iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM E967-03

(Practice)

Standard Practice for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers

Standard Practice for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers

SIGNIFICANCE AND USE
Differential scanning calorimeters and differential thermal analyzers are used to determine the transition temperatures of materials. For this information to be meaningful in an absolute sense, temperature calibration of the apparatus or comparison of the resulting data to that of known standard materials is required.
This test method is useful in calibrating the temperature axis of differential scanning calorimeters and differential thermal analyzers.
SCOPE
1.1 This test method describes the temperature calibration of differential thermal analyzers and differential scanning calorimeters over the temperature range from -40 to +2500°C.
1.2 Computer or electronic based instruments, techniques, or data manipulation equivalent to this test method may also be used.
1.3 SI units are the standard.
1.4 This test method is similar to ISO standard 11357-1.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7.

General Information

Status
Historical
Publication Date
09-Mar-2003
ICS
17.200.10 - Heat. Calorimetry
Technical Committee
E37 - Thermal Measurements
Drafting Committee
E37.01 - Calorimetry and Mass Loss
Current Stage
Ref Project

Relations

Replaces
ASTM E967-97 - Standard Practice for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers
Effective Date
10-Mar-2003
Replaced By
ASTM E967-08 - Standard Practice for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers
Effective Date
01-Sep-2008
Referred By
ASTM D7309-21b - Standard Test Method for Determining Flammability Characteristics of Plastics and Other Solid Materials Using Microscale Combustion Calorimetry
Effective Date
10-Mar-2003
Referred By
ASTM E2009-23 - Standard Test Methods for Oxidation Onset Temperature of Hydrocarbons by Differential Scanning Calorimetry
Effective Date
10-Mar-2003
Referred By
ASTM E2716-23 - Standard Test Method for Determining Specific Heat Capacity by Modulated Temperature Differential Scanning Calorimetry
Effective Date
10-Mar-2003
Referred By
ASTM E3142-18a(2023) - Standard Test Method for Thermal Lag of Thermal Analysis Apparatus
Effective Date
10-Mar-2003
Referred By
ASTM E1582-21 - Standard Test Method for Temperature Calibration of Thermogravimetric Analyzers
Effective Date
10-Mar-2003
Referred By
ASTM F2625-10(2016) - Standard Test Method for Measurement of Enthalpy of Fusion, Percent Crystallinity, and Melting Point of Ultra-High-Molecular Weight Polyethylene by Means of Differential Scanning Calorimetry
Effective Date
10-Mar-2003
Referred By
ASTM D5885/D5885M-20 - Standard Test Method for Oxidative Induction Time of Polyolefin Geosynthetics by High-Pressure Differential Scanning Calorimetry
Effective Date
10-Mar-2003
Referred By
ASTM E2602-22 - Standard Test Methods for Assignment of the Glass Transition Temperature by Modulated Temperature Differential Scanning Calorimetry
Effective Date
10-Mar-2003
Referred By
ASTM F3384-21 - Standard Specification for Polydioxanone Polymer Resins for Surgical Implants
Effective Date
10-Mar-2003
Referred By
ASTM E2890-21 - Standard Test Method for Determination of Kinetic Parameters and Reaction Order for Thermally Unstable Materials by Differential Scanning Calorimetry Using the Kissinger and Farjas Methods
Effective Date
10-Mar-2003
Referred By
ASTM E2070-13(2018) - Standard Test Methods for Kinetic Parameters by Differential Scanning Calorimetry Using Isothermal Methods
Effective Date
10-Mar-2003
Referred By
ASTM E928-19 - Standard Test Method for Purity by Differential Scanning Calorimetry
Effective Date
10-Mar-2003
Referred By
ASTM F2150-19 - Standard Guide for Characterization and Testing of Biomaterial Scaffolds Used in Regenerative Medicine and Tissue-Engineered Medical Products
Effective Date
10-Mar-2003

