Standard Practice for Manual Piston Cylinder Sampling for Volatile Crude Oils, Condensates, and Liquid Petroleum Products

SIGNIFICANCE AND USE
5.1 This practice allows the collection of a representative sample of crude oil and/or condensate that may contain trace volatile dissolved components such as methane, ethane, propane, and fixed gases that would normally be lost using conventional atmospheric sampling methods. These highly volatile components can result in vapor pressure conditions above atmospheric pressure. This practice is recommended whenever accurate determination of vapor pressure, flash point, or other properties are required and where loss of volatile components can affect the test results.  
5.2 This practice is intended for capturing samples of crude oil and/or condensate for testing for the purpose of classification for transportation of dangerous goods as UN Class 3 Flammable Liquids, but is not limited to classification testing. Other test methods with sensitivities to light end loss may also utilize this sampling practice.  
5.3 Practice D3700 using a floating piston cylinder is recommended whenever true vapor pressures greater than 300 kPa at 50 °C are anticipated.
SCOPE
1.1 This practice includes the equipment and procedures for obtaining a representative sample of “live” or high vapor pressure crude oils, condensates, and/or liquid petroleum products from low pressure sample points, where there is insufficient sample point pressure to use a Floating Piston Cylinder (FPC) as described in Practice D3700.  
1.2 This practice is intended for use with sample types, such as UN Class 3 Flammable Liquids, that might have been collected and transported using open containers. The use of a manual piston cylinder in place of open containers is intended to prevent the loss of volatile (light end) components, which can impact subsequent test results.  
1.3 This practice is suitable for sampling crude oils, condensates, and/or liquid petroleum products having true vapor pressures less than 300 kPa (43 psia nominal) at 50 °C. This practice applies to samples that will typically fall between Practices D4057 (API MPMS Chapter 8.1) and D3700. This practice shall not be used for materials classified as UN Class 2 Gases2 (“…having a vapor pressure greater than 300 kPa at 50 °C or is completely gaseous at 20 °C at 101.3 kPa.”).  
1.4 This practice allows for sampling of crude oils that flow freely at the conditions of sampling.  
1.5 It is the responsibility of the user to ensure that the sampling point is located so as to obtain a representative sample.  
1.6 The values stated in SI units are to be regarded as standard.  
1.6.1 Exception—The values given in parentheses are for information only.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Published
Publication Date
30-Jun-2022
Current Stage
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D8009 − 22
Manual of Petroleum Measurement Standards (MPMS), Chapter 8.5
Standard Practice for
Manual Piston Cylinder Sampling for Volatile Crude Oils,
1
Condensates, and Liquid Petroleum Products
This standard is issued under the fixed designation D8009; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* 1.6.1 Exception—The values given in parentheses are for
information only.
1.1 This practice includes the equipment and procedures for
obtaining a representative sample of “live” or high vapor
1.7 This standard does not purport to address all of the
pressure crude oils, condensates, and/or liquid petroleum
safety concerns, if any, associated with its use. It is the
products from low pressure sample points, where there is
responsibility of the user of this standard to establish appro-
insufficient sample point pressure to use a Floating Piston
priate safety, health, and environmental practices and deter-
Cylinder (FPC) as described in Practice D3700.
mine the applicability of regulatory limitations prior to use.
1.2 Thispracticeisintendedforusewithsampletypes,such
1.8 This international standard was developed in accor-
as UN Class 3 Flammable Liquids, that might have been
dance with internationally recognized principles on standard-
collected and transported using open containers. The use of a
ization established in the Decision on Principles for the
manual piston cylinder in place of open containers is intended
Development of International Standards, Guides and Recom-
to prevent the loss of volatile (light end) components, which
mendations issued by the World Trade Organization Technical
can impact subsequent test results.
Barriers to Trade (TBT) Committee.
1.3 This practice is suitable for sampling crude oils,
condensates, and/or liquid petroleum products having true 2. Referenced Documents
vapor pressures less than 300 kPa (43 psia nominal) at 50 °C.
3
2.1 ASTM Standards:
This practice applies to samples that will typically fall between
D3700 Practice for Obtaining LPG Samples Using a Float-
Practices D4057 (API MPMS Chapter 8.1) and D3700. This
ing Piston Cylinder
practice shall not be used for materials classified as UN Class
2 D4057 Practice for Manual Sampling of Petroleum and
2 Gases (“…having a vapor pressure greater than 300 kPa at
Petroleum Products
50 °C or is completely gaseous at 20 °C at 101.3 kPa.”).
