Bitumen and bituminous binders - Bituminous emulsions, fluxed and cut-back bitumen factory production control

This European Standard specifies Factory Production Control (FPC) requirements for use by the manufacturers of bituminous emulsions, cut-back and fluxed binders. This European Standard is applicable to the control of bituminous binders where the constituents and composition are known, having been derived from a prescriptive specification or from the Initial Type Test (ITT) procedure for demonstration of performance related properties described in the appropriate product standard or from a European Technical Approval.

Bitumen und bitumenhaltige Bindemittel - Werkseigene Produktionskontrolle von Bitumenemulsionen, gefluxtem und verschnittenem Bitumen

Diese Europäische Norm legt Anforderungen an die werkseigene Produktionskontrolle (WPK) fest, die von den Herstellern von Bitumenemulsionen, verschnittenem und gefluxtem Bitumen anzuwenden sind.
Diese Europäische Norm gilt für die Kontrolle von bitumenhaltigen Bindemitteln, deren Bestandteile und Zusammensetzung bekannt sind, da sie aus einer vorschreibenden Spezifikation oder aus dem Erst-Typ-Prüfverfahren (ITT) für den Nachweis leistungsbezogener Eigenschaften, die in der entsprechenden Produk-tnorm beschrieben sind, oder aus einer Europäischen Technischen Zulassung entnommen wurden.
ANMERKUNG 1 Die werkseigene Produktionskontrolle ist eine Anforderung an alle harmonisierten Elemente von harmonisierten Europäischen Normen und Europäischen Technischen Zulassungen für bitumenhaltige Bindemittel, sofern das CE-Konformitätszeichen verwendet werden soll. Das System kann ebenso auf die nicht harmonisierten Elemente und in solchen Fällen angewendet werden, in denen eine CE-Kennzeichnung nicht verbindlich gefordert ist.
ANMERKUNG 2 In dieses Dokument wurden verbindlich vorgeschriebene Eigenschaften einbezogen.

Bitumes et liants bitumineux - Maîtrise de la production en usine des émulsions de bitume, des bitumes fluxés et fluidifiés

La présente Norme européenne spécifie les exigences relatives à la maîtrise de la production en usine (FPC),
à l'usage des producteurs d'émulsions de bitume, de liants fluidifiés et fluxés.
La présente Norme européenne est applicable à la maîtrise des liants bitumineux dont la nature des constituants et
leur teneur sont connues. Ces liants ayant été mis au point à partir soit de spécifications prescriptives, soit de la
procédure d'essai de type initial (ITT) destinée à révéler les propriétés reliées aux performances décrites dans la
norme appropriée relative au produit ou encore d’un Agrément Technique Européen.
NOTE 1 La maîtrise de la production en usine (FPC) est une exigence requise pour l'ensemble des éléments harmonisés
des Normes européennes harmonisées et des Agréments Techniques Européens (ETA) qui concernent les liants bitumineux,
lorsque la marque de conformité CE doit être apposée. Ce système peut aussi être appliqué à des éléments non harmonisés
et dans des cas où le marquage CE n'est pas obligatoire.
NOTE 2 Les propriétés réglementées des produits sont incluses dans le présent document.

Bitumen in bitumenska veziva - Kontrola proizvodnje v obratih za proizvodnjo bitumenskih emulzij ter fluksiranih in rezanih bitumnov

Ta evropski standard določa zahteve za kontrolo proizvodnje v obratih (FPC), ki jo uporabljajo proizvajalci bitumenskih emulzij, rezanih in fluksiranih bitumnov. Ta evropski standard se uporablja za nadzor bitumenskih veziv, kjer so sestavine in sestava znane in pridobljene iz predpisanih specifikacij ali s postopkom začetnega tipskega preskusa (ITT) za prikaz lastnosti, povezanih z delovanjem, opisanim v ustreznem standardu proizvoda ali v evropskih tehničnih soglasjih.

