Standard Specification for Anaerobic Single-Component Adhesives (AN)

ABSTRACT
This specification establishes the requirements for single-component anaerobic adhesives suitable for locking, sealing, and retaining threaded or cylindrical assemblies. It is intended to be a means of classifying the adhesives, and does not address engineering design purposes. The adhesives are cured to a solid state when confined between closely fitting active metal surfaces. Materials shall undergo test procedures and conform accordingly to the following requirements: ultraviolet fluorescence; color and workmanship; flash point; storage stability; toxicity; solvent resistance; hot strength; heat aging; cold strength; lubricity; fluid tightness; wicking; viscosity; speed of cure; prevailing torque strength (strength at standard conditions); and qualification of primers.
SCOPE
1.1 This specification covers single-component anaerobic adhesives suitable for locking, sealing, and retaining threaded or cylindrical assemblies. The adhesives are cured to a solid state when confined between closely fitting active metal surfaces.
1.2 This specification is intended to be a means of classifying anaerobic adhesives. It is not intended for engineering design purposes.
1.3 This specification is intended to replace Military Specifications MIL-S-22473, MIL-S-46163, and MIL-R-46082.
1.4 The values stated in SI units are to be regarded as the standard.
The following safety hazards caveat pertains only to the test methods portion, Section , of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
30-Nov-2003
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ASTM D5363-03e1 - Standard Specification for Anaerobic Single-Component Adhesives (AN)
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
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Designation: D 5363 – 03
Standard Specification for
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Anaerobic Single-Component Adhesives (AN)
This standard is issued under the fixed designation D5363; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
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e NOTE—Editorial corrections were made in Table1 and footnote 1 in TableAN in August 2006.
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1. Scope D439 Specification for Automotive Gasoline
D445 Test Method for Kinematic Viscosity of Transparent
1.1 This specification covers single-component anaerobic
and Opaque Liquids (and Calculation of Dynamic Viscos-
adhesives suitable for locking, sealing, and retaining threaded
ity)
or cylindrical assemblies. The adhesives are cured to a solid
D770 Specification for Isopropyl Alcohol
state when confined between closely fitting active metal
D907 Terminology of Adhesives
surfaces.
D1084 Test Methods for Viscosity of Adhesives
1.2 This specification is intended to be a means of classify-
D1193 Specification for Reagent Water
ing anaerobic adhesives. It is not intended for engineering
D2693 Specification for Ethylene Glycol
design purposes.
D3951 Practice for Commercial Packaging
1.3 This specification is intended to replace Military Speci-
D4562 TestMethodforShearStrengthofAdhesivesUsing
fications MIL-S-22473, MIL-S-46163, and MIL-R-46082.
Pin-and-Collar Specimen
1.4 The values stated in SI units are to be regarded as the
D4800 Guide for Classifying and Specifying Adhesives
standard.
D5648 Test Method for Torque-Tension Relationship of
1.5 The following safety hazards caveat pertains only to the
Adhesives Used on Threaded Fasteners (Lubricity)
test methods portion, Section 7, of this specification. This
D5649 TestMethodforTorqueStrengthofAdhesivesUsed
standard does not purport to address all of the safety concerns,
on Threaded Fasteners
if any, associated with its use. It is the responsibility of the user
D5657 Test Method for Fluid Tightness Ability of Adhe-
of this standard to establish appropriate safety and health
sives Used on Threaded Fasteners
practices and determine the applicability of regulatory limita-
E122 Practice for Calculating Sample Size to Estimate,
tions prior to use.
With a Specified Tolerable Error, the Average for a
2. Referenced Documents
Characteristic of a Lot or Process
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2.2 Military Standards:
2.1 ASTM Standards:
MIL-STD-105 Sampling Procedures and Tables for Inspec-
A109/A109M Specification for Steel, Strip, Carbon (0.25
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tion by Attributes
Maximum Percent), Cold-Rolled
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MIL-STD-129 Marking for Shipment and Storage
B36/B36M SpecificationforBrassPlate,Sheet,Strip,And
MIL-STD-810 Environmental Test Methods and Engineer-
Rolled Bar
4
ing Guides
B209 Specification for Aluminum and Aluminum-Alloy
MIL-STD-118 Commercial Packaging of Supplies and
Sheet and Plate
4
Equipment
B633 Specification for Electrodeposited Coatings of Zinc
2.3 Federal Standards:
on Iron and Steel
FED-STD-313 Material Safety Data Sheets, Preparation
D56 TestMethodforFlashPointbyTagClosedCupTester
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and Submission of
2.4 Federal Specifications:
FF-N-836 Nut: Square, Hexagon, Cap, Slotted, Castle,
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This specification is under the jurisdiction of ASTM Committee D14 on
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Knurled, Welding and Single Ball Seat
Adhesives and is the direct responsibility of Subcommittee D14.60 on Adhesive
Material Classification System.
Current edition approved Dec. 1, 2003. Published January 2004. Originally
approved in 1993. Last previous edition approved in 1997 as D5363–97.
2 3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Withdrawn.
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contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
Standards volume information, refer to the standard’s Document Summary page on Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http://
the ASTM website. www.dodssp.daps.mil.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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D5363–03
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PPP-B-636 Box, Shipping, Fiberboard nut. Studies have shown that the torque measured at 180°
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QQ-P-416 Plating, Cadmium, Electrodeposited rotation of the nut is statistically equivalent to the average of
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2.5 Military Specifications:
the torque measured at the four ⁄4 turns. Since measuring the
MIL-R-46082 Retaining Compounds, Single-Component, torque at the one angle of rotation is more efficient, prevailing
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Anaerobic
torque is most often defined as the torque measured at 180°
MIL-S-22473 Sealing,
...

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