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ASTM D1448-05

(Test Method)

Standard Test Method for Micronaire Reading of Cotton Fibers

Standard Test Method for Micronaire Reading of Cotton Fibers

SIGNIFICANCE AND USE
This test method for determining micronaire reading of cotton fibers is considered satisfactory for acceptance testing of commercial shipments when the levels are controlled by use of a full range of calibration cotton standards.
5.1.1 In case of a dispute arising from differences in reported test results when using this test method for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens that are as homogeneous as possible and that are from a lot of material of the type in question. The test specimens should then be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using Student’t-test for unpaired data and an acceptable probability level chosen by the two parties before the testing is begun. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results in the light of the known bias.
The micronaire reading of cotton fibers is a function of both fineness and maturity and is related to mill processing performance and to the quality of the end products. Factors correlated with micronaire reading include cleaning efficiency, neppiness, and the strength and uniformity of the yarn.
Note 2—A modification of this test method is used in commercial trading to select bales which will conform to contract guarantees for specified micronaire readings. For this purpose, it is usual practice to test only one specimen per sample.
SCOPE
1.1 This test method covers the determination of the micronaire reading of loose cotton fibers by measuring the resistance of a plug of cotton fibers to air flow under prescribed conditions. Note 1For other methods for determining the fineness of fibers based on the air-flow principle, refer to Test Method D 1449, Test Method for Specific Area and Immaturity Ratio of Cotton Fibers (Arealometer Method), and to Test Method D 1282, Test Method for Resistance to Air Flow as an Indication of Average Fiber Diameter of Wool Top, Card Sliver, and Scoured Wool.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
28-Feb-2005
ICS
59.060.10 - Natural fibres
Technical Committee
D13 - Textiles
Drafting Committee
D13.11 - Cotton Fibers
Current Stage
Ref Project

Relations

Replaces
ASTM D1448-97 - Standard Test Method for Micronaire Reading of Cotton Fibers
Effective Date
01-Mar-2005
Replaced By
ASTM D1448-11 - Standard Test Method for Micronaire Reading of Cotton Fibers (Withdrawn 2020)
Effective Date
01-Jan-2011
Referred By
ASTM D7139-20 - Standard Terminology for Cotton Fibers
Effective Date
01-Mar-2005
Referred By
ASTM D1441-12(2020) - Standard Practice for Sampling Cotton Fibers for Testing
Effective Date
01-Mar-2005
Referred By
ASTM D3025-07(2021) - Standard Practice for Standardizing Cotton Fiber Test Results by Use of Calibration Cotton Standards
Effective Date
01-Mar-2005
Referred By
ASTM D1282-18 - Standard Test Method for Resistance to Airflow as an Indication of Average Fiber Diameter of Wool Top, Card Sliver, and Scoured Wool
Effective Date
01-Mar-2005