General Information

Status
Withdrawn
Publication Date
08-Mar-2011
Withdrawal Date
18-Jun-2013
Technical Committee
Current Stage
9900 - Withdrawal (Adopted Project)
Start Date
19-Jun-2013
Due Date
12-Jul-2013
Completion Date
19-Jun-2013

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen in bitumenska veziva - Kontrola proizvodnje v obratih za proizvodnjo bitumenskih emulzij ter fluksiranih in rezanih bitumnovBitumen und bitumenhaltige Bindemittel - Werkseigene Produktionskontrolle von Bitumenemulsionen, gefluxtem und verschnittenem BitumenBitumes et liants bitumineux - Maîtrise de la production en usine des émulsions de bitume, des bitumes fluxés et fluidifiésBitumen and bituminous binders - Bituminous emulsions, fluxed and cut-back bitumen factory production control91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 14733:2005+A1:2010SIST EN 14733:2005+A1:2011en,fr,de01-april-2011SIST EN 14733:2005+A1:2011SLOVENSKI
STANDARD



SIST EN 14733:2005+A1:2011



EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 14733:2005+A1
October 2010 ICS 75.140; 91.100.50 Supersedes EN 14733:2005English Version
Bitumen and bituminous binders - Bituminous emulsions, fluxed and cut-back bitumen factory production control
Bitumes et liants bitumineux - Maîtrise de la production en usine des émulsions de bitume, des bitumes fluxés et fluidifiés
Bitumen und bitumenhaltige Bindemittel - Werkseigene Produktionskontrolle von Bitumenemulsionen, gefluxtem und verschnittenem Bitumen This European Standard was approved by CEN on 21 April 2005 and includes Amendment 1 approved by CEN on 16 August 2010.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 14733:2005+A1:2010: ESIST EN 14733:2005+A1:2011



EN 14733:2005+A1:2010 (E) 2 Contents Page Foreword . 3Introduction . 41Scope . 52Normative references . 53Terms and definitions . 74Requirements . 74.1Factory Production Control (FPC): general . 74.2Quality Plan . 74.3Organisation . 84.4Document control . 95Control procedures. 95.1Constituent materials . 95.2Purchaser supplied product . 95.3Process control . 105.4Handling, storage and delivery . 105.5Factory calibration and maintenance . 106Inspection and testing . 106.1General . 106.2Incoming constituent materials . 106.3Finished binders . 117Non-conformity . 117.1General . 117.2Non-conformity of constituent material . 127.3Non-conformity of binders (arising from in-process inspection) . 127.4Non-conformity of binder (arising from analysis of finished product) . 128Inspection, measuring and test equipment . 129Records . 1310Operative competence . 13Bibliography . 20
SIST EN 14733:2005+A1:2011



EN 14733:2005+A1:2010 (E) 3 Foreword This document (EN 14733:2005+A1:2010) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by April 2011, and conflicting national standards shall be withdrawn at the latest by
April 2011. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. This document includes Amendment 1, approved by CEN on 2010-08-16. This document supersedes EN 14733:2005. The start and finish of text introduced or altered by amendment is indicated in the text by tags ! ". This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association, and supports essential requirements of EU Construction Products Directive 89/106/CE. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. SIST EN 14733:2005+A1:2011



EN 14733:2005+A1:2010 (E) 4 Introduction This European Standard for Factory Production Control (FPC) is suitable for use in more general quality systems in the binder industry. The document is based on certain requirements of EN ISO 9001 but stands alone and does not require reference to EN ISO 9001 for its application. The system in this European Standard builds mainly upon traditional sampling and testing of constituent materials and finished product. Processes as well as process control systems are continuously being developed which means that new systems for Factory Production Control will be introduced and implemented. If a producer is able to demonstrate that his process control system is able to secure the fulfilment of the requirements on the finished products in a satisfactory way then alternative frequencies of inspection and testing to those indicated in this document may be appropriate. The Factory Production Control (FPC) has the aim of providing adequate assurance that the binder conforms with the relevant technical specifications. The basis of this European Standard is that of the control of constituents, composition and manufacturing. It does not involve the routine monitoring of the performance properties of the binder. Concerning !cationic emulsions", this is dealt with separately in EN 13808 whereas for cut-back and bituminous binders, is dealt with by another standard, which is currently in progress. SIST EN 14733:2005+A1:2011



