Organic and organo-mineral fertilizers - Determination of specific elements

The document establishes the methodology for the determination of :
- total P2O5, K2O, CaO, MgO, Na2O, SO3 content in organic and organo-mineral fertilizers;
- inorganic As, Cd, total Cr, Hg, Ni, Pb, Cu, Zn content in organic and organo-mineral fertilizers;  
- water soluble CaO, MgO, Na2O, SO3 content in organic and organo-mineral fertilizers;
- water soluble P2O5, K2O content in organo-mineral fertilizers;
- neutral ammonium citrate soluble P2O5 content in organo-mineral fertilizers;
- formic acid soluble P2O5 content in organo-mineral fertilizers;
- total B, Co, Fe, Mn, Mo content in organo-mineral fertilizers;
- water soluble B, Co, Cu, Fe, Mn, Mo, and Zn content in organo-mineral fertilizers;

Organische und organisch-mineralische Düngemittel - Bestimmung spezifischer Elemente

Engrais organiques et organo-minéraux - Détermination des éléments spécifiques

Le présent document spécifie les références aux méthodes de détermination des éléments spécifiques suivants dans les engrais organiques et organo-minéraux :
—   Détermination de la teneur en phosphore total ;
—   Détermination de la teneur en potassium total ;
—   Détermination de la teneur en calcium total ;
—   Détermination de la teneur en magnésium total ;
—   Détermination de la teneur en sodium total ;
—   Détermination de la teneur en soufre total ;
—   Détermination de la teneur en arsenic inorganique ;
—   Détermination de la teneur en cadmium ;
—   Détermination de la teneur en chrome total ;
—   Détermination de la teneur en mercure total ;
—   Détermination de la teneur en nickel total ;
—   Détermination de la teneur en plomb total ;
—   Détermination de la teneur en cuivre total ;
—   Détermination de la teneur en zinc total ;
—   Détermination de la teneur en calcium soluble dans l'eau ;
—   Détermination de la teneur en magnésium soluble dans l'eau ;
—   Détermination de la teneur en sodium soluble dans l'eau ;
—   Détermination de la teneur en soufre soluble dans l'eau.
Le présent document spécifie les références aux méthodes de détermination des éléments spécifiques suivants dans les engrais organo-minéraux :
—   Détermination de la teneur en phosphore soluble dans l'eau ;
—   Détermination de la teneur en potassium soluble dans l'eau ;
—   Détermination de la teneur en phosphore soluble dans le citrate d'ammonium neutre ;
—   Détermination de la teneur en phosphore soluble dans l'acide formique ;
—   Détermination de la teneur en bore total ;
—   Détermination de la teneur en cobalt total ;
—   Détermination de la teneur en fer total ;
—   Détermination de la teneur en manganèse total ;
—   Détermination de la teneur en molybdène total ;
—   Détermination de la teneur en bore soluble dans l'eau ;
—   Détermination de la teneur en cobalt soluble dans l'eau ;
—   Détermination de la teneur en cuivre soluble dans l'eau ;
—   Détermination de la teneur en fer soluble dans l'eau ;
—   Détermination de la teneur en manganèse soluble dans l'eau ;
—   Détermination de la teneur en molybdène soluble dans l'eau ;
—   Détermination de la teneur en zinc soluble dans l'eau.
Le présent document est applicable aux fertilisants, qui sont classés comme PFC 1(A) et PFC 1(B) ou comme composant PFC 1(A) et PFC 1(B) dans la PFC 7 du règlement (UE) 2019/1009 [1]. Cependant, la présente méthode n'a pas été validée pour les combinaisons.

Organska in organsko-mineralna gnojila - Določevanje specifičnih elementov

General Information

Status
Published
Public Enquiry End Date
02-Jan-2022
Publication Date
09-Jan-2023
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
06-Jan-2023
Due Date
13-Mar-2023
Completion Date
10-Jan-2023

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST-TS CEN/TS 17777:2023
01-februar-2023
Organska in organsko-mineralna gnojila - Določevanje specifičnih elementov
Organic and organo-mineral fertilizers - Determination of specific elements
Organische und organisch-mineralische Düngemittel - Bestimmung spezifischer
Elemente
Engrais organiques et organo-minéraux - Détermination des éléments spécifiques
Ta slovenski standard je istoveten z: CEN/TS 17777:2022
ICS:
65.080 Gnojila Fertilizers
SIST-TS CEN/TS 17777:2023 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST-TS CEN/TS 17777:2023
---------------------- Page: 2 ----------------------
SIST-TS CEN/TS 17777:2023
CEN/TS 17777
TECHNICAL SPECIFICATION
SPÉCIFICATION TECHNIQUE
April 2022
TECHNISCHE SPEZIFIKATION
ICS 65.080
English Version
Organic and organo-mineral fertilizers - Determination of
specific elements

