SIST EN ISO 3262-18:2023
(Main)Extenders - Specifications and methods of test - Part 18: Precipitated sodium aluminium silicate (ISO 3262-18:2023)
Extenders - Specifications and methods of test - Part 18: Precipitated sodium aluminium silicate (ISO 3262-18:2023)
This document specifies requirements and corresponding methods of test for precipitated sodium aluminium silicate.
Füllstoffe - Anforderungen und Prüfverfahren - Teil 18: Gefälltes Natriumaluminiumsilicat (ISO 3262-18:2023)
Dieses Dokument legt Anforderungen und die entsprechenden Prüfverfahren für gefälltes Natriumaluminiumsilicat fest.
Matières de charge - Spécifications et méthodes d’essai - Partie 18: Silicoaluminate de sodium précipité (ISO 3262-18:2023)
Le présent document spécifie les exigences relatives au silicoaluminate de sodium précipité ainsi que les méthodes d’essai correspondantes.
Polnila - Specifikacije in preskusne metode - 18. del: Oborjeni natrijev aluminijev silikat (ISO 3262-18:2023)
Ta del standarda ISO 3262 določa zahteve in ustrezne preskusne metode za oborjeni natrijev aluminijev silikat.
General Information
Relations
Standards Content (Sample)
SLOVENSKI STANDARD
01-oktober-2023
Nadomešča:
SIST EN ISO 3262-18:2001
Polnila - Specifikacije in preskusne metode - 18. del: Oborjeni natrijev aluminijev
silikat (ISO 3262-18:2023)
Extenders - Specifications and methods of test - Part 18: Precipitated sodium aluminium
silicate (ISO 3262-18:2023)
Füllstoffe - Anforderungen und Prüfverfahren - Teil 18: Gefälltes Natriumaluminiumsilicat
(ISO 3262-18:2023)
Matières de charge - Spécifications et méthodes d’essai - Partie 18: Silicoaluminate de
sodium précipité (ISO 3262-18:2023)
Ta slovenski standard je istoveten z: EN ISO 3262-18:2023
ICS:
87.060.10 Pigmenti in polnila Pigments and extenders
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EN ISO 3262-18
EUROPEAN STANDARD
NORME EUROPÉENNE
August 2023
EUROPÄISCHE NORM
ICS 87.060.10 Supersedes EN ISO 3262-18:2000
English Version
Extenders - Specifications and methods of test - Part 18:
Precipitated sodium aluminium silicate (ISO 3262-
18:2023)
Matières de charge - Spécifications et méthodes d'essai Füllstoffe - Anforderungen und Prüfverfahren - Teil 18:
- Partie 18: Silicoaluminate de sodium précipité (ISO Gefälltes Natriumaluminiumsilicat (ISO 3262-18:2023)
3262-18:2023)
This European Standard was approved by CEN on 2 July 2023.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 3262-18:2023 E
worldwide for CEN national Members.
Contents Page
European foreword . 3
European foreword
This document (EN ISO 3262-18:2023) has been prepared by Technical Committee ISO/TC 256
"Pigments, dyestuffs and extenders" in collaboration with Technical Committee CEN/TC 298 “Pigments
and extenders” the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by February 2024, and conflicting national standards
shall be withdrawn at the latest by February 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 3262-18:2000.
Any feedback and questions on this document should be directed to the users’ national standards
body/national committee. A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 3262-18:2023 has been approved by CEN as EN ISO 3262-18:2023 without any
modification.
INTERNATIONAL ISO
STANDARD 3262-18
Second edition
2023-07
Extenders — Specifications and
methods of test —
Part 18:
Precipitated sodium aluminium
silicate
Matières de charge — Spécifications et méthodes d’essai —
Partie 18: Silicoaluminate de sodium précipité
Reference number
ISO 3262-18:2023(E)
ISO 3262-18:2023(E)
© ISO 2023
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
ISO 3262-18:2023(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Requirements and test methods . 2
5 Sampling . 2
6 Determination of silica content . 2
6.1 Principle . 2
6.2 Reagents . 2
6.3 Apparatus . 3
6.4 Procedure . 3
6.4.1 Number of determinations . 3
6.4.2 Test portion . 4
6.4.3 Determination . 4
6.4.4 Determination of the total loss on ignition . 4
6.5 Expression of results . . 5
6.6 Precision . . . 5
6.6.1 Repeatability, r . 5
6.6.2 Reproducibility, R . 5
7 Determination of the composition by spectrometry . 5
7.1 Principle . 5
7.2 Reagents and materials . 6
7.3 Apparatus . 6
7.4 Procedure . 7
7.4.1 Preparation of standard matching solutions . 7
7.4.2 Spectrometric measurement . 7
7.4.3 Calibration graph . 8
7.4.4 Preparation of the test solution . 8
7.4.5 Determination . 8
7.5 Expression of results . 9
7.5.1 Concentration of Al, Na and Si . 9
7.5.2 Calculation of the oxide content for each element . 9
7.6 Precision . . . 9
7.6.1 Repeatability, r . 9
7.6.2 Reproducibility, R . 10
8 Determination of residue on sieve .10
8.1 Principle . 10
8.2 Materials . 10
8.3 Apparatus . 10
8.4 Procedure . 10
8.4.1 Number of determinations . 10
8.4.2 Test portion . 10
8.4.3 Determination . 11
8.5 Expression of results . . 11
8.6 Precision . . . 11
9 Test report .11
Bibliography .12
iii
ISO 3262-18:2023(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO document should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
ISO draws attention to the possibility that the implementation of this document may involve the use
of (a) patent(s). ISO takes no position concerning the evidence, validity or applicability of any claimed
patent rights in respect thereof. As of the date of publication of this document, ISO had not received
notice of (a) patent(s) which may be required to implement this document. However, implementers are
cautioned that this may not represent the latest information, which may be obtained from the patent
database available at www.iso.org/patents. ISO shall not be held responsible for identifying any or all
such patent rights.
