Labelling of samples . 23
Annex A (informative) Procedure for sampling at intermediate levels (making up of the
average sample) . 25
Annex B (informative) Procedure for testing the integrity of the syringes . 26

Figure 1 – Thief dipper . 8
Figure 2 – Cream dipper . 9
Figure 3 – Pipette . 10
Figure 4 – Siphon . 10
Figure 5 – Sampling of oil by syringe . 15
Figure 6 – Sampling of oil by ampoule . 16
Figure 7 – Sampling of oil by bottle . 17

Table 1 – Types of samples of new insulating liquids . 11
Table 2 – Sample containers for oil tests (Y = Yes) . 18
Table 3 – Information required on oil sample labels . 24

60475 © IEC:2011 – 3 –
INTERNATIONAL ELECTROTECHNICAL COMMISSION
____________
METHOD OF SAMPLING INSULATING LIQUIDS

FOREWORD
1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising
all national electrotechnical committees (IEC National Committees). The object of IEC is to promote
international co-operation on all questions concerning standardization in the electrical and electronic fields. To
this end and in addition to other activities, IEC publishes International Standards, Technical Specifications,
Technical Reports, Publicly Available Specifications (PAS) and Guides (hereafter referred to as “IEC
Publication(s)”). Their preparation is entrusted to technical committees; any IEC National Committee interested
in the subject dealt with may participate in this preparatory work. International, governmental and non-
governmental organizations liaising with the IEC also participate in this preparation. IEC collaborates closely
with the International Organization for Standardization (ISO) in accordance with conditions determined by
agreement between the two organizations.
2) The formal decisions or agreements of IEC on technical matters express, as nearly as possible, an international
consensus of opinion on the relevant subjects since each technical committee has representation from all
interested IEC National Committees.
3) IEC Publications have the form of recommendations for international use and are accepted by IEC National
Committees in that sense. While all reasonable efforts are made to ensure that the technical content of IEC
Publications is accurate, IEC cannot be held responsible for the way in which they are used or for any
misinterpretation by any end user.
4) In order to promote international uniformity, IEC National Committees undertake to apply IEC Publications
transparently to the maximum extent possible in their national and regional publications. Any divergence
between any IEC Publication and the corresponding national or regional publication shall be clearly indicated in
the latter.
5) IEC itself does not provide any attestation of conformity. Independent certification bodies provide conformity
assessment services and, in some areas, access to IEC marks of conformity. IEC is not responsible for any
services carried out by independent certification bodies.
6) All users should ensure that they have the latest edition of this publication.
7) No liability shall attach to IEC or its directors, employees, servants or agents including individual experts and
members of its technical committees and IEC National Committees for any personal injury, property damage or
other damage of any nature whatsoever, whether direct or indirect, or for costs (including legal fees) and
expenses arising out of the publication, use of, or reliance upon, this IEC Publication or any other IEC
Publications.
8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publications is
indispensable for the correct application of this publication.
9) Attention is drawn to the possibility that some of the elements of this IEC Publication may be the subject of
patent rights. IEC shall not be held responsible for identifying any or all such patent rights.
International Standard IEC 60475 has been prepared by IEC technical committee 10: Fluids
for electrotechnical applications.
This second edition cancels and replaces the first edition, published in 1974, and constitutes
a technical revision.
The main changes with respect to the previous edition are listed below:
– since the publication of the first edition of this standard, askarels have been banned and
therefore have been withdrawn from this second edition;
– recommendations concerning general health, safety and environmental protection have
been added as an Introduction;
– the first edition was mainly about sampling from drums and tank cars. This second edition
addresses in more detail the sampling of oil from electrical equipment, using various types
of sampling devices appropriate for the different types of oil tests to be performed in the
laboratory, including dissolved gas analysis (DGA).

– 4 – 60475 © IEC:2011
The text of this standard is based on the following documents:
FDIS Report on voting
10/848/FDIS 10/871/RVD
Full information on the voting for the approval of this standard can be found in the report on
voting indicated in the above table.
This publication has been drafted in accordance with the ISO/IEC Directives, Part 2.
The committee has decided that the contents of this publication will remain unchanged until
the stability date indicated on the IEC web site under "http://webstore.iec.ch" in the data
related to the specific publication. At this date, the publication will be
• reconfirmed,
• withdrawn,
• replaced by a revised edition, or
• amended.
60475 © IEC:2011 – 5 –
INTRODUCTION
General caution, health, safety and environmental protection
This International Standard does not purport to address all the safety problems associated
with its use. It is the responsibility of the user of the standard to establish appropriate health
and safety practices and determine the applicability of regulatory limitations prior to use.
The insulating oils which are the subject of this standard should be handled with due regard to
personal hygiene. Direct contact with the eyes may cause irritation. In the case
...