Vitreous and porcelain enamels - Preparation of samples and determination of thermal expansion coefficient (ISO 20274:2017)

This standard specifies the procedures for the preparation of enamel samples for measurement of the thermal dilatation and calculation of the thermal expansion coefficient.

Emails und Emaillierungen - Herstellung von Proben und Bestimmung des thermischen Ausdehnungskoeffizienten (ISO 20274:2017)

Emaux vitrifiés - Préparation d'échantillons émaillés et détermination du coefficient de la dilatation thermique (ISO 20274:2017)

ISO 20274:2017 spécifie des modes opératoires de préparation d'échantillons d'émail en vue de mesurer la variation de longueur en fonction de la température et de calculer le coefficient de dilatation thermique.

Steklasti in keramični emajli - Priprava vzorcev in določanje koeficienta toplotne razteznosti (ISO 20274:2017)

Ta standard določa postopke za pripravo vzorcev emajlov za merjenje toplotne dilatacije in izračun koeficienta toplotne razteznosti.

General Information

Status
Published
Public Enquiry End Date
14-Oct-2016
Publication Date
15-Oct-2017
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
05-Oct-2017
Due Date
10-Dec-2017
Completion Date
16-Oct-2017

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 20274:2017
01-november-2017
6WHNODVWLLQNHUDPLþQLHPDMOL3ULSUDYDY]RUFHYLQGRORþDQMHNRHILFLHQWDWRSORWQH
UD]WH]QRVWL ,62
Vitreous and porcelain enamels - Preparation of samples and determination of thermal
expansion coefficient (ISO 20274:2017)
Emails und Emaillierungen - Herstellung von Proben und Bestimmung des thermischen
Ausdehnungskoeffizienten (ISO 20274:2017)
Emaux vitrifiés - Préparation d'échantillons émaillés et détermination du coefficient de la
dilatation thermique (ISO 20274:2017)
Ta slovenski standard je istoveten z: EN ISO 20274:2017
ICS:
25.220.50 Emajlne prevleke Enamels
SIST EN ISO 20274:2017 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 20274:2017

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SIST EN ISO 20274:2017


EN ISO 20274
EUROPEAN STANDARD

NORME EUROPÉENNE

August 2017
EUROPÄISCHE NORM
ICS 25.220.50
English Version

Vitreous and porcelain enamels - Preparation of samples
and determination of thermal expansion coefficient (ISO
20274:2017)
Emaux vitrifiés - Préparation d'échantillons d'émail et Emails und Emaillierungen - Herstellung von Proben
détermination du coefficient de dilatation thermique und Bestimmung des thermischen
(ISO 20274:2017) Ausdehnungskoeffizienten (ISO 20274:2017)
This European Standard was approved by CEN on 22 June 2017.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 20274:2017 E
worldwide for CEN national Members.

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SIST EN ISO 20274:2017
EN ISO 20274:2017 (E)
Contents Page
European foreword . 3

2

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SIST EN ISO 20274:2017
EN ISO 20274:2017 (E)
European foreword
This document (EN ISO 20274:2017) has been prepared by Technical Committee ISO/TC 107 “Metallic
and other inorganic coatings” in collaboration with Technical Committee CEN/TC 262 “Metallic and
other inorganic coatings, including for corrosion protection and corrosion testing of metals and alloys”
the secretariat of which is held by BSI.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by February 2018, and conflicting national standards
shall be withdrawn at the latest by February 2018.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 20274:2017 has been approved by CEN as EN ISO 20274:2017 without any modification.
3

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SIST EN ISO 20274:2017

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SIST EN ISO 20274:2017
INTERNATIONAL ISO
STANDARD 20274
First edition
2017-07
Vitreous and porcelain enamels —
Preparation of samples and
determination of thermal expansion
coefficient
Emaux vitrifiés — Préparation d’échantillons d’émail et
détermination du coefficient de dilatation thermique
Reference number
ISO 20274:2017(E)
©
ISO 2017

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SIST EN ISO 20274:2017
ISO 20274:2017(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2017, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
ii © ISO 2017 – All rights reserved

---------------------- Page: 8 ----------------------

SIST EN ISO 20274:2017
ISO 20274:2017(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Apparatus . 1
5 Requirements for the test specimen . 1
6 Preparation of the test specimens . 2
6.1 General . 2
6.2 Production by casting. 2
6.3 Production by drawing out of the melt . 2
6.4 Production by sintering . 3
7 Determination of the thermal expansion coefficient . 3
8 Calculation and indication of the results . 4
9 Test report . 4
Annex A (informative) Metallic casting mould . 5
Annex B (informative) Drawing from the melt . 6
© ISO 2017 – All rights reserved iii

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SIST EN ISO 20274:2017
ISO 20274:2017(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/ patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO’s adherence to the
World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following
URL: w w w . i s o .org/ iso/ foreword .html.
This document was prepared by Technical Committee ISO/TC 107, Metallic and other inorganic coatings.
iv © ISO 2017 – All rights reserved

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SIST EN ISO 20274:2017
ISO 20274:2017(E)

Introduction
The thermal expansion coefficient of enamel and the relevant substrate is an important material
characteristic, as it provides information on the stress ratios in the composite material.
© ISO 2017 – All rights reserved v

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SIST EN ISO 20274:2017

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SIST EN ISO 20274:2017
INTERNATIONAL STANDARD ISO 20274:2017(E)
Vitreous and porcelain enamels — Preparation of samples
and determination of thermal expansion coefficient
1 Scope
This document specifies the procedures for the preparation of enamel samples for measurement of the
thermal length change and calculation of the thermal expansion coefficient.
2 Normative references
The following documents are referred to in the text in s
...