Buy Standard

ASTM E967-03 - Standard Practice for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal AnalyzersASTM E967-03 - Standard Practice for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers
PreviousNext
Standard
ASTM E967-03 - Standard Practice for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers
English language
4 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:E967–03
Standard Test Method for
Temperature Calibration of Differential Scanning
1
Calorimeters and Differential Thermal Analyzers
This standard is issued under the fixed designation E967; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Summary of Test Method
1.1 This test method describes the temperature calibration 4.1 This test method consists of heating the calibration
of differential thermal analyzers and differential scanning materials at a controlled rate in a controlled atmosphere
calorimeters over the temperature range from−40 to+2500°C. through a region of known thermal transition. The heat flow
1.2 Computer or electronic based instruments, techniques, into the calibration material or the difference of temperature
ordatamanipulationequivalenttothistestmethodmayalsobe between the calibration material and a reference sample and a
used. reference material is monitored and continuously recorded. A
1.3 SI units are the standard. transition is marked by the absorption of energy by the
1.4 This test method is similar to ISO standard 11357–1. specimenresultinginacorrespondingendothermicpeakinthe
1.5 This standard does not purport to address all of the heating curve.
safety concerns, if any, associated with its use. It is the
NOTE 1—Heat flow calibrations are sometimes determined in conjunc-
responsibility of the user of this standard to establish appro-
tion with temperature calibration. Some differential scanning calorimeters
priate safety and health practices and determine the applica-
permitbothheatflowandtemperaturecalibrationstobeobtainedfromthe
bility of regulatory limitations prior to use. Specific precau-
same experimental procedure.
tionary statements are given in Section 7.
5. Significance and Use
2. Referenced Documents
5.1 Differential scanning calorimeters and differential ther-
2.1 ASTM Standards: malanalyzersareusedtodeterminethetransitiontemperatures
2
E473 Terminology Relating to Thermal Analysis of materials. For this information to be meaningful in an
E968 Practice for Heat Flow Calibration of Differential absolute sense, temperature calibration of the apparatus or
2
Scanning Calorimeters comparison of the resulting data to that of known standard
E1142 Terminology Relating to Thermophysical Proper- materials is required.
2
ties 5.2 This test method is useful in calibrating the temperature
E1953 Practice for Description of ThermalAnalysisAppa- axis of differential scanning calorimeters and differential ther-
3
ratus mal analyzers.
2.2 ISO Standard:
6. Apparatus
11357–1 Plastics-Differential Scanning Calorimetry (DSC)-
Part 1: General Principles 6.1 Apparatus shall be of either type listed below:
6.1.1 Differential Scanning Calorimeter (DSC), capable of
3. Terminology
heatingatestspecimenandareferencematerialatacontrolled
3.1 Specific technical terms used in this test method are rate and of automatically recording the differential heat flow
defined in Terminologies E473 and E1142. between the sample and the reference material to the required
sensitivity and precision.
6.1.1.1 A Furnace(s), to provide uniform controlled heating
1
ThistestmethodisunderthejurisdictionofASTMCommitteeE37onThermal
or cooling of a specimen and reference to a constant tempera-
Measurements and is the direct responsibility of Subcommittee E37.01 on Test
ture or at a constant rate within the applicable temperature
Methods and Practices.
Current edition approved March 10, 2003. PublishedApril 20038. Originallyap-
range of this test method.
proved in 1983. Last previous edition approved in 1997 as E967–97.
6.1.1.2 A Temperature Sensor, to provide an indication of
2
Annual Book of ASTM Standards, Vol 14.02.
3 the specimen temperature.
Available form American National Standards Institute, 11 W. 42nd St., 13th
Floor, New York, NY 10036.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
E967–03
TABLE 1 Melting Temperature of Calibration Material
6.1.1.3 Differential sensors, to detect a heat flow (power)
difference between the specimen and reference.
NOTE 1—The values in Table 1 were determined under special, highly
6.1.1.4 Test Chamber Environment—a means of sustaining
accurate steady state conditions that are not attainable or applicable to
atestchamberenvironmentofnitrogenorotherinertpurgegas thermal analysis techniques. The actual precision of this test method is
given in Section 12 of this test method.
at a purge rate of 10 to 50 mL/min.
A
6.1.1.5 A Temperature Control
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM E473-23b(Terminology)
Standard Terminology Relating to Thermal Analysis and Rheology