Engrais organiques et organo-minéraux - Organische und organisch-mineralische Düngemittel -

Détermination des éléments spécifiques Bestimmung spezifischer Elemente

This Technical Specification (CEN/TS) was approved by CEN on 13 March 2022 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to

submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS

available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in

parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATIO N
EUROPÄISCHES KOMITEE FÜR NORMUN G
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 17777:2022 E

worldwide for CEN national Members.
---------------------- Page: 3 ----------------------
SIST-TS CEN/TS 17777:2023
CEN/TS 17777:2022 (E)
Contents Page

European foreword ...................................................................................................................................................... 3

Introduction .................................................................................................................................................................... 4

1 Scope .................................................................................................................................................................... 5

2 Normative references .................................................................................................................................... 6

3 Terms and definitions ................................................................................................................................... 7

4 Sampling and sample preparation ........................................................................................................... 7

5 Determination of specific elements ......................................................................................................... 7

5.1 Total phosphorus content............................................................................................................................ 7

5.2 Total potassium content ............................................................................................................................... 7

5.3 Total calcium content .................................................................................................................................... 7

5.4 Total magnesium content ............................................................................................................................ 7

5.5 Total sodium content ..................................................................................................................................... 7

5.6 Total sulphur content .................................................................................................................................... 7

5.7 Inorganic arsenic content ............................................................................................................................ 7

5.8 Cadmium content ............................................................................................................................................ 8

5.9 Total chromium content ............................................................................................................................... 8

5.10 Total mercury content .................................................................................................................................. 8

5.11 Total nickel content ....................................................................................................................................... 8

5.12 Total lead content ........................................................................................................................................... 8

5.13 Total copper content ..................................................................................................................................... 8

5.14 Total zinc content ........................................................................................................................................... 8

5.15 Water-soluble calcium content .................................................................................................................. 8

5.16 Water-soluble magnesium content .......................................................................................................... 8

5.17 Water-soluble sodium content ................................................................................................................... 8

5.18 Water-soluble sulphur content .................................................................................................................. 8

5.19 Water-soluble phosphorus content ......................................................................................................... 8

5.20 Water-soluble potassium content ............................................................................................................. 9

5.21 Neutral ammonium citrate soluble phosphorus content ................................................................. 9

5.22 Formic acid soluble phosphorus content ............................................................................................... 9

5.23 Total boron content ....................................................................................................................................... 9

5.24 Total cobalt content ....................................................................................................................................... 9

5.25 Total iron content ........................................................................................................................................... 9

5.26 Total manganese content ............................................................................................................................. 9

5.27 Total molybdenum content ......................................................................................................................... 9

5.28 Water-soluble boron content ..................................................................................................................... 9

5.29 Water-soluble cobalt content ..................................................................................................................... 9

5.30 Water-soluble copper content ................................................................................................................... 9

5.31 Water-soluble iron content ......................................................................................................................... 9

5.32 Water-soluble manganese content ......................................................................................................... 10

5.33 Water-soluble molybdenum content ..................................................................................................... 10

5.34 Water-soluble zinc content ....................................................................................................................... 10

Bibliography ................................................................................................................................................................. 11

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SIST-TS CEN/TS 17777:2023
CEN/TS 17777:2022 (E)
European foreword

This document (CEN/TS 17777:2022) has been prepared by Technical Committee CEN/TC 260

“Fertilizers and liming materials” the secretariat of which is held by DIN.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. CEN shall not be held responsible for identifying any or all such patent rights.

This document has been prepared under a standardization request given to CEN by the European

Commission and the European Free Trade Association.

Any feedback and questions on this document should be directed to the users’ national standards body.

A complete listing of these bodies can be found on the CEN website.

According to the CEN/CENELEC Internal Regulations, the national standards organisations of the

following countries are bound to announce this Technical Specification: Austria, Belgium, Bulgaria,

Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,

Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of

North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United

Kingdom.
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SIST-TS CEN/TS 17777:2023
CEN/TS 17777:2022 (E)
Introduction

Regulation (EU) 2019/1009 [1] lays down the rules on the making available on the market of EU

fertiliz
...

SLOVENSKI STANDARD
kSIST-TS FprCEN/TS 17777:2021
01-december-2021
Organska in organsko-mineralna gnojila - Določevanje določenih elementov
Organic and organo-mineral fertilizers - Determination of specific elements
Organische und organisch-mineralische Düngemittel - Bestimmung spezifischer
Elemente
Engrais organiques et organo-minéraux - Détermination des éléments spécifiques
Ta slovenski standard je istoveten z: FprCEN/TS 17777
ICS:
65.080 Gnojila Fertilizers
kSIST-TS FprCEN/TS 17777:2021 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
kSIST-TS FprCEN/TS 17777:2021
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kSIST-TS FprCEN/TS 17777:2021
FINAL DRAFT
TECHNICAL SPECIFICATION
FprCEN/TS 17777
SPÉCIFICATION TECHNIQUE
TECHNISCHE SPEZIFIKATION
November 2021
ICS 65.080
English Version
Organic and organo-mineral fertilizers - Determination of
specific elements

Engrais organiques et organo-minéraux - Organische und organisch-mineralische Düngemittel ¿

Détermination des éléments spécifiques Bestimmung spezifischer Elemente

This draft Technical Specification is submitted to CEN members for Vote. It has been drawn up by the Technical Committee

CEN/TC 260.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are

aware and to provide supporting documentation.