EN 14733:2005+A1:2010 (E) 5 1 Scope This European Standard specifies Factory Production Control (FPC) requirements for use by the manufacturers of bituminous emulsions, cut-back and fluxed binders. This European Standard is applicable to the control of bituminous binders where the constituents and composition are known, having been derived from a prescriptive specification or from the Initial Type Test (ITT) procedure for demonstration of performance related properties described in the appropriate product standard or from a European Technical Approval. NOTE 1 Factory Production Control is a requirement of all harmonised elements of harmonised European Standards and European Technical Approvals for bituminous binders if the CE mark of conformity is to be affixed. The system can also be applied to non-harmonised elements and to situations where CE marking is not mandatory. NOTE 2 Regulated properties of the products are involved in this document. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 1425, Bitumen and bituminous binders
Characterization of perceptible properties EN 1426, Bitumen and bituminous binders
Determination of needle penetration EN 1427, Bitumen and bituminous binders
Determination of the softening point
Ring and Ball method EN 1428, Bitumen and bituminous binders
Determination of water content in bitumen emulsions
Azeotropic distillation method EN 1429, Bitumen and bituminous binders
Determination of residue on sieving of bituminous emulsions and determination of storage stability by sieving EN 1431, !Bitumen and bituminous binders
Determination of residual binder and oil distillate from bitumen emulsions by distillation" !EN 12592, Bitumen and bituminous binders
Determination of solubility" EN 12595, Bitumen and bituminous binders
Determination of kinematic viscosity EN 12596, Bitumen and bituminous binders
Determination of dynamic viscosity by vacuum capillary !prEN 12846-1, Bitumen and bituminous binders
Determination of efflux time by the efflux viscometer
Part 1 : Bituminous emulsions" !prEN 12846-2, Bitumen and bituminous binders
Determination of efflux time by the efflux viscometer
Part 2 : Cut-back and fluxed bituminous binders" !EN 12847, Bitumen and bituminous binders
Determination of settling tendency of bituminous emulsions"
EN 12848, Bitumen and bituminous binders
Determination of mixing stability with cement of bituminous emulsions EN 12850, Bitumen and bituminous binders
Determination of the pH value of bituminous emulsions !prEN 13074-1:2008, Bitumen and bituminous binders
Recovery of binder from bituminous emulsion or from cut-back or fluxed bitumen by evaporation" SIST EN 14733:2005+A1:2011



EN 14733:2005+A1:2010 (E) 6 !prEN 13074-2, Bitumen and bituminous binders
Stabilisation of binder from bituminous emulsion or from cut-back or fluxed bitumen after recovery" EN 13075-1, Bitumen and bituminous binders
Determination of breaking behaviour
Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method EN 13075-2, Bitumen and bituminous binders
Determination of breaking behaviour
Part 2: Determination of fines mixing time of cationic bituminous emulsions !EN 13302, Bitumen and bituminous binders
Determination of dynamic viscosity of bituminous binder using a rotating spindle apparatus" !deleted text" EN 13358, Bitumen and bituminous binders
Determination of the distillation characteristics of petroleum cut-back bitumen products !EN 13398, Bitumen and bituminous binders
Determination of the elastic recovery of modified bitumen" EN 13587, Bitumen and bituminous binders
Determination of the tensile properties of bituminous binders by the tensile test method EN 13588, Bitumen and bituminous binders
Determination of cohesion of bituminous binders with pendulum test EN 13589, Bitumen and bituminous binders
Determination of the tensile properties of modified bitumen by the force ductility method !EN 13614, Bitumen and bituminous binders
Determination of adhesivity of bitumen emulsions by water immersion test
Aggregate method" EN 13703, Bitumen and bituminous binders
Determination of deformation energy !EN 13808, Bitumen and bituminous binders
Framework for specifying cationic bituminous emulsions" !EN 14769, Bitumen and bituminous binders
Accelerated long-term ageing conditioning by a Pressure Ageing Vessel (PAV)" !deleted text" !EN 15322, Bitumen and bituminous binders
Framework for specifying cut-back and fluxed bituminous binders EN 15626, Bitumen and bituminous binders
Determination of adhesivity of cut-back and fluxed bituminous binders by water immersion test
Aggregate method EN ISO 2592, Determination of flash and fire points
Cleveland open cup method (ISO 2592:2000)" EN ISO 2719, Determination of flash point
Pensky-Martens closed cup method (ISO 2719:2002) EN ISO 3405, Petroleum products
Determination of distillation characteristics at atmospheric pressure (ISO 3405:2000) EN ISO 3675, Crude petroleum and liquid petroleum products
Laboratory determination of density
Hydrometer method (ISO 3675:1998) EN ISO 9001, !Quality management systems
Requirements (ISO 9001:2008)" !EN ISO 13736, Determination of flash point
Abel closed cup method (ISO 13736:2008)" SIST EN 14733:2005+A1:2011