SCOPE
1.1 This terminology is a compilation of definitions of terms used in ASTM documents relating to thermal analysis and rheology. This terminology includes only those terms for which ASTM either has standards or is contemplating some action. It is not intended to be an all-inclusive listing of terms related to thermal analysis and rheology.  
1.2 This terminology specifically supports the single-word form for terms using thermo as a prefix, such as thermoanalytical or thermomagnetometry, while recognizing that for some terms a two-word form can be used, such as thermal analysis. This terminology does not support, nor does it recommend, use of the grammatically incorrect, single-word form using thermal as a prefix, such as, thermalanalytical or thermalmagnetometry.  
1.3 A definition is a single sentence with additional information included in a Discussion area. It is reviewed every five years.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    4 pages
    English language
    sale 15% off
  • Standard
    4 pages
    English language
    sale 15% off
ASTM
ASTM E2070-23(Test Method)
Standard Test Methods for Kinetic Parameters by Differential Scanning Calorimetry Using Isothermal Methods

SIGNIFICANCE AND USE
6.1 These test methods are useful for research and development, quality assurance, regulatory compliance, and specification acceptance purposes.  
6.2 The determination of the order of a chemical reaction or transformation at specific temperatures or time conditions is beyond the scope of these test methods.  
6.3 The activation energy results obtained by these test methods may be compared with those obtained from Test Method E698 for nth order and accelerating reactions. Activation energy, pre-exponential factor, and reaction order results by these test methods may be compared to those for Test Method E2041 for nth order reactions.
SCOPE
1.1 Test Methods A, B, and C determine kinetic parameters for activation energy, pre-exponential factor and reaction order using differential scanning calorimetry (DSC) from a series of isothermal experiments over a small (≈10 K) temperature range. Test Method A is applicable to low nth order reactions. Test Methods B and C are applicable to accelerating reactions such as thermoset curing or pyrotechnic reactions and crystallization transformations in the temperature range from 300 K to 900 K (nominally 30 °C to 630 °C). These test methods are applicable only to these types of exothermic reactions when the thermal curves do not exhibit shoulders, double peaks, discontinuities or shifts in baseline.  
1.2 Test Methods D and E also determines the activation energy of a set of time-to-event and isothermal temperature data generated by this or other procedures  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    12 pages
    English language
    sale 15% off
  • Standard
    12 pages
    English language
    sale 15% off
ASTM
ASTM E1142-23b(Terminology)
Standard Terminology Relating to Thermophysical Properties

SCOPE
1.1 This is a compilation of only those terms and corresponding definitions included in or being considered for inclusion in ASTM documents relating to thermophysical properties. It is not intended as an all-inclusive listing of thermophysical property terms. Terms that are generally understood or defined adequately in other readily available sources are not included.  
1.2 A definition is a single sentence with additional information included in a Discussion.  
1.3 Definitions of terms specific to a particular field (such as dynamic mechanical measurements) are identified with an italicized introductory phrase.  
1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM E1356-23(Test Method)
Standard Test Method for Assignment of the Glass Transition Temperatures by Differential Scanning Calorimetry