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ASTM D1448-05 - Standard Test Method for Micronaire Reading of Cotton Fibers
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D1448–05
Standard Test Method for
1
Micronaire Reading of Cotton Fibers
This standard is issued under the fixed designation D1448; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 3. Terminology
1.1 This test method covers the determination of the 3.1 For all terminology related to D13.11, refer to Termi-
micronaire reading of loose cotton fibers by measuring the nology D7139.
resistanceofaplugofcottonfiberstoairflowunderprescribed 3.1.1 The following terms are relevant to this standard:
conditions. calibration cotton standards, fineness, micronaire reading.,
3.2 For all other terminology related to textiles, refer to
NOTE 1—Forothermethodsfordeterminingthefinenessoffibersbased
Terminology D123.
on the air-flow principle, refer to Test Method D1449, Test Method for
Specific Area and Immaturity Ratio of Cotton Fibers (Arealometer
4. Summary of Test Method
2
Method), and to Test Method D1282, Test Method for Resistance to Air
Flow as an Indication of Average Fiber Diameter of Wool Top, Card
4.1 The resistance a plug of cotton fibers offers to the flow
Sliver, and Scoured Wool.
of air is measured as an approximate indication of the fineness
of fiber. A predetermined mass of loose cotton fibers is placed
1.2 This standard does not purport to address all of the
in the specimen holder and compressed to a fixed volume. The
safety concerns, if any, associated with its use. It is the
resistance to air flow is measured and expressed as micronaire
responsibility of the user of this standard to establish appro-
reading. Instruments available to measure resistance to air flow
priate safety and health practices and determine the applica-
use compressed air or vacuum and are constructed to measure
bility of regulatory limitations prior to use.
air flow under constant pressure drop across the plug, to
2. Referenced Documents
measure pressure drop when a constant flow of air is main-
2
tained,ortoindicateresistancetoairflowfrombothabalanced
2.1 ASTM Standards:
and unbalanced wheatstone bridge.
D123 Terminology Relating to Textiles
D1282 Test Method for Resistance toAirflow as an Indica-
5. Significance and Use
tion of Average Fiber Diameter of Wool Top, Card Sliver,
5.1 This test method for determining micronaire reading of
and Scoured Wool
cottonfibersisconsideredsatisfactoryforacceptancetestingof
D1441 Practice for Sampling Cotton Fibers for Testing
commercial shipments when the levels are controlled by use of
D1449 Discontinued 1978; Method of Test for Specific
a full range of calibration cotton standards.
Area and Immaturity Ratio of Cotton Fibers (Arealometer
3
5.1.1 In case of a dispute arising from differences in
Method)
reported test results when using this test method for acceptance
D1776 Practice for Conditioning and Testing Textiles
testing of commercial shipments, the purchaser and the sup-
D7139 Terminology for Cotton Fibers
plier should conduct comparative tests to determine if there is
a statistical bias between their laboratories. Competent statis-
1
tical assistance is recommended for the investigation of bias.
This test method is under the jurisdiction ofASTM Committee D13 onTextiles
and is the direct responsibility of Subcommittee D13.11 on Cotton Fibers. As a minimum, the two parties should take a group of test
Current edition approved March 1, 2005. Published April 2005. Originally
specimens that are as homogeneous as possible and that are
approved in 1954 to replace portions of D414. Last previous edition approved in
from a lot of material of the type in question. The test
1997 as D1448–97. DOI: 10.1520/D1448-05.
2
specimens should then be randomly assigned in equal numbers
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
to each laboratory for testing.The average results from the two
Standards volume information, refer to the standard’s Document Summary page on
laboratories should be compared using Student’s t-test for
the ASTM website.
3 unpaireddataandanacceptableprobabilitylevelchosenbythe
Withdrawn. The last approved version of this historical standard is referenced
on www.astm.org. two parties before the testing is begun. If a bias is found, either
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D1448–05
its cause must be found and corrected or the purchaser and the International Calibra
...

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ASTM D2462-22(Test Method)
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5.1 Test Method D2462 for testing for moisture in wool is considered satisfactory for acceptance testing of commercial shipments since current estimates of between-laboratory precision are acceptable.  
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1.3 This test method is not applicable to material known to contain any steam-distillable, water-soluble matter. If it is suspected that such matter is present, the method should be used with caution.  
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ASTM D2525-22(Practice)
Standard Practice for Sampling Wool for Moisture

SIGNIFICANCE AND USE
5.1 This recommended practice furnishes directions for the sampling of wool of the various forms indicated in Section 1, in order that correct probability statements may be made about the relationship between the sample mean and the population mean. If these statements are to be correct, certain conditions, which are stated, must hold.  
5.2 This recommended practice requires that a deliberate act of randomization be performed so that all potential sampling units have approximately the same chance of being taken and no sampling unit is deprived of its chance of being taken.  
5.3 In any case where insufficient information about the variability of the sampling units within the lot is available, directions are given for calculating confidence limits for the sample mean so that a correct probability statement can still be made.
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1.1 This practice covers the design of a sampling plan to be used to obtain samples for the determination of the moisture content of grease wool, scoured wool, carded wool, garnetted wool, wool top and intermediate products, and rovings.  
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ASTM D2130-22(Test Method)
Standard Test Method for Diameter of Wool and Other Animal Fibers by Microprojection

SIGNIFICANCE AND USE
5.1 This test method specifies a sampling and testing procedure for the measurement of average fiber diameter and variation in diameter of animal fibers as required in Test Method D2968.  
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SIGNIFICANCE AND USE
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ASTM D2524-22(Test Method)
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1.1 This test method covers the determination of the breaking tenacity of wool fibers as a flat bundle with a 1/8 in. (3.2 mm) clamp separation.  
1.2 This test method is especially adapted to the fiber bundle clamps and strength testing instruments specified, but may be used on other tensile testing machines when equipped with appropriate adapters to accommodate the prescribed clamps.  
1.3 This test method is applicable to wool in any form which can be hand-combed into small bundles of parallelized fibers.  
Note 1: Other test methods for measuring breaking tenacity of fiber bundles include Test Methods D1294, D1445, and D540.  
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
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ASTM D1576-22(Test Method)
Standard Test Method for Moisture in Wool by Oven-Drying