Warning : This document is not a Technical Specification. It is distributed for review and comments. It is subject to change

without notice and shall not be referred to as a Technical Specification.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2021 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprCEN/TS 17777:2021 E

worldwide for CEN national Members.
---------------------- Page: 3 ----------------------
kSIST-TS FprCEN/TS 17777:2021
FprCEN/TS 1777:2021 (E)
Contents Page

European foreword ............................................................................................................................................ 3

Introduction .......................................................................................................................................................... 4

1 Scope .......................................................................................................................................................... 5

2 Normative references .......................................................................................................................... 6

3 Terms and definitions ......................................................................................................................... 7

4 Sampling and sample preparation ................................................................................................. 7

5 Determination of specific elements ............................................................................................... 7

5.1 Total phosphorus content.................................................................................................................. 7

5.2 Total potassium content ..................................................................................................................... 7

5.3 Total calcium content .......................................................................................................................... 7

5.4 Total magnesium content .................................................................................................................. 7

5.5 Total sodium content ........................................................................................................................... 7

5.6 Total sulphur content .......................................................................................................................... 7

5.7 Inorganic arsenic content .................................................................................................................. 7

5.8 Cadmium content .................................................................................................................................. 8

5.9 Total chromium content ..................................................................................................................... 8

5.10 Total mercury content ........................................................................................................................ 8

5.11 Total nickel content ............................................................................................................................. 8

5.12 Total lead content ................................................................................................................................. 8

5.13 Total copper content ........................................................................................................................... 8

5.14 Total zinc content ................................................................................................................................. 8

5.15 Water-soluble calcium content ........................................................................................................ 8

5.16 Water-soluble magnesium content ................................................................................................ 8

5.17 Water-soluble sodium content ......................................................................................................... 8

5.18 Water-soluble sulphur content ........................................................................................................ 8

5.19 Water-soluble phosphorus content ............................................................................................... 8

5.20 Water-soluble potassium content ................................................................................................... 9

5.21 Neutral ammonium citrate soluble phosphorus content ....................................................... 9

5.22 Formic acid soluble phosphorus content ..................................................................................... 9

5.23 Total boron content ............................................................................................................................. 9

5.24 Total cobalt content ............................................................................................................................. 9

5.25 Total iron content ................................................................................................................................. 9

5.26 Total manganese content ................................................................................................................... 9

5.27 Total molybdenum content ............................................................................................................... 9

5.28 Water-soluble boron content ........................................................................................................... 9

5.29 Water-soluble cobalt content ........................................................................................................... 9

5.30 Water-soluble copper content ......................................................................................................... 9

5.31 Water-soluble iron content ............................................................................................................... 9

5.32 Water-soluble manganese content ............................................................................................... 10

5.33 Water-soluble molybdenum content ........................................................................................... 10

5.34 Water-soluble zinc content ............................................................................................................. 10

Bibliography ....................................................................................................................................................... 11

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kSIST-TS FprCEN/TS 17777:2021
FprCEN/TS 17777:2021 (E)
European foreword

This document (FprCEN/TS 17777:2021) has been prepared by Technical Committee CEN/TC 260

“Fertilizers and liming materials” the secretariat of which is held by DIN.
This document is currently submitted to the Vote on TS.

This document has been prepared under a standardization request given to CEN by the European

Commission and the European Free Trade Association.
---------------------- Page: 5 ----------------------
kSIST-TS FprCEN/TS 17777:2021
FprCEN/TS 17777:2021 (E)
Introduction

Regulation (EU) 2019/1009 [1] lays down the rules on the making available on the market of EU

fertilizing products and the specific safety and quality requirements for the defined product function

categories (PFCs). Organic and organo-mineral fertilizers have been classified as PFC 1(A) and PFC 1(B).

In this document the normative references of the test methods to be used for organic and organo-mineral

fertilizers are defined in order to measure the compliance with the related requirement in the Regulation

(EU) 2019/1009 [1].
---------------------- Page: 6 ----------------------
kSIST-TS FprCEN/TS 17777:2021
FprCEN/TS 17777:2021 (E)
1 Scope

This document specifies references to the methods for the determination of the following specific

elements in organic and organo-mineral fertilizers:
— Determination of the total phosphorus content;
— Determination of the tot
...

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