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ASTM E396-12e1

(Test Method)

Standard Test Methods for Chemical Analysis of Cadmium

Standard Test Methods for Chemical Analysis of Cadmium

SIGNIFICANCE AND USE
These test methods for the chemical analysis of cadmium are primarily intended to test such material for compliance with compositional specifications in Specification B440. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
SCOPE
1.1 These test methods cover the chemical analysis of cadmium having chemical compositions with the following limits:
ElementComposition, max, %   Antimony0.001 Arsenic0.003 Copper0.015 Lead0.025 Silver0.010 Thallium0.003 Tin0.010 Zinc0.035
1.2 The test methods appear in the following order:
Sections Antimony by the Rhodamine B Spectrophotometric Method
[0.0002 % to 0.0010 %]62-72 Arsenic by the Molybdenum Blue Spectrophotometric Method
[0.001 % to 0.005 %]40-50 Copper by the Neocuproine Spectrophotometric Method [0.002 % to 0.030 %] 10-19 Copper, Lead, Silver, and Zinc by the Atomic Absorption Method [0.004 % to 0.02 % Cu, 0.01 % to 0.05 % Pb, 0.004 % to 0.02 % Ag
and 0.01 % to 0.05 % Zn]51-61 Lead by the Dithizone Spectrophotometric Method [0.001 % to 0.05 %]20-29 Thallium by the Rhodamine B Spectrophotometric Method
[0.0003 % to 0.005%]30-39 Tin by the 8-Quinolinol Spectrophotometric Method [0.0025 % to 0.0150 %]73-82
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary information is given in Section 6, 25.8, 35.2, and 35.3.

General Information

Status
Historical
Publication Date
26-Jan-2012
ICS
71.040.40 - Chemical analysis
77.040.30 - Chemical analysis of metals
Technical Committee
E01 - Analytical Chemistry for Metals, Ores, and Related Materials
Drafting Committee
E01.05 - Cu, Pb, Zn, Cd, Sn, Be, Precious Metals, their Alloys, and Related Metals
Current Stage
Ref Project

Relations

Replaces
ASTM E396-12 - Standard Test Methods for Chemical Analysis of Cadmium
Effective Date
27-Jan-2012
Replaced By
ASTM E396-17 - Standard Test Methods for Chemical Analysis of Cadmium
Effective Date
15-Dec-2017
Referred By
ASTM B440-12(2021) - Standard Specification for Cadmium
Effective Date
27-Jan-2012
Referred By
ASTM B816-00(2021) - Standard Specification for Coatings of Cadmium-Zinc Mechanically Deposited
Effective Date
27-Jan-2012
Referred By
ASTM B635-00(2023) - Standard Specification for Coatings of Cadmium-Tin Mechanically Deposited
Effective Date
27-Jan-2012
Referred By
ASTM B699-86(2021)e1 - Standard Specification for Coatings of Cadmium Vacuum-Deposited on Iron and Steel
Effective Date
27-Jan-2012

