Bitumen and bituminous binders - Bituminous emulsions, fluxed and cut-back bitumen factory production control

This European Standard specifies Factory Production Control (FPC) requirements for use by the manufacturers of bituminous emulsions, cut-back and fluxed binders.
This European Standard is applicable to the control of bituminous binders where the constituents and composition are known, having been derived from a prescriptive specification or from the Initial Type Test (ITT) procedure for demonstration of performance related properties described in the appropriate product standard or from a European Technical Approval.
NOTE 1      Factory Production Control is a requirement of all harmonised elements of harmonised European Standards and European Technical Approvals for bituminous binders if the CE mark of conformity is to be affixed. The system can also be applied to non-harmonised elements and to situations where CE marking is not mandatory.
NOTE 2      Regulated properties of the products are involved in this document.

Bitumen und bitumenhaltige Bindemittel - Werkseigene Produktionskontrolle von Bitumenemulsionen, gefluxtem und verschnittenem Bitumen

Diese Europäische Norm legt Anforderungen an die werkseigene Produktionskontrolle (WPK) fest, die von
den Herstellern von Bitumenemulsionen, verschnittenem und gefluxtem Bitumen anzuwenden sind.
Diese Europäische Norm gilt für die Kontrolle von bitumenhaltigen Bindemitteln, deren Bestandteile und
Zusammensetzung bekannt sind, da sie aus einer vorschreibenden Spezifikation oder aus dem Erst-Typ-
prüfverfahren (ITT) für den Nachweis leistungsbezogener Eigenschaften, die in der entsprechenden
Produktnorm beschrieben sind, oder aus einer Europäischen Technischen Zulassung entnommen wurden.
ANMERKUNG 1 Die werkseigene Produktionskontrolle ist eine Anforderung an alle harmonisierten Elemente von
harmonisierten Europäischen Normen und Europäischen Technischen Zulassungen für bitumenhaltige Bindemittel, sofern
das CE-Konformitätszeichen verwendet werden soll. Das System kann ebenso auf die nicht harmonisierten Elemente und
in solchen Fällen angewendet werden, in denen eine CE-Kennzeichnung nicht verbindlich gefordert ist.
ANMERKUNG 2 In dieses Dokument wurden verbindlich vorgeschriebene Eigenschaften einbezogen.

Bitumes et liants bitumineux - Maîtrise de la production en usine des émulsions de bitume, des bitumes fluxés et fluidifiés

La présente Norme européenne spécifie les exigences relatives a la maîtrise de la production en usine (FPC), a
l'usage des producteurs d'émulsions de bitume, de liants fluidifiés et fluxés.
La présente Norme européenne est applicable a la maîtrise des liants bitumineux dont la nature des constituants et
leur teneur sont connues. Ces liants ayant été mis au point a partir soit de spécifications prescriptives, soit de la
procédure d'essai de type initial (ITT) destinée a révéler les propriétés reliées aux performances décrites dans la
norme appropriée relative au produit ou encore d?un Agrément Technique Européen.
NOTE 1 La maîtrise de la production en usine (FPC) est une exigence requise pour l'ensemble des éléments harmonisés
des Normes européennes harmonisées et des Agréments Techniques Européens (ETA) qui concernent les liants bitumineux,
lorsque la marque de conformité CE doit etre apposée. Ce systeme peut aussi etre appliqué a des éléments non harmonisés et
dans des cas ou le marquage CE n'est pas obligatoire.
NOTE 2 Les propriétés réglementées des produits sont incluses dans le présent document.