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to
the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see
www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 256, Pigments, dyestuffs and extenders, in
collaboration with the European Committee for Standardization (CEN) Technical Committee CEN/TC
298, Pigments and extenders, in accordance with the Agreement on technical cooperation between ISO
and CEN (Vienna Agreement).
This second edition cancels and replaces the first edition (ISO 3262-18:2000), which has been technically
revised.
The main changes are as follows:
— the first part of the title has been changed to “Extenders”;
— the normative references have been updated.
A list of all parts in the ISO 3262 series can be found on the ISO website.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.
iv
INTERNATIONAL STANDARD ISO 3262-18:2023(E)
Extenders — Specifications and methods of test —
Part 18:
Precipitated sodium aluminium silicate
1 Scope
This document specifies requirements and corresponding methods of test for precipitated sodium
aluminium silicate.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 648, Laboratory glassware — Single-volume pipettes
ISO 787-2, General methods of test for pigments and extenders — Part 2: Determination of matter volatile
at 105 °C
ISO 787-5, General methods of test for pigments and extenders — Part 5: Determination of oil absorption
value
ISO 787-9, General methods of test for pigments and extenders — Part 9: Determination of pH value of an
aqueous suspension
ISO 3262-1, Extenders — Specifications and methods of test — Part 1: Introduction and general test
methods
ISO 3696, Water for analytical laboratory use — Specification and test methods
ISO 5794-1:2022, Rubber compounding ingredients — Silica, precipitated, hydrated — Part 1: Non-rubber
tests
ISO 15528, Paints, varnishes and raw materials for paints and varnishes — Sampling
ISO 18451-1, Pigments, dyestuffs and extenders — Terminology — Part 1: General terms
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO 18451-1 and the following
apply.
ISO and IEC maintain terminology databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https:// www .iso .org/ obp
— IEC Electropedia: available at https:// www .electropedia .org/
3.1
precipitated sodium aluminium silicate
amorphous silicate precipitated by the reaction of sodium silicate solution with a mineral acid and/or
an aluminium salt
ISO 3262-18:2023(E)
4 Requirements and test methods
For precipitated sodium aluminium silicate complying with this document, the essential requirements
are specified in Table 1 and the conditional requirements are listed in Table 2. The test methods listed
in Tables 1 and 2 shall apply.
Table 1 — Essential requirements
Characteristic Unit Requirement Test method
Silica content, min. 75 See Clause 6 or 7
Oxide content
% mass fraction 3 to 10
— Na O
2 See Clause 7
— Al O
5 to 15
2 3
Residue on 45 µm sieve, max. % mass fraction 2 See Clause 8
Lightness, min. % 95 Test method in preparation
Matter volatile at 105 °C, max. % mass fraction 10 ISO 787-2
Loss on ignition % mass fraction 3 to 12 ISO 3262-1
a
Oil absorption value , min. g/100 g 70 ISO 787-5
pH value of aqueous suspension — 7 to 12 ISO 787-9
a
A test method with higher reproducibility and repeatability is described in ASTM D2414. However, the results cannot
be compared directly with oil absorption values determined in accordance with ISO 787-5.
Table 2 — Conditional requirements
Characteristic Unit Requirement Test method
Particle size distribution To be agreed between
% mass fraction
To be agreed between
(instrumental method) the interested parties
the interested parties
Specific surface area m /g ISO 5794-1:2022, Annex D
5 Sampling
Take a representative sample of the product to be tested, in accordance with ISO 15528.
6 Determination of silica content
6.1 Principle
A test portion is repeatedly treated with hydrochloric acid and evaporated to dryness. To render the
dehydrated silicic acid thus formed as insoluble as possible, it is then heated for 2
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.
Loading comments...