Petroleum and natural gas industries — Corrosion-resistant alloy seamless tubes for use as casing, tubing and coupling stock — Technical delivery conditions

ISO 13680:2008 specifies the technical delivery conditions for corrosion-resistant alloy seamless tubulars for casing, tubing and coupling stock for two product specification levels: PSL-1, which is the basis of ISO 13680:2008; PSL-2, which provides additional requirements for a product that is intended to be both corrosion resistant and cracking resistant for the environments and qualification method specified in ISO 15156-3 and Annex G of ISO 13680:2008. At the option of the manufacturer, PSL-2 products can be provided in lieu of PSL-1. ISO 13680:2008 is applicable to the following four groups of product: group 1, which is comprised of stainless alloys with a martensitic or martensitic/ferritic structure; group 2, which is comprised of stainless alloys with a ferritic-austenitic structure, such as duplex and super-duplex stainless alloy; group 3, which is comprised of stainless alloys with an austenitic structure (iron base); group 4, which is comprised of nickel-based alloys with an austenitic structure (nickel base). ISO 13680:2008 contains no provisions relating to the connection of individual lengths of pipe.

Industries du pétrole et du gaz naturel — Tubes sans soudure en acier allié résistant à la corrosion utilisés comme tubes de cuvelage, tubes de production et tubes-ébauches pour manchons — Conditions techniques de livraison

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Status
Withdrawn
Publication Date
14-Oct-2008
Withdrawal Date
14-Oct-2008
Current Stage
9599 - Withdrawal of International Standard
Completion Date
06-Sep-2010
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INTERNATIONAL ISO
STANDARD 13680
Second edition
2008-10-15


Petroleum and natural gas industries —
Corrosion-resistant alloy seamless tubes
for use as casing, tubing and coupling
stock — Technical delivery conditions
Industries du pétrole et du gaz naturel — Tubes sans soudure en acier
allié résistant à la corrosion utilisés comme tubes de cuvelage, tubes de
production et tubes-ébauches pour manchons — Conditions techniques
de livraison





Reference number
ISO 13680:2008(E)
©
ISO 2008

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ISO 13680:2008(E)
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©  ISO 2008
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means,
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ii © ISO 2008 – All rights reserved

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ISO 13680:2008(E)
Contents Page
Foreword. v
Introduction . vi
1 Scope . 1
2 Conformance. 2
2.1 Dual normative references. 2
2.2 Units of measurement . 2
3 Normative references . 2
4 Terms, abbreviated terms, symbols and definitions. 4
4.1 Terms and definitions. 4
4.2 Symbols . 6
4.3 Abbreviated terms . 7
5 Information to be supplied by the purchaser . 8
6 Manufacturing process . 9
6.1 Manufacturing of corrosion-resistant alloys .9
6.2 Product manufacturing process . 9
6.3 Pipe end sizing. 9
6.4 Straightening. 9
7 Material requirements. 10
7.1 Chemical composition. 10
7.2 Tensile properties. 10
7.3 Hardness properties. 10
7.4 Charpy V-notch test properties — General requirements. 10
7.5 Charpy V-notch — Absorbed energy requirements for coupling stock – All grades. 11
7.6 Charpy V-notch — Absorbed energy requirements for pipe — All grades . 12
7.7 Flattening requirements. 13
7.8 Corrosion properties . 13
7.9 Microstructure properties . 13
7.10 Surface condition. 14
7.11 Defects . 14
7.12 Hydrostatic test. 14
8 Dimensions, masses and tolerances. 15
8.1 Outside diameter, wall thickness and mass . 15
8.2 Length . 15
8.3 Tolerances . 15
8.4 Product ends . 16
9 Inspection and testing. 16
9.1 Test equipment . 16
9.2 Type and frequency of tests . 16
9.3 Testing of chemical composition. 16
9.4 Testing of mechanical characteristics. 17
9.5 Tensile test . 17
9.6 Hardness test . 18
9.7 Impact or flattening test . 19
9.8 Microstructural examination. 21
9.9 Dimensional testing. 21
9.10 Drift test . 22
9.11 Length . 22
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ISO 13680:2008(E)
9.12 Straightness. 22
9.13 Mass determination . 23
9.14 Hydrostatic test . 23
9.15 Visual inspection. 23
9.16 Non-destructive examination. 24
10 Surface treatment. 29
10.1 Group 1. 29
10.2 Groups 2, 3 and 4 . 29
11 Marking. 29
11.1 General . 29
11.2 Marking on the product . 29
11.3 Date of manufacture . 31
12 Surface protection — Group 1. 31
13 Documents. 31
13.1 Electronic media . 31
13.2 Retention of records . 31
14 Handling, packaging and storage . 31
14.1 General . 31
14.2 Handling. 32
14.3 Packaging . 32
14.4 Storage . 32
Annex A (normative) Tables in SI units. 33
Annex B (normative) Figures in SI (USC) Units. 53
Annex C (normative) Tables in USC units . 58
Annex D (normative) Purchaser inspection. 78
Annex E (normative) Cleanliness requirements. 79
Annex F (informative) Marking instructions for API licensees — API monogram. 81
Annex G (normative) Product specification level 2 (PSL-2). 82
Bibliography . 84