SLOVENSKI STANDARD
oSIST prEN ISO 20274:2016
01-oktober-2016
6WHNODVWLLQNHUDPLþQLHPDMOL3ULSUDYDY]RUFHYLQGRORþDQMHNRHILFLHQWDWRSORWQH
UD]WH]QRVWL ,62',6
Vitreous and porcelain enamels - Preparation of samples and determination of thermal
expansion coefficient (ISO/DIS 20274:2016)
Emails und Emaillierungen - Herstellung von Proben und Bestimmung des thermischen
Ausdehnungskoeffizienten (ISO/DIS 20274:2016)
Emaux vitrifiés - Préparation d'échantillons émaillés et détermination du coefficient de la
dilatation thermique (ISO/DIS 20274:2016)
Ta slovenski standard je istoveten z: prEN ISO 20274
ICS:
25.220.50 Emajlne prevleke Enamels
oSIST prEN ISO 20274:2016 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN ISO 20274:2016

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oSIST prEN ISO 20274:2016
DRAFT INTERNATIONAL STANDARD
ISO/DIS 20274
ISO/TC 107 Secretariat: KATS
Voting begins on: Voting terminates on:
2016-07-02 2016-09-24
Vitreous and Porcelain enamels — Preparation of samples
and determination of thermal expansion coefficient
Emaux vitrifiés — Préparation d’échantillons émaillés et détermination du coefficient de la dilatation
thermique
ICS: 25.220.50
ISO/CEN PARALLEL PROCESSING
This draft has been developed within the International Organization for
Standardization (ISO), and processed under the ISO lead mode of collaboration
as defined in the Vienna Agreement.
This draft is hereby submitted to the ISO member bodies and to the CEN member
bodies for a parallel five month enquiry.
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENT AND APPROVAL. IT IS
THEREFORE SUBJECT TO CHANGE AND MAY
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
To expedite distribution, this document is circulated as received from the
IN ADDITION TO THEIR EVALUATION AS
committee secretariat. ISO Central Secretariat work of editing and text
BEING ACCEPTABLE FOR INDUSTRIAL,
composition will be undertaken at publication stage.
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 20274:2016(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
©
PROVIDE SUPPORTING DOCUMENTATION. ISO 2016

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oSIST prEN ISO 20274:2016
ISO/DIS 20274:2016(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2016, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
ii © ISO 2016 – All rights reserved

---------------------- Page: 4 ----------------------
oSIST prEN ISO 20274:2016
ISO/DIS 20274:2016(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Apparatus . 1
4 Requirements for the test specimen . 1
5 Preparation of the test specimens . 2
5.1 General . 2
5.2 Production by casting. 2
5.3 Production by drawing out of the melt . 2
5.4 Production by sintering . 3
6 Determination of the thermal expansion coefficient . 3
7 Calculation and indication of the results . 4
8 Test report . 4
Annex A (Informative)Metallic casting mould . 5
Annex B (Informative)Drawing from the melt . 6
© ISO 2016 – All rights reserved iii

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oSIST prEN ISO 20274:2016
ISO/DIS 20274:2016(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International
Standards adopted by the technical committees are circulated to the member bodies for voting.
Publication as an International Standard requires approval by at least 75 % of the member bodies
casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO was prepared by Technical Committee ISO/TC 107, Metallic and other inorganic coatings,
Subcommittee SC , .
This second/third/. edition cancels and replaces the first/second/. edition (), [clause(s) / subclause(s)
/ table(s) / figure(s) / annex(es)] of which [has / have] been technically revised.
iv © ISO 2016 – All rights reserved

---------------------- Page: 6 ----------------------
oSIST prEN ISO 20274:2016
ISO/DIS 20274:2016(E)

Introduction
The thermal expansion coefficient of enamel and the relevant substrate is an important material
characteristic, as it provides information on the stress ratios in the composite material.
© ISO 2016 – All rights reserved v

---------------------- Page: 7 ----------------------
oSIST prEN ISO 20274:2016

---------------------- Page: 8 ----------------------
oSIST prEN ISO 20274:2016
DRAFT INTERNATIONAL STANDARD ISO/DIS 20274:2016(E)
Vitreous and Porcelain enamels — Preparation of samples
and determination of thermal expansion coefficient
1 Scope
This standard specifies the procedures for the preparation of enamel samples for measurement of the
thermal length change and calculation of the thermal expansion coefficient.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
ISO 7991, Glass – Determination of coefficient of mean linear thermal expansion
3 Apparatus
3.1 Standard laboratory instruments, instruments according to ISO 7991 and 3.2 to 3.4.
Note: An optical dilatometer may be used as an alternative to a pushrod dilatometer.
3.2 Casting mould made from ceramic, e.g. boat made from corundum, porcelain, or casting mould
made from metal, e.g. tool steel (see Annex A).
3.3 Melting crucible made from non-contaminating material, e.g. corundum, porcelain, with a height
of about 55 mm and a diameter of approximately 40 mm.
3.4 Laboratory furnace, in the temperature range from 800 °C to 1 100 °C controllable to ± 5 °C
4 Requirements for the test specimen
The test specimen shall be rod shaped and straight with either approximately circular cross section
with a diameter constant to ± 1mm over its length or approximately square cross section with an
edge length constant to ± 1mm over its length. The diameter or edge length of the test specimen shall
correspond ± 1mm to the diameter or edge length of the reference sample.
The faces shall be plane-parallel and vertical to the longitudinal axis of the specimen to maximum ± 3°.
The initial length shall be ± 0
...

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