SIGNIFICANCE AND USE
5.1 Differential scanning calorimetry provides a rapid test method for determining changes in specific heat capacity in a homogeneous material. The glass transition is manifested as a step change in specific heat capacity. For amorphous and semicrystalline materials the determination of the glass transition temperature may lead to important information about their thermal history, processing conditions, stability, progress of chemical reactions, and mechanical and electrical behavior.  
5.2 This test method is useful for research, quality control, and specification acceptance.
SCOPE
1.1 This test method covers the assignment of the glass transition temperatures of materials using differential scanning calorimetry or differential thermal analysis.  
1.2 This test method is applicable to amorphous materials or to partially crystalline materials containing amorphous regions, that are stable and do not undergo decomposition or sublimation in the glass transition region.  
1.3 The normal operating temperature range is from −120 °C to 500 °C. The temperature range may be extended, depending upon the instrumentation used.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 ISO standards 11357–2 is equivalent to this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    4 pages
    English language
    sale 15% off
ASTM
ASTM E2603-15(2023)(Practice)
Standard Practice for Calibration of Fixed-Cell Differential Scanning Calorimeters

SIGNIFICANCE AND USE
5.1 Fixed-cell differential scanning calorimeters are used to determine the transition temperatures and energetics of materials in solution. For this information to be accepted with confidence in an absolute sense, temperature and heat calibration of the apparatus or comparison of the resulting data to that of known standard materials is required.  
5.2 This practice is useful in calibrating the temperature and heat flow axes of fixed-cell differential scanning calorimeters.
SCOPE
1.1 This practice covers the calibration of fixed-cell differential scanning calorimeters over the temperature range from –10 °C to +120 °C.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    5 pages
    English language
    sale 15% off
ASTM
ASTM E2041-23(Test Method)
Standard Test Method for Estimating Kinetic Parameters by Differential Scanning Calorimeter Using the Borchardt and Daniels Method

SIGNIFICANCE AND USE
6.1 This test method is useful in research and development.  
6.2 The determination of the appropriate model for a chemical reaction or transformation and the values associated with its kinetic parameters may be used in the estimation of reaction performance at temperatures or time conditions not easily tested. This use, however, is not described in this test method.
SCOPE
1.1 This test method describes the determination of the kinetic parameters of activation energy, Arrhenius pre-exponential factor, and reaction order using the Borchardt and Daniels2 treatment of data obtained by differential scanning calorimetry. This test method is applicable to the temperature range from 170 K to 870 K (−100 °C to 600°C).  
1.2 This treatment is applicable only to smooth exothermic reactions with no shoulders, discontinuous changes, or shifts in baseline. It is applicable only to reactions with reaction order n ≤ 2. It is not applicable to acceleratory reactions and, therefore, is not applicable to the determination of kinetic parameters for most thermoset curing reactions or to crystallization reactions.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    9 pages
    English language
    sale 15% off
  • Standard
    9 pages
    English language
    sale 15% off
ASTM
ASTM E1952-23(Test Method)
Standard Test Method for Thermal Conductivity and Thermal Diffusivity by Modulated Temperature Differential Scanning Calorimetry

SIGNIFICANCE AND USE
5.1 Thermal conductivity is a useful design parameter for the rate of heat transfer through a material.  
5.2 The results of this test method may be used for design purposes, service evaluation, manufacturing control, research and development, and hazard evaluation. (See Practice E1231.)
SCOPE
1.1 This test method describes the determination of thermal conductivity of homogeneous, non-porous solid materials in the range of 0.10 W/(K·m) to 1.0 W/(K·m) by modulated temperature differential scanning calorimeter. This range includes many polymeric, glass, and ceramic materials. Thermal diffusivity, which is related to thermal conductivity through specific heat capacity and density, may also be derived. Thermal conductivity and diffusivity can be determined at one or more temperatures over the range of 0 °C to 90 °C.  
1.2 The values stated in SI units are to be regarded as standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM E1970-23(Practice)
Standard Practice for Statistical Treatment of Thermoanalytical Data