EN 14733:2005+A1:2010 (E) 7 3 Terms and definitions For the purposes of this European Standard, the following terms and definitions apply. 3.1 Factory Production Control (FPC) permanent internal control of production exercised by the manufacturer. All the elements, requirements and provisions adopted by the manufacturer are documented in a systematic manner in the form of written policies and procedures. This production control system documentation ensures a common understanding of quality assurance and enables the achievement of the required product characteristics and the effective operation of the production control system to be checked NOTE 1 Factory Production Control (FPC) includes the inspections and tests used to monitor the equipment, constituent materials, manufacturing process and the finished product. NOTE 2 The task of Factory Production Control (FPC) is to give assurance that production conforms with the relevant Initial Type Test. 3.2 technical specifications harmonised European Standards and European Technical Approvals for bituminous emulsion, cut-back and fluxed binders 3.3 perceptible properties evaluation made with the senses: sight, touch, smell, hearing, etc. It is a broader concept than the more commonly used term of a visual inspection. EXAMPLE A check on a bitumen delivery might involve visual (colour, fuming and texture), smell (odour) and touch (how it feels when cold). This would detect whether the bitumen conformed with the expectations of the tester and would be the quickest way to detect a defective load. NOTE In all cases organoleptic checks should extend only as far as health and safety regulations permit. 3.4 Initial Type Test (ITT) complete set of tests or other procedures described in the technical specification, determining the performance of samples of products representative of the product type 4 Requirements ! 4.1 Factory Production Control (FPC): general The producer shall operate a documented Factory Production Control (FPC) system complying with the requirements of this document. The manufacturer shall establish, document and maintain an FPC system to ensure that the products placed on the market conform to the stated characteristics. The FPC system shall consist of procedures, regular inspections and tests and/or assessments and the use of the results to control the quality of the finished product. An FPC system conforming to the requirements of EN ISO 9001 and made specific to the requirements of this standard shall be deemed to satisfy the above requirements." 4.2 Quality Plan The producer shall establish and maintain his policy and procedures for Factory Production Control in a written Quality Plan. SIST EN 14733:2005+A1:2011



EN 14733:2005+A1:2010 (E) 8 The Quality Plan shall particularly include means for identifying and detailing the specific processes, which directly affect product quality and conformity. The Quality Plan shall particularly include:  producer's organisational structure relating to conformity;  document control;  control procedures for constituent materials and purchaser supplied product;  control procedures for the competence of production operators in the use and maintenance of production and test equipment;  identification of characteristics subject to FPC;  process control;  requirements for the handling and storage of the product;  factory calibration and maintenance of manufacturing and test equipment;  requirements for inspection and testing processes and products;  procedures for handling non-conformity;  sampling frequency and retention (if appropriate). The Quality Plan shall also include frequencies of inspection and testing. The frequencies given under Tables 1 to 4 are the minimum frequencies to be used initially. These may be changed where an alternative statistical system is developed and is accepted which provides equal or better confidence in the conformity of the product. NOTE The detail of the Quality Plan and of the Factory Production Control procedures will be factory and process dependent. 4.3 Organisation 4.3.1 Responsibilities and authority The responsibilities, authority and inter-relation of all personnel who manage, perform and verify work affecting quality and conformity shall be defined in the Quality Plan, particularly for personnel who have authority to: a) initiate action to prevent the occurrence of product non-conformity; b) identify and record any product quality problems; c) initiate and manage corrective action. 4.3.2 Management representative The management shall appoint a person with appropriate authority, knowledge and experience to supervise factory production control and to ensure that the requirements of the Quality Plan are implemented and maintained. NOTE An individual may exercise such supervision over a group of production units. SIST EN 14733:2005+A1:2011



EN 14733:2005+A1:2010 (E) 9 4.3.3 Internal audits The producer shall carry out internal quality and conformity audits to verify which process activities comply with the FPC and to determine the effectiveness of the FPC system. Audits shall be scheduled on the basis of the nature of the process used status and importance of the activity and record of conformity. The audits and follow up action shall be carried out in accordance with documented procedures. The results of the audits shall be documented and brought to the attention of the personnel having responsibility in the area audited. The management personnel responsible for the area shall take timely corrective action on the deficiencies found by the audit and shall keep a record of the action taken. 4.3.4 Management review The Factory Production Control (FPC) system shall be reviewed at least once per year by management to ensure its continuing suitability and effectiveness. Records of such reviews shall be maintained. 4.3.5 Sub-contract services Where any sub-contracted services are supplied from outside the producer’s resources, an agreed and document
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