iv © ISO 2008 – All rights reserved

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ISO 13680:2008(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the
International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 13680 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures
for petroleum, petrochemical and natural gas industries, Subcommittee SC 5, Casing, tubing and drill pipe.
This second edition cancels and replaces the first edition (ISO 13680:2000), which has been technically
revised, after the six-month overlap period. (It also incorporates the Technical corrigenda
ISO 13680:2000/Cor.1:2002 and ISO 13680:2000/Cor.2:2004.)
It is the intent of ISO/TC 67 that the first and second editions of ISO 13680 both be applicable, at the option of
the purchaser, for a period of six months from the first day of the calendar quarter immediately following the
date of publication of this second edition, after which period the first edition will no longer be applicable.

© ISO 2008 – All rights reserved v

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ISO 13680:2008(E)
Introduction
Users of this International Standard should be aware that further or differing requirements may be needed for
individual applications. This International Standard is not intended to inhibit a vendor from offering, or the
purchaser from accepting, alternative equipment or engineering solutions for the individual application. This
may be particularly applicable where there is innovative or developing technology. Where an alternative is
offered, the vendor should identify any variations from this International Standard and provide details.
This International Standard includes requirements of various nature. These are identified by the use of certain
verbal forms:
SHALL is used to indicate that a provision is MANDATORY;
SHOULD is used to indicate that a provision is not mandatory, but RECOMMENDED as good practice;
MAY is used to indicate that a provision is OPTIONAL.

vi © ISO 2008 – All rights reserved

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INTERNATIONAL STANDARD ISO 13680:2008(E)

Petroleum and natural gas industries — Corrosion-resistant
alloy seamless tubes for use as casing, tubing and coupling
stock — Technical delivery conditions
WARNING — It is the purchaser’s responsibility to specify the product specification level (PSL),
corrosion-resistant alloy (CRA) group, category, grade, delivery conditions and any other
requirements in addition to those specified herewith to ensure that the product is adequate for the
intended service environment. ISO 15156 (all parts) or NACE MR0175/ISO 15156 should be considered
when making specific requirements for H S containing environment (see Annex G).
2
1 Scope
This International Standard specifies the technical delivery conditions for corrosion-resistant alloy seamless
tubulars for casing, tubing and coupling stock for two product specification levels:
⎯ PSL-1, which is the basis of this International Standard;
⎯ PSL-2, which provides additional requirements for a product that is intended to be both corrosion resistant
and cracking resistant for the environments and qualification method specified in ISO 15156-3 and
Annex G of this International Standard.
At the option of the manufacturer, PSL-2 products can be provided in lieu of PSL-1.
NOTE 1 The corrosion-resistant alloys included in this International Standard are special alloys in accordance with
ISO 4948-1 and ISO 4948-2.
This International Standard is applicable to the following four groups of product:
a) group 1, which is comprised of stainless alloys with a martensitic or martensitic/ferritic structure;
b) group 2, which is comprised of stainless alloys with a ferritic-austenitic structure, such as duplex and
super-duplex stainless alloy;
c) group 3, which is comprised of stainless alloys with an austenitic structure (iron base);
d) group 4, which is comprised of nickel-based alloys with an austenitic structure (nickel base).
This International Standard contains no provisions relating to the connection of individual lengths of pipe.
NOTE 2 The connection or joining method can influence the corrosion performance of the materials specified in this
International Standard.
NOTE 3 It is necessary to recognize that not all PSL-1 categories and grades can be made cracking resistant per
ISO 15156-3 and are, therefore, not included in PSL-2.
© ISO 2008 – All rights reserved 1