SIGNIFICANCE AND USE
5.1 Test Method D2462 for the determination of the moisture in wool by distillation with toluene is the preferred method for testing wool for moisture for the acceptance testing of commercial shipments. If, however, the purchaser and the supplier agree, Test Method D1576 for the determination of the moisture in wool by oven drying may be used instead. Comparative tests as directed in 5.1.1, may be advisable.  
5.1.1 In case of a dispute arising from differences in reported test results when using Test Method D1576 for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens which are as homogeneous as possible and which are from a lot of material of the type in question. The test specimens should then be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using Student's t-test for unpaired data and an acceptable probability level chosen by the two parties before testing is begun. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results in the light of the known bias.  
5.2 This test method is a simple and convenient method for routine process control, in-plant evaluation, estimation of moisture content of a lot of wool, or any other purpose for which a high degree of reproducibility is not necessary (see Section 13).
SCOPE
1.1 This test method covers the determination of the amount of moisture present in ordinary commercial and industrial samples of wool in all forms except grease wool, using the oven-drying technique.  
1.2 Formulas for calculating the moisture content (as-received basis) and moisture regain (oven-dried basis) are given. It is always important to use the correct term which corresponds to the basis used in the calculation (see 12.2.1).  
Note 1: The determination of moisture content for textile materials in general is covered in Test Methods D2654, and an optimal method for determining the moisture in wool by distillation with toluene is covered in Test Method D2462. A method for sampling wool for the determination of moisture in wool is covered in Practice D2525. The oven-drying method has been adapted for cotton in Test Method D2495.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D1574-22(Test Method)
Standard Test Method for Extractable Matter in Wool and Other Animal Fibers

SIGNIFICANCE AND USE
5.1 Test Method D1574 is considered satisfactory for acceptance testing since the method has been used extensively in the trade for acceptance testing.  
5.1.1 In case of a dispute arising from differences in reported test results when using Test Method D1574 for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens that are as homogeneous as possible and that are from a lot of material of the type in question. The test specimens should then be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using Student's t-test for unpaired data and an acceptable probability level chosen by the two parties before the testing is begun. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results in the light of the known bias.  
5.2 This test method may be used to estimate the quantity of oil, grease, and waxy materials remaining on or in wool fibers after scouring, or the quantity of lubricant added before carding or remaining after carding, or the quantity of such materials added or removed in subsequent processing operations.  
5.3 The residues obtained in this test may be subjected to chemical analysis for identification and assay of the component materials, if desired.  
5.4 The specified solvent in this test method does not remove some materials, such as soaps, that may be present in wool and hence in some cases may reflect more closely the added content of some extractables in wool such as oils. When such materials are present and an estimate of their quantity is desired, some other solvent or combination of solvents should be used as spec...
SCOPE
1.1 This test method covers the determination of the amount of extractable matter in samples of all forms of wool, except grease wool, that is extractable with a non-flammable vapor degreasing and cleaning solvent.  
1.2 This test method does not cover the determination of the amounts of different components in the extracted matter nor their identification.  
1.3 This test method is suitable for use with other animal fibers.  
Note 1: The determination of extractable matter in yarns and in felts is covered in Test Methods D2257 and D461. For the determination of alcohol-extractable matter in oven-dry scoured wool, refer to Test Methods D584 and D1334.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See 5.4 and Note 3.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D1294-22(Test Method)
Standard Test Method for Tensile Strength and Breaking Tenacity of Wool Fiber Bundles 1-in. (25.4 mm) Gage Length