Bitumen in bitumenska veziva – Kontrola proizvodnje v obratih za proizvodnjo bitumenskih emulzij ter fluksiranih in rezanih bitumnov

General Information

Status
Withdrawn
Publication Date
31-Oct-2005
Withdrawal Date
06-Feb-2011
Technical Committee
Current Stage
9900 - Withdrawal (Adopted Project)
Start Date
04-Feb-2011
Due Date
27-Feb-2011
Completion Date
07-Feb-2011

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SLOVENSKI STANDARD
SIST EN 14733:2005
01-november-2005
Bitumen in bitumenska veziva – Kontrola proizvodnje v obratih za proizvodnjo
bitumenskih emulzij ter fluksiranih in rezanih bitumnov
Bitumen and bituminous binders - Bituminous emulsions, fluxed and cut-back bitumen
factory production control
Bitumen und bitumenhaltige Bindemittel - Werkseigene Produktionskontrolle von
Bitumenemulsionen, gefluxtem und verschnittenem Bitumen
Bitumes et liants bitumineux - Maîtrise de la production en usine des émulsions de
bitume, des bitumes fluxés et fluidifiés
Ta slovenski standard je istoveten z: EN 14733:2005
ICS:
75.140 Voski, bitumni in drugi naftni Waxes, bituminous materials
proizvodi and other petroleum products
91.100.50 Veziva. Tesnilni materiali Binders. Sealing materials
SIST EN 14733:2005 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN 14733:2005

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SIST EN 14733:2005
EUROPEAN STANDARD
EN 14733
NORME EUROPÉENNE
EUROPÄISCHE NORM
May 2005
ICS 75.140; 91.100.50
English version
Bitumen and bituminous binders - Bituminous emulsions, fluxed
and cut-back bitumen factory production control
Bitumes et liants bitumineux - Maîtrise de la production en Bitumen und bitumenhaltige Bindemittel - Werkseigene
usine des émulsions de bitume, des bitumes fluxés et Produktionskontrolle von Bitumenemulsionen, gefluxtem
fluidifiés und verschnittenem Bitumen
This European Standard was approved by CEN on 21 April 2005.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Central Secretariat or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official
versions.
CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,
Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,
Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2005 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 14733:2005: E
worldwide for CEN national Members.

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SIST EN 14733:2005
EN 14733:2005 (E)
Contents
Page
Foreword .3
Introduction.4
1 Scope .5
2 Normative references .5
3 Terms and definitions.7
4 Requirements .7
4.1 Factory Production Control (FPC) .7
4.2 Quality Plan .7
4.3 Organisation.8
4.4 Document control .9
5 Control procedures.9
5.1 Constituent materials .9
5.2 Purchaser supplied product.9
5.3 Process control.9
5.4 Handling, storage and delivery .10
5.5 Factory calibration and maintenance.10
6 Inspection and testing .10
6.1 General .10
6.2 Incoming constituent materials .10
6.3 Finished binders .10
7 Non-conformity .11
7.1 General .11
7.2 Non-conformity of constituent material .11
7.3 Non-conformity of binders (arising from in-process inspection).11
7.4 Non-conformity of binder (arising from analysis of finished product) .11
8 Inspection, measuring and test equipment.12
9 Records .12
10 Operative competence.12
Bibliography.17


2

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SIST EN 14733:2005
EN 14733:2005 (E)
Foreword
This document (EN 14733:2005) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”,
the secretariat of which is held by AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an identical text or
by endorsement, at the latest by November 2005, and conflicting national standards shall be withdrawn at the latest
by November 2005.
This document has been prepared under a mandate given to CEN by the European Commission and the European
Free Trade Association, and supports essential requirements of EU Construction Products Directive 89/106/CE.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark,
Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
3

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SIST EN 14733:2005
EN 14733:2005 (E)
Introduction
This European Standard for Factory Production Control (FPC) is suitable for use in more general quality systems in
the binder industry. The document is based on certain requirements of EN ISO 9001 but stands alone and does not
require reference to EN ISO 9001 for its application.
The system in this European Standard builds mainly upon traditional sampling and testing of constituent materials
and finished product. Processes as well as process control systems are continuously being developed which
means that new systems for Factory Production Control will be introduced and implemented. If a producer is able to
demonstrate that his process control system is able to secure the fulfilment of the requirements on the finished
products in a satisfactory way then alternative frequencies of inspection and testing to those indicated in this
document may be appropriate.
The Factory Production Control (FPC) has the aim of providing adequate assurance that the binder conforms with
the relevant technical specifications.
The basis of this European Standard is that of the control of constituents, composition and manufacturing. It does not
involve the routine monitoring of the performance properties of the binder. Concerning catatonic emulsions, this is
dealt with separately in EN 13808 whereas for cut-back and bituminous binders, is dealt with by another standard,
which is currently in progress.
4