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ISO 13680:2008(E)
2 Conformance
2.1 Dual normative references
In the interests of world-wide application of this International Standard, ISO/TC 67 has decided, after detailed
technical analysis, that certain of the normative documents listed in Clause 3 and prepared by ISO/TC 67 or
another ISO Technical Committee are interchangeable in the context of the relevant requirement with the
relevant document prepared by the American Petroleum Institute (API), the American Society for Testing and
Materials (ASTM) or the American National Standards Institute (ANSI). These latter documents are cited in
the running text following the ISO reference and preceded by “or”, for example “ISO XXXX or API YYYY”.
Application of an alternative normative document cited in this manner can lead to technical results different
from the use of the preceding ISO reference. However, both results are acceptable and these documents are
thus considered interchangeable in practice.
2.2 Units of measurement
In this International Standard, data are expressed in both the International System (SI) of units and the United
States Customary (USC) system of units. For a specific order item, it is intended that only one system of units
be used, without combining data expressed in the other system.
Products manufactured to specifications expressed in either of these unit systems shall be considered
equivalent and totally interchangeable. Consequently, compliance with the requirements of this International
Standard as expressed in one system provides compliance with requirements expressed in the other system.
For data expressed in SI units, a comma is used as the decimal separator and a space as the thousands
separator.
For data expressed in USC units, a dot (on the line) is used as the decimal separator and a space as the
thousands separator.
In the text, data in SI units are followed by data in USC units in parentheses.
Separate tables for data expressed in SI units and USC units are given in Annex A and Annex C, respectively.
Figures are contained in Annex B and express data in both SI and USC units.
3 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
ISO 31-0, Quantities and units — Part 0: General principles
ISO 377, Steel and steel products — Location and preparation of samples and test pieces for mechanical
testing
ISO 404, Steel and steel products — General
ISO 525, Bonded abrasive products — General requirements
ISO 783, Metallic materials — Tensile testing at elevated temperature
ISO 4885, Ferrous products — Heat treatments — Vocabulary
ISO 4948-1, Steels — Classification — Part 1: Classification of steels into unalloyed and alloy steels based on
chemical composition
ISO 4948-2, Steels — Classification — Part 2: Classification of unalloyed and alloy steels according to main
quality classes and main property or application characteristics
2 © ISO 2008 – All rights reserved

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ISO 13680:2008(E)
ISO 6508-1, Metallic materials — Rockwell hardness test — Part 1: Test method (scales A, B, C, D, E, F, G, H,
K, N, T)
ISO 6892, Metallic materials — Tensile testing at ambient temperature
ISO 6929, Steel products — Definitions and classification
ISO 8501-1:2007, Preparation of steel substrates before application of paints and related products — Visual
assessment of surface cleanliness — Part 1: Rust grades and preparation grades of uncoated steel
substrates and of steel substrates after overall removal of previous coatings
ISO 9303, Seamless and welded (except submerged arc-welded) steel tubes for pressure purposes — Full
peripheral ultrasonic testing for the detection of longitudinal imperfections
ISO 9304, Seamless and welded (except submerged arc-welded) steel tubes for pressure purposes — Eddy
current testing for the detection of imperfections
ISO 9305, Seamless steel tubes for pressure purposes — Full peripheral ultrasonic testing for the detection of
transverse imperfections
ISO 9402, Seamless and welded (except submerged arc-welded) steel tubes for pressure purposes — Full
peripheral magnetic transducer/flux leakage testing of ferromagnetic steel tubes for the detection of
longitudinal imperfections
ISO 9598, Seamless steel tubes for pressure purposes — Full peripheral magnetic transducer/flux leakage
testing of ferromagnetic steel tubes for the detection of transverse imperfections
ISO 10124, Seamless and welded (except submerged arc-welded) steel tubes for pressure purposes —
Ultrasonic testing for the detection of laminar imperfections
ISO 10474, Steel and steel products — Inspection documents
ISO 10543, Seamless and hot-stretch-reduced welded steel tubes for pressure purposes — Full peripheral
ultrasonic thickness testing
1)
ISO 11484 , Steel products — Employer's qualification system of non-destructive testing (NDT) personnel
ISO 11496, Seamless and welded steel tubes for pressure purposes — Ultrasonic testing of tube ends for the
detection of laminar imperfections
ISO 12095, Seamless end welded steel tubes for pressure purposes — Liquid penetrant testing
ISO 13665, Seamless and welded steel tubes for pressure purposes — Magnetic particle inspection of the
tube body for the detection of surface imperfections
ISO 14284, Steel and iron — Sampling and preparation of samples for the determination of chemical
composition
ISO 15156-3:2003, Petroleum and natural gas industries — Materials for use in H S-containing environments
2
in oil and gas production — Part 3: Cracking-resistant CRAs (corrosion resistant alloys) and other alloys
ISO 15156-3:2003/Cor 1:2005, Petroleum and natural gas industries — Materials for use in H S-containing
2
environments in oil and gas production — Part 3: Cracking-resistant CRAs (corrosion resistant alloys) and
other alloys — Technical Corrigendum 1
ISO 15156-3:2003/Cor 2:2005, Petroleum and natural gas industries — Materials for use in H S-containing
2
environments in oil and gas production — Part 3: Cracking-resistant CRAs (corrosion resistant alloys) and
other alloys — Technical Corrigendum 2

