Standard Test Method for Insoluble Residue in Carbonate Aggregates

SIGNIFICANCE AND USE
3.1 The amount and size distribution of noncarbonate (insoluble) material in carbonate aggregates is of interest to those conducting research on the polish susceptibility of stone used in pavements or on the friction properties of pavement surfaces. In addition, some agencies utilize the test for acceptance purposes to delineate carbonate aggregates that polish excessively and become slippery and those that will not.
Note 1: The quality of the results produced by this standard are dependent upon the competence of the personnel performing the procedure and the capability, calibration, and the maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing/sampling/inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors: following the suggestions of Specification D3666 or similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers determination of the percentage of insoluble residue in carbonate aggregates using hydrochloric acid solution to react the carbonates.  
1.2 The values stated in SI units are to be regarded as standard. Regarding sieves, per Specification E11, “The values stated in SI units shall be considered standard for the dimensions of the wire cloth openings and the diameter of the wires used in the wire cloth. The values stated in inch-pound units shall be considered standard with regard to the sieve frames.” When sieve mesh sizes are referenced, the alternate inch-pound designations are provided for information purposes and enclosed in parentheses.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precaution statements are given in Section 7.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Publication Date
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D3042 − 17
Standard Test Method for
1
Insoluble Residue in Carbonate Aggregates
This standard is issued under the fixed designation D3042; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope C294 Descriptive Nomenclature for Constituents of Con-
crete Aggregates
1.1 This test method covers determination of the percentage
C670 Practice for Preparing Precision and Bias Statements
ofinsolubleresidueincarbonateaggregatesusinghydrochloric
for Test Methods for Construction Materials
acid solution to react the carbonates.
D3666 Specification for Minimum Requirements for Agen-
1.2 The values stated in SI units are to be regarded as
cies Testing and Inspecting Road and Paving Materials
standard. Regarding sieves, per Specification E11, “The values
D4753 Guide for Evaluating, Selecting, and Specifying Bal-
stated in SI units shall be considered standard for the dimen-
ances and Standard Masses for Use in Soil, Rock, and
sions of the wire cloth openings and the diameter of the wires
Construction Materials Testing
used in the wire cloth. The values stated in inch-pound units
E11 Specification for Woven Wire Test Sieve Cloth and Test
shall be considered standard with regard to the sieve frames.”
Sieves
Whensievemeshsizesarereferenced,thealternateinch-pound
3. Significance and Use
designations are provided for information purposes and en-
closed in parentheses.
3.1 The amount and size distribution of noncarbonate (in-
soluble) material in carbonate aggregates is of interest to those
1.3 The text of this standard references notes and footnotes
conducting research on the polish susceptibility of stone used
which provide explanatory material. These notes and footnotes
in pavements or on the friction properties of pavement sur-
(excluding those in tables and figures) shall not be considered
faces. In addition, some agencies utilize the test for acceptance
as requirements of the standard.
purposes to delineate carbonate aggregates that polish exces-
1.4 This standard does not purport to address all of the
sively and become slippery and those that will not.
safety concerns, if any, associated with its use. It is the
NOTE 1—The quality of the results produced by this standard are
responsibility of the user of this standard to establish appro-
dependent upon the competence of the personnel performing the proce-
priate safety and health practices and determine the applica-
dure and the capability, calibration, and the maintenance of the equipment
bility of regulatory limitations prior to use. Specific precaution
used.Agencies that meet the criteria of Specification D3666 are generally
statements are given in Section 7.
considered capable of competent and objective testing/sampling/
1.5 This international standard was developed in accor-
inspection, etc. Users of this standard are cautioned that compliance with
Specification D3666 alone does not completely ensure reliable results.
dance with internationally recognized principles on standard-
Reliable results depend on many factors: following the suggestions of
ization established in the Decision on Principles for the
Specification D3666 or similar acceptable guideline provides a means of
Development of International Standards, Guides and Recom-
evaluating and controlling some of those factors.
mendations issued by the World Trade Organization Technical
4. Apparatus
Barriers to Trade (TBT) Committee.
4.1 Sieves, U.S. standard 8-in. diameter, conforming to
2. Referenced Documents
Specification E11 in the following sizes:
2
2.1 ASTM Standards:
3
9.5-mm ( ⁄8-in.)
C136 Test Method for Sieve Analysis of Fine and Coarse
4.75-mm (No. 4)
2.36-mm (No. 8)
Aggregates
1.18-mm (No. 16)
600-µm (No. 30)
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
300-µm (No. 50)
and Paving Materials and is the direct responsibility of Subcommittee D04.51 on
150-µm (No. 100)
Aggregate Tests. 75-µm (No. 200)
Current edition approved April 1, 2017. Published April 2017. Originally
4.2 Balance—A balance having a minimum capacity of
approved in 1972. Last previous edition approved in 2015 as D3042 – 09 (2015).
15 kg and meeting the requirements of Guide D4753, Class
DOI: 10.1520/D3042-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
GP5.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4.3 Oven, of appropriate size capable of being maintained at
Standards volume
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D3042 − 09 (Reapproved 2015) D3042 − 17
Standard Test Method for
1
Insoluble Residue in Carbonate Aggregates
This standard is issued under the fixed designation D3042; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers determination of the percentage of insoluble residue in carbonate aggregates using hydrochloric acid
solution to react the carbonates.
1.2 The values stated in SI units are to be regarded as standard. Regarding sieves, per Specification E11, “The values stated in
SI units shall be considered standard for the dimensions of the wire cloth openings and the diameter of the wires used in the wire
cloth. The values stated in inch-pound units shall be considered standard with regard to the sieve frames.” When sieve mesh sizes
are referenced, the alternate inch-pound designations are provided for information purposes and enclosed in parentheses.
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes
(excluding those in tables and figures) shall not be considered as requirements of the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. Specific precaution statements are given in Section 7.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
C136 Test Method for Sieve Analysis of Fine and Coarse Aggregates
C294 Descriptive Nomenclature for Constituents of Concrete Aggregates
C670 Practice for Preparing Precision and Bias Statements for Test Methods for Construction Materials
D3666 Specification for Minimum Requirements for Agencies Testing and Inspecting Road and Paving Materials
D4753 Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction
Materials Testing
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
3. Significance and Use
3.1 The amount and size distribution of noncarbonate (insoluble) material in carbonate aggregates is of interest to those
conducting research on the polish susceptibility of stone used in pavements or on the friction properties of pavement surfaces. In
addition, some agencies utilize the test for acceptance purposes to delineate carbonate aggregates that polish excessively and
become slippery and those that will not.
NOTE 1—The quality of the results produced by this standard are dependent upon the competence of the personnel performing the procedure and the
capability, calibration, and the maintenance of the equipment used. Agencies that meet the criteria of PracticeSpecification D3666 are generally considered
capable of competent and objective testing/sampling/inspection/etc. testing/sampling/inspection, etc. Users of this standard are cautioned that compliance
with PracticeSpecification D3666 alone does not completely assureensure reliable results. Reliable results depend on many factors: following the
suggestions of PracticeSpecification D3666 or similar acceptable guideline provides a means of evaluating and controlling some of those factors.
1
This test method is under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.51 on Aggregate
Tests.
Current edition approved Dec. 1, 2015April 1, 2017. Published February 2016April 2017. Originally approved in 1972. Last previous edition approved in 20092015 as
D3042 – 09.D3042 – 09 (2015). DOI: 10.1520/D3042-09R15.10.1520/D3042-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Con
...

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