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SIST EN 14733:2005
EN 14733:2005 (E)

1 Scope
This European Standard specifies Factory Production Control (FPC) requirements for use by the manufacturers of
bituminous emulsions, cut-back and fluxed binders.
This European Standard is applicable to the control of bituminous binders where the constituents and composition
are known, having been derived from a prescriptive specification or from the Initial Type Test (ITT) procedure for
demonstration of performance related properties described in the appropriate product standard or from a European
Technical Approval.
NOTE 1 Factory Production Control is a requirement of all harmonised elements of harmonised European Standards and
European Technical Approvals for bituminous binders if the CE mark of conformity is to be affixed. The system can also be
applied to non-harmonised elements and to situations where CE marking is not mandatory.
NOTE 2 Regulated properties of the products are involved in this document.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated references,
only the edition cited applies. For undated references, the latest edition of the referenced document (including any
amendments) applies.
EN 1425, Bitumen and bituminous binders – Characterization of perceptible properties
EN 1426, Bitumen and bituminous binders – Determination of needle penetration
EN 1427, Bitumen and bituminous binders – Determination of softening point – Ring and Ball method
EN 1428, Bitumen and bituminous binders – Determination of water content in bitumen emulsions – Azeotropic
distillation method
EN 1429, Bitumen and bituminous binders – Determination of residue on sieving of bitumen emulsions and
determination of storage stability by sieving
EN 1431, Bitumen and bituminous binders – Determination of recovered binder and oil distillate from bitumen
emulsions by distillation
EN 12595, Bitumen and bituminous binders – Determination of kinematic viscosity
EN 12596, Bitumen and bituminous binders – Determination of dynamic viscosity by vacuum capillary
EN 12846, Bitumen and bituminous binders – Determination of the efflux time of bitumen emulsions by the efflux
viscosimeter
EN 12848, Bitumen and bituminous binders – Determination of mixing stability with cement of bitumen emulsions
EN 12850, Bitumen and bituminous binders – Determination of the pH value of bitumen emulsions
EN 13074, Bitumen and bituminous binders – Recovery of binder from emulsion by evaporation
EN 13075-1, Bitumen and bituminous binders – Determination of breaking behaviour – Part 1: Determination of
breaking value of cationic bitumen emulsions, mineral filler method
EN 13075-2, Bitumen and bituminous binders – Determination of breaking behaviour – Part 2: Determination of
fines mixing time of cationic bitumen emulsions
5

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SIST EN 14733:2005
EN 14733:2005 (E)
EN 13357, Bitumen and bituminous binders – Determination of the efflux time of petroleum cut-back and fluxed
bitumen
EN 13358, Bitumen and bituminous binders – Determination of the distillation characteristics of petroleum cut-back
bitumen products
EN 13587, Bitumen and bituminous binders – Determination of the tensile properties of bituminous binders by the
tensile test method
EN 13588, Bitumen and bituminous binders – Determination of cohesion of bituminous binders with pendulum test
EN 13589, Bitumen and bituminous binders – Determination of the tensile properties of modified bitumen by the
force ductility method
EN 13703, Bitumen and bituminous binders – Determination of deformation energy
prEN 14769, Bitumen and bituminous binders – Accelerated long-term ageing - Pressure Ageing Vessel (PAV)
prEN 14895, Bitumen and bituminous binders – Stabilisation of binder from bituminous emulsion or from cut-back
and fluxed bitumen
prEN 14896, Bitumen and bituminous binders – Determination of the dynamic viscosity of bituminous emulsions –
Rotating spindle viscometer method
EN ISO 2719, Determination of flash point – Pensky-Martens closed cup method (ISO 2719:2002)
EN ISO 3405, Petroleum products – Determination of distillation characteristics method at atmospheric pressure
(ISO 3405:2000)
EN ISO 3675, Crude petroleum and liquid petroleum products – Laboratory determination of density – Hydrometer
method (ISO 3675:1998)
EN ISO 9001, Quality management systems – Requirements (ISO 9001:2000)
6

