Standard Test Method for Examination and Analysis of Hardened Masonry Mortar

SIGNIFICANCE AND USE
This test method provides procedures for petrographic examination and chemical analysis of mortar for components of masonry mortar. These components may include portland cement, hydrated calcitic or dolomitic lime, masonry cement, aggregates, and air.
The test method consists of procedures and sub-procedures, each requiring a substantial degree of petrographic and chemical skills and relatively elaborate instrumentation.
The chemical data considered together with results of petrographic examination of a mortar provide for calculation of component proportions and thus allow a determination of mortar composition as represented by Types M, N, S, and O in Table 1 (Proportion Specification Requirements) of Specification C 270.
Failure of a mortar to have the composition of any type as defined in Table 1 of Specification C 270 does not necessarily mean that the mortar does not meet the requirements of Specification C 270. The mortar may meet the alternative requirements of Table 2 (Property Specification Requirements) of Specification C 270.
The maleic acid method of analysis is not applicable for the analysis of mortar because it is greatly influenced by carbonation and does not provide for the determination of calcium.
SCOPE
1.1 This test method covers procedures for petrographic examination and chemical analysis of samples of masonry mortars. Based upon such examination and analysis, proportions of components in masonry mortars can be determined.
Note 1—This method is also applicable to hydraulic cement-based stucco and plaster. Some historic mortars may contain non-resolvable constituents that may interfere. However, significant information may be obtained by petrographic examinations.
1.2 Interpretations and calculations of chemical results are dependent upon results of the petrographic examination. The use of the chemical results alone is contrary to the requirements of this test method.
1.3 Procedures for sampling, petrographic examination, chemical analysis, and calculations of component proportions are given in the following sections:SectionSampling7Petrographic examination8Chemical analysis9Mortar proportion calculations10Report11
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
30-Nov-2005
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ASTM C1324-05 - Standard Test Method for Examination and Analysis of Hardened Masonry Mortar
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:C1324–05
Standard Test Method for
1
Examination and Analysis of Hardened Masonry Mortar
This standard is issued under the fixed designation C1324; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* C114 Test Methods for Chemical Analysis of Hydraulic
Cement
1.1 This test method covers procedures for petrographic
C125 Terminology Relating to Concrete and Concrete Ag-
examination and chemical analysis of samples of masonry
gregates
mortars. Based upon such examination and analysis, propor-
C144 Specification for Aggregate for Masonry Mortar
tions of components in masonry mortars can be determined.
C270 Specification for Mortar for Unit Masonry
NOTE 1—This method is also applicable to hydraulic cement-based
C295 Guide for Petrographic Examination of Aggregates
stucco and plaster. Some historic mortars may contain non-resolvable
for Concrete
constituents that may interfere. However, significant information may be
C457 Test Method for Microscopical Determination of
obtained by petrographic examinations.
Parameters of the Air-Void System in Hardened Concrete
1.2 Interpretations and calculations of chemical results are
C823 Practice for Examination and Sampling of Hardened
dependent upon results of the petrographic examination. The
Concrete in Constructions
useofthechemicalresultsaloneiscontrarytotherequirements
C856 Practice for Petrographic Examination of Hardened
of this test method.
Concrete
1.3 Procedures for sampling, petrographic examination,
C1084 Test Method for Portland-Cement Content of Hard-
chemical analysis, and calculations of component proportions
ened Hydraulic-Cement Concrete
are given in the following sections:
D1193 Specification for Reagent Water
Section
Sampling 7
3. Terminology
Petrographic examination 8
Chemical analysis 9
3.1 Terms used in this test method are defined in Terminol-
Mortar proportion calculations 10
ogy C125 or the other referenced ASTM standards.
Report 11
4. Significance and Use
1.4 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information
4.1 This test method provides procedures for petrographic
only.
examination and chemical analysis of mortar for components
1.5 This standard does not purport to address all of the
of masonry mortar. These components may include portland
safety concerns, if any, associated with its use. It is the
cement, hydrated calcitic or dolomitic lime, masonry cement,
responsibility of the user of this standard to establish appro-
aggregates, and air.
priate safety and health practices and determine the applica-
4.2 The test method consists of procedures and sub-
bility of regulatory limitations prior to use.
procedures, each requiring a substantial degree of petrographic
and chemical skills and relatively elaborate instrumentation.
2. Referenced Documents
4.3 The chemical data considered together with results of
2
2.1 ASTM Standards:
petrographicexaminationofamortarprovideforcalculationof
component proportions and thus allow a determination of
mortar composition as represented by Types M, N, S, and O in
1
This test method is under the jurisdiction ofASTM Committee C12 on Mortars
Table 1 (Proportion Specification Requirements) of Specifica-
for Unit Masonry and is the direct responsibility of Subcommittee C12.02 on
tion C270.
Research and Methods of Test.
4.4 Failure of a mortar to have the composition of any type
Current edition approved Dec. 1, 2005. Published December 2005. Originally
as defined in Table 1 of Specification C270 does not necessar-
approved in 2002. Last previous edition approved in 2004 as C1324 – 04. DOI:
10.1520/C1324-05.
ily mean that the mortar does not meet the requirements of
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Specification C270. The mortar may meet the alternative
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
requirements of Table 2 (Property Specification Requirements)
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. of Specification C270.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

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C1324–05
4.5 The maleic acid method of analysis is not applicable for 6.3.4 Water—All references to water shall be understood to
the analysis of mortar because it is greatly influenced by mean reagent water Type I through IV of Specification D1193.
carbonation and
...

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