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ASTM E396-12e1 - Standard Test Methods for Chemical Analysis of CadmiumASTM E396-12e1 - Standard Test Methods for Chemical Analysis of Cadmium
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ASTM E396-12e1 - Standard Test Methods for Chemical Analysis of Cadmium
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation: E396 − 12
Standard Test Methods for
1
Chemical Analysis of Cadmium
This standard is issued under the fixed designation E396; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—Editorial corrections were made throughout in August 2012.
1. Scope 2. Referenced Documents
2
1.1 These test methods cover the chemical analysis of 2.1 ASTM Standards:
cadmium having chemical compositions with the following B440 Specification for Cadmium
limits: D1193 Specification for Reagent Water
E29 Practice for Using Significant Digits in Test Data to
Element Composition, max, %
Determine Conformance with Specifications
Antimony 0.001
E50 Practices for Apparatus, Reagents, and Safety Consid-
Arsenic 0.003
erations for Chemical Analysis of Metals, Ores, and
Copper 0.015
Lead 0.025
Related Materials
Silver 0.010
E55 Practice for Sampling Wrought Nonferrous Metals and
Thallium 0.003
Alloys for Determination of Chemical Composition
Tin 0.010
Zinc 0.035
E60 Practice for Analysis of Metals, Ores, and Related
Materials by Spectrophotometry
1.2 The test methods appear in the following order:
E88 Practice for Sampling Nonferrous Metals and Alloys in
Sections
Antimony by the Rhodamine B Spectrophotometric Method 62-72 Cast Form for Determination of Chemical Composition
[0.0002 % to 0.0010 %]
E135 Terminology Relating to Analytical Chemistry for
Arsenic by the Molybdenum Blue Spectrophotometric Method 40-50
Metals, Ores, and Related Materials
[0.001 % to 0.005 %]
Copper by the Neocuproine Spectrophotometric Method [0.002 % to 10-19 E173 Practice for Conducting Interlaboratory Studies of
0.030 %]
Methods for Chemical Analysis of Metals (Withdrawn
Copper, Lead, Silver, and Zinc by the Atomic Absorption Method 51-61
3
1998)
[0.004 % to 0.02 % Cu, 0.01 % to 0.05 % Pb, 0.004 % to 0.02 % Ag
and 0.01 % to 0.05 % Zn] E1601 Practice for Conducting an Interlaboratory Study to
Lead by the Dithizone Spectrophotometric Method [0.001 % to 20-29
Evaluate the Performance of an Analytical Method
0.05 %]
Thallium by the Rhodamine B Spectrophotometric Method 30-39
3. Terminology
[0.0003 % to 0.005%]
Tin by the 8-Quinolinol Spectrophotometric Method [0.0025 % to 73-82
3.1 For definitions of terms used in this test method, refer to
0.0150 %]
Terminology E135.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
4. Significance and Use
responsibility of the user of this standard to establish appro-
4.1 These test methods for the chemical analysis of cad-
priate safety and health practices and determine the applica-
mium are primarily intended to test such material for compli-
bility of regulatory limitations prior to use. Specific precau-
ance with compositional specifications in Specification B440.
tionary information is given in Section 6, 25.8, 35.2, and 35.3.
Itisassumedthatallwhousethesetestmethodswillbetrained
analysts capable of performing common laboratory procedures
1
These test methods are under the jurisdiction of ASTM Committee E01 on
2
Analytical Chemistry for Metals, Ores, and Related Materials and are the direct
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
responsibility of Subcommittee E01.05 on Cu, Pb, Zn, Cd, Sn, Be, theirAlloys, and contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Related Metals. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved Jan. 27, 2012. Published February 2012. Originally the ASTM website.
3
approvedin1970.Lastpreviouseditionapprovedin2011asE396 – 05(2011).DOI: The last approved version of this historical standard is referenced on
10.1520/E0396-12. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
´1
E396 − 12
skillfully and safely. It is expected that work will be performed 14. Interferences
in a properly equipped laboratory.
14.1 The elements ordinarily present do not interfere if their
contents are under the maximum limits shown in 1.1.
5. Apparatus, Reagents, and Spectrophotometric Practice
5.1 Apparatus and reagents required for each determination
15. Reagents
are listed in separate sections preceding the procedure. The
15.1 Chloroform (CHCl ).
3
apparatus,standardsolutions,andreagentsshallconformtothe
requirements prescribed in Practices E50. Spectrophotometers 15.2 Copper, Standard Solution (1 mL = 0.01 mg Cu)—
shall conform to the requirements prescribed in Practice E60. Dissolve 0.100
...

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SIGNIFICANCE AND USE
4.1 These test methods for the chemical analysis of cadmium are primarily intended to test such material for compliance with compositional specifications in Specification B440. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
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1.1 These test methods cover the chemical analysis of cadmium having chemical compositions with the following limits:    
Element  
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Antimony  
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1.2 The test methods appear in the following order:    
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Antimony by the Rhodamine B Spectrophotometric Method
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62 – 72  
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Standard Test Methods for Chemical Analysis of Cadmium

SIGNIFICANCE AND USE
4.1 These test methods for the chemical analysis of cadmium are primarily intended to test such material for compliance with compositional specifications in Specification B440. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
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1.1 These test methods cover the chemical analysis of cadmium having chemical compositions with the following limits:    
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1.2 The test methods appear in the following order:    
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Antimony by the Rhodamine B Spectrophotometric Method
[0.0002 % to 0.0010 %]  
62 – 72  
Arsenic by the Molybdenum Blue Spectrophotometric Method
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