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SIST EN 14733:2005
EN 14733:2005 (E)
3 Terms and definitions
For the purposes of this European Standard, the following terms and definitions apply.
3.1
Factory Production Control (FPC)
permanent internal control of production exercised by the manufacturer. All the elements, requirements and
provisions adopted by the manufacturer are documented in a systematic manner in the form of written policies and
procedures. This production control system documentation ensures a common understanding of quality assurance
and enables the achievement of the required product characteristics and the effective operation of the production
control system to be checked
NOTE 1 Factory Production Control (FPC) includes the inspections and tests used to monitor the equipment, constituent
materials, manufacturing process and the finished product.
NOTE 2 The task of Factory Production Control (FPC) is to give assurance that production conforms with the relevant Initial
Type Test.
3.2
technical specifications
harmonised European Standards and European Technical Approvals for bituminous emulsion, cut-back and fluxed
binders
3.3
perceptible properties
evaluation made with the senses: sight, touch, smell, hearing, etc. It is a broader concept than the more commonly
used term of a visual inspection.
EXAMPLE a check on a bitumen delivery might involve visual (colour, fuming and texture), smell (odour) and
touch (how it feels when cold). This would detect whether the bitumen conformed with the expectations of the
tester and would be the quickest way to detect a defective load
NOTE In all cases organoleptic checks should extend only as far as health and safety regulations permit.
3.4
Initial Type Test (ITT)
complete set of tests or other procedures described in the technical specification, determining the performance of
samples of products representative of the product type
4 Requirements
4.1 Factory Production Control (FPC)
The producer shall operate a documented Factory Production Control (FPC) system complying with the
requirements of this document.
4.2 Quality Plan
The producer shall establish and maintain his policy and procedures for Factory Production Control in a written
Quality Plan.
The Quality Plan shall particularly include means for identifying and detailing the specific processes, which directly
affect product quality and conformity.
The Quality Plan shall particularly include:
 producer's organisational structure relating to conformity;
7

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SIST EN 14733:2005
EN 14733:2005 (E)
 document control;
 control procedures for constituent materials and purchaser supplied product;
 control procedures for the competence of production operators in the use and maintenance of production
and test equipment;
 identification of characteristics subject to FPC;
 process control;
 requirements for the handling and storage of the product;
 factory calibration and maintenance of manufacturing and test equipment;
 requirements for inspection and testing processes and products;
 procedures for handling non-conformity;
 sampling frequency and retention (if appropriate).
The Quality Plan shall also include frequencies of inspection and testing. The frequencies given under Tables 1 to
4 are the minimum frequencies to be used initially. These may be changed where an alternative statistical system
is developed and is accepted which provides equal or better confidence in the conformity of the product.
NOTE The detail of the Quality Plan and of the Factory Production Control procedures will be factory and process
dependent.
4.3 Organisation
4.3.1 Responsibilities and authority
The responsibilities, authority and inter-relation of all personnel who manage, perform and verify work affecting
quality and conformity shall be defined in the Quality Plan, particularly for personnel who have authority to:
a) initiate action to prevent the occurrence of product non-conformity;
b) identify and record any product quality problems;
c) initiate and manage corrective action.
4.3.2 Management representative
The management shall appoint a person with appropriate authority, knowledge and experience to supervise factory
production control and to ensure that the requirements of the Quality Plan are implemented and maintained.
NOTE An individual may exercise such supervision over a group of produc
...

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