1) To be published. (Revision of ISO 11484:1994)
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ISO 13680:2008(E)
ASNT SNT-TC-1A, Recommended practice — Non-destructive Testing
ASTM A370, Standard Test Methods and Definitions for Mechanical Testing of Steel Products
ASTM A604/A604M, Standard Practice for Macroetch Testing of Consumable Electrode Remelted Steel Bars
and Billets
ASTM A941, Terminology Relating to Steel, Stainless Steel, Related Alloys and Ferroalloys
ASTM E18, Standard Test Methods for Rockwell Hardness of Metallic Materials
ASTM E21, Standard Test Methods for Elevated Temperature Tension Tests of Metallic Materials
ASTM E23, Standard Test Methods for Notched Bar Impact Testing of Metallic Materials
ASTM E29, Standard Practice for Using Significant Digits in Test Data to Determine Conformance with
Specifications
ASTM E45, Standard Test Methods for Determining the Inclusion Content of Steel
ASTM E165, Standard Test Method for Liquid Penetrant Examination
ASTM E213, Standard Practice for Ultrasonic Examination of Metal Pipe and Tubing
ASTM E309, Standard Practice for Eddy-Current Examination of Steel Tubular Products Using Magnetic
Saturation
ASTM E340, Standard Test Method for Macroetching Metals and Alloys
ASTM E381, Standard Method of Macroetch Testing Steel Bars, Billets, Blooms, and Forgings
ASTM E407, Standard Practice for Microetching Metals and Alloys
ASTM E562, Standard Test Method for Determining Volume Fraction by Systematic Manual Point Count
ASTM E570, Standard Practice for Flux Leakage Examination of Ferromagnetic Steel Tubular Products
ASTM E709, Standard Guide for Magnetic Particle Testing
NACE MR0175/ISO 15156-3, Petroleum and natural gas industries — Materials for use in H S-containing
2
environments in oil and gas production — Part 3: Cracking-resistant CRAs (corrosion resistant alloys) and
other alloys
4 Terms, abbreviated terms, symbols and definitions
4.1 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO 377, ISO 404, ISO 4885,
ISO 4948-1, ISO 4948-2, ISO 6929, ISO 10474, ASTM A941 and the following apply.
4.1.1
casing
pipe intended to line the walls of a drilled well
4.1.2
cast
heat
material of the same category melted in the same manufacturing process at the same time sequence poured
into multiple ingots or continuous strand cast
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ISO 13680:2008(E)
4.1.3
cold hardened
material condition where the mechanical properties are obtained by a cold finishing process not followed by
heat treatment
NOTE 1 Cold finishing is a plastic deformation of material at a temperature below the recrystallization temperature
such that permanent strain hardening occurs.
NOTE 2 The percentage of cold hardening depends on the specified strength level for each material grade, as shown
in Table A.3 or Table C.3 for the cold hardened condition.
4.1.4
corrosion-resistant alloy
CRA
alloy intended to be resistant to general and localized corrosion and/or environmental cracking in
environments that are corrosive to carbon and low-alloy steels
4.1.5
coupling stock
seamless thick-wall tubular product used for the manufacture of coupling blanks
4.1.6
defect
imperfection having sufficient magnitude to warrant rejection of the product based on the criteria defined in
this International Standard
4.1.7
hot finished
material condition obtained by deforming metal plastically at such a temperature and strain rate that
recrystallization takes place simultaneously with the deformation, thus preventing permanent strain hardening
4.1.8
imperfection
discontinuity on the product surface or in the product wall that can be detected by visual inspection or an NDE
method outlined in this International Standard
4.1.9
label 1
dimensionless designation for the size or specified outside diameter that may be used when ordering pipe
4.1.10
label 2
dimensionless designation for the linear density that may
...

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