SIGNIFICANCE AND USE
5.1 The standard deviation, or one of its derivatives, such as relative standard deviation or pooled standard deviation, derived from this practice, provides an estimate of precision in a measured value. Such results are ordinarily expressed as the mean value ± the standard deviation, that is, X ± s.  
5.2 If the measured values are, in the statistical sense, “normally” distributed about their mean, then the meaning of the standard deviation is that there is a 67 % chance, that is 2 in 3, that a given value will lie within the range of ± one standard deviation of the mean value. Similarly, there is a 95 % chance, that is 19 in 20, that a given value will lie within the range of ± two standard deviations of the mean. The two standard deviation range is sometimes used as a test for outlying measurements.  
5.3 The calculation of precision in the slope and intercept of a line, derived from experimental data, commonly is required in the determination of kinetic parameters, vapor pressure or enthalpy of vaporization. This practice describes how to obtain these and other statistically derived values associated with measurements by thermal analysis.
SCOPE
1.1 This practice details the statistical data treatment used in some thermal analysis methods.  
1.2 The method describes the commonly encountered statistical tools of the mean, standard derivation, relative standard deviation, pooled standard deviation, pooled relative standard deviation, the best fit to a (linear regression of a) straight line (or plane), and propagation of uncertainties for all calculations encountered in thermal analysis methods (see Practice E2586).  
1.3 Some thermal analysis methods derive the analytical value from the slope or intercept of a linear regression straight line (or plane) assigned to three or more sets of data pairs. Such methods may require an estimation of the precision in the determined slope or intercept. The determination of this precision is not a common statistical tool. This practice details the process for obtaining such information about precision.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    5 pages
    English language
    sale 15% off
  • Standard
    5 pages
    English language
    sale 15% off
ASTM
ASTM E2009-23(Test Method)
Standard Test Methods for Oxidation Onset Temperature of Hydrocarbons by Differential Scanning Calorimetry

SIGNIFICANCE AND USE
5.1 Oxidation onset temperature is a relative measure of the degree of oxidative stability of the material evaluated at a given heating rate and oxidative environment (e.g., oxygen); the higher the OOT value the more stable the material. The OOT is described in Fig. 1. The OOT values can be used for comparative purposes and are not an absolute measurement, like the oxidation induction time (OIT) at a constant temperature (see Test Method E1858). The presence or effectiveness of antioxidants may be determined by these test methods.
FIG. 1 DSC Oxidation (Extrapolated) Onset Temperature (OOT)  
5.2 Typical uses of these test methods include the oxidative stability of edible oils and fats (oxidative rancidity), lubricants, greases, and polyolefins.
SCOPE
1.1 These test methods describe the determination of the oxidative properties of hydrocarbons by differential scanning calorimetry or pressure differential scanning calorimetry under linear heating rate conditions and are applicable to hydrocarbons, which oxidize exothermically in their analyzed form.  
1.2 Test Method A—A differential scanning calorimeter (DSC) is used at ambient pressure of one atmosphere of oxygen.  
1.3 Test Method B—A pressure DSC (PDSC) is used at high pressure (e.g., 3.5 MPa (500 psig) of oxygen).  
1.4 Test Method C—A differential scanning calorimeter (DSC) is used at ambient pressure of one atmosphere of air.  
1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    6 pages
    English language
    sale 15% off
  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM E2716-23(Test Method)
Standard Test Method for Determining Specific Heat Capacity by Modulated Temperature Differential Scanning Calorimetry

SIGNIFICANCE AND USE
5.1 Modulated temperature differential scanning calorimetric measurements provide a rapid, simple method for determining specific heat capacities of materials, even under quasi-isothermal conditions.  
5.2 Specific heat capacities are important for design purposes, quality control, and research and development.  
5.3 The use of a stepped quasi-isothermal program may be used to follow structure changes in materials.
SCOPE
1.1 This test method describes the determination of specific heat capacity by modulated temperature differential scanning calorimetry. For the determination of specific heat capacity by a step-isothermal or multiple step-isothermal temperature program, the reader is referred to Test Method E1269.  
1.2 This test method is generally applicable to thermally stable solids and liquids.  
1.3 The normal operating range of the test is from (–100 to 600) °C. The temperature range may be extended depending upon the instrumentation and specimen holders used.  
1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    4 pages
    English language
    sale 15% off
  • Standard
    4 pages
    English language
    sale 15% off