SIGNIFICANCE AND USE
5.1 Test Method D1294 for the determination of tensile strength may be used for the acceptance testing of commercial shipments of wool, but caution is advised since technicians may fail to get good agreement between results. Comparative tests as directed in 5.1.1 may be advisable.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative test should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative test that are as homogenous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 This test method is useful in studying the relationship between fiber strength and product quality; results should be considered comparative rather than fundamental since the strength found will be lower than the sum of the strengths of the individual fibers present due to slight differences in tensioning.  
5.3 Elongation may be obtained also but the accuracy of elongation measurements is limited and their determination is, therefore, not included as a formal part of this test method.  
5.4 The basic differences between the procedures employed in this test method and those of Test Method D2524 are in the gage lengths employed and the methods of clamping. In Test Method D2524, specific clamps are required whereas in Test Method D1294, any conventional clamps may be used. Results for breaking load determined by Test Method D2524 average 30 % higher than ...
SCOPE
1.1 This test method covers the determination of the breaking force (or load) and estimation of the tensile strength and tenacity of wool fiber bundles with a 1-in. (25.4 mm) gage length. A procedure for preparation of the fiber bundle is included.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. Because the instrument is calibrated in inch-pound units, inch-pound units are shown first, contrary to Committee D13 policy.  
Note 1: For other methods of measuring breaking tenacity of fiber bundles, refer to Test Methods D1445 and D2524.
Note 2: This test method can be used for other fibers that lend themselves to the same kind of preparation but the difference in density must be taken into account when calculating the tensile strength. It is not necessary to know or correct for the density of a fiber when calculating breaking tenacity.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D8394-21(Test Method)
Standard Test Method for Automated Measurement of Maturity, Fineness, Ribbon Width, and Micronaire of Cotton Fibers

SIGNIFICANCE AND USE
5.1 Cotton fiber that is on average finer and more mature is more desirable than coarse or immature fiber, although distinction between these qualities cannot be made quickly and accurately using current test methods. Immature fibers break more easily during processing and have a tendency to form into neps (small entanglements) during processing in the spinning mill. These consequences adversely affect yarn and fabric quality and appearance. Yarn and fabric produced from immature fiber is typically also less lustrous and does not take up dye consistently so yarn and fabric appearance may be different after dyeing.  
5.2 Maturity has a high positive correlation with fiber length and strength but genetic differences and differences in fiber wall thickness caused by plant diseases, soil, and water conditions during the growing season interfere with this relationship.  
5.2.1 Fine fibers are required for fine count yarn manufacture and fiber fineness affects yarn count, evenness and strength. Both fineness and ribbon width are strong genetic traits evident between species and affected by growing conditions within species.  
5.2.2 Micronaire has traditionally been used as a measure of fiber fineness although the value actually measures fiber specific surface area or surface area per unit weight. As a result, micronaire varies concomitantly with both maturity and fineness (see Fig. 2). Maturity and fineness are related to micronaire via Lord’s equation.4
FIG. 2 Relationship Between Micronaire (X), Fineness (H), and Maturity (M)  
5.3 Cottonscope values have been judged against fineness, maturity and ribbon width values produced by examination of thousands of individual, magnified fiber cross-sections. Relationships with equivalent values by these and other older test methods are highly significant5,6 particularly if the number of cross-sections analyzed is high (>3000) and the cross-sections are carefully prepared and measured. Cottonscope measures approximately 20,...
SCOPE
1.1 This test method covers the determination of linear density (gravimetric fineness hereafter stated as fineness), maturity, micronaire, and ribbon width of cotton fibers from a loose, chemically untreated sample taken before harvest, during ginning, during mill processing or unraveled from raw (undyed) yarn or fabric.  
1.2 This test method requires the use of an integrated instrument, for example, the Cottonscope (see Fig. 1), that measures the maturity, fineness, ribbon width, and micronaire of cotton fiber.2
FIG. 1 Cottonscope Instrument
Note 1: For another test method to determine the maturity of cotton fibers, refer to Test Method D1442.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D6961/D6961M-09(2021)(Test Method)
Standard Test Method for Color Measurement of Flax Fiber

SIGNIFICANCE AND USE
5.1 Few standards exist to objectively judge flax quality. Color is an important factor in the quality of flax fiber. Natural variations in raw flax fiber, various processing steps, fiber blending, and a wide range of end uses contribute to the need for a standard method of objectively measuring the color of flax fiber. Spectrophotometic data provide an accurate, precise determination of the color of flax fiber. Colorimetric data are obtained through specimen measurement by combining specimen spectral data with data representing a CIE standard observer and a CIE standard illuminant, as described in Practice E308.  
5.2 If there are differences of practical significance between reported test results for two (or more) laboratories, comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative test that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that fiber sample type must be adjusted in consideration of the known bias.
SCOPE
1.1 This test method covers the instrumental color measurement of flax fiber.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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