D4175 Terminology Relating to Petroleum Products, Liquid
1.4 This practice allows for sampling of crude oils that flow
Fuels, and Lubricants
freely at the conditions of sampling.
D4177 Practice for Automatic Sampling of Petroleum and
1.5 It is the responsibility of the user to ensure that the
Petroleum Products
sampling point is located so as to obtain a representative
D6377 Test Method for Determination of Vapor Pressure of
sample.
Crude Oil: VPCR (Expansion Method)
x
1.6 The values stated in SI units are to be regarded as D6378 Test Method for Determination of Vapor Pressure
standard. (VP ) of Petroleum Products, Hydrocarbons, and
X
Hydrocarbon-Oxygenate Mixtures (Triple Expansion
Method)
1
This practice is under the jurisdiction ofASTM Committee D02 on Petroleum
Products, Liquid Fuels, and Lubricants and the API Committee on Petroleum D7975 Test Method for Determination of Vapor Pressure of
Measurement, and is the direct responsibility of Subcommittee D02.02 /COMQ the
Crude Oil: VPCR -F(Tm°C) (Manual Expansion Field
x
joint ASTM-API Committee on Hydrocarbon Measurement for Custody Transfer
Method)
(Joint ASTM-API). This practice has been approved by the sponsoring committees
and accepted by the Cooperating Societies in accordance with established proce-
dures. This practice was issued as a joint ASTM-API standard in 2015.
Current edition approved July 1, 2022. Published August 2022. Originally
3
approved in 2015. Last previous edition approved in 2015 as D8009 – 15. DOI: For referenced ASTM standards, visit the ASTM website, www.astm.org, or
10.1520/D8009-22. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
2
UN Recommendations of the Transportation of Dangerous Goods, Chapter Standards volume information, refer to the standard’s Document Summary page on
2.2.1.1. the ASTM website.
*A Summary of Changes section appears at the end of this standard
© Jointly copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, USA and the American Petroleu
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D8009 − 15 D8009 − 22
Manual of Petroleum Measurement Standards (MPMS), Chapter 8.5
Standard Practice for
Manual Piston Cylinder Sampling for Volatile Crude Oils,
1
Condensates, and Liquid Petroleum Products
This standard is issued under the fixed designation D8009; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Scope*
1.1 This practice includes the equipment and procedures for obtaining a representative sample of “live” or high vapor pressure
crude oils, condensates, and/or liquid petroleum products from low pressure sample points, where there is insufficient sample point
pressure to use a Floating Piston Cylinder (FPC) as described in Practice D3700.
1.2 This practice is intended for use with sample types, such as UN Class 3 Flammable Liquids, that might have been collected
and transported using open containers. The use of a manual piston cylinder in place of open containers is intended to prevent the
loss of volatile (light end) components, which can impact subsequent test results.
1.3 This practice is suitable for sampling crude oils, condensates, and/or liquid petroleum products having true vapor pressures
less than 300 kPa (43 psia nominal) at 50 °C. This practice applies to samples that will typically fall between Practices D4057 (API
2
MPMS Chapter 8.1) and D3700. This practice shall not be used for materials classified as UN Class 2 Gases (“…having a vapor
pressure greater than 300 kPa at 50 °C or is completely gaseous at 20 °C at 101.3 kPa.”).
1.4 This practice allows for sampling of crude oils that flow freely at the conditions of sampling.
1.5 It is the responsibility of the user to ensure that the sampling point is located so as to obtain a representative sample.
1.6 The values stated in SI units are to be regarded as standard.
1.6.1 Exception—The values given in parentheses are for information only.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
1
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and the API Committee on Petroleum Measurement,
and is the direct responsibility of Subcommittee D02.02 /COMQ the joint ASTM-API Committee on Hydrocarbon Measurement for Custody Transfer (Joint ASTM-API).
This practice has been approved by the sponsoring committees and accepted by the Cooperating Societies in accordance with established procedures. This practice was issued
as a joint ASTM-API standard in 2015.
Current edition approved Dec. 1, 2015July 1, 2022. Published December 2015August 2022. Originally approved in 2015. Last previous edition approved in 2015 as
D8009 – 15. DOI: 10.1520/D8009-15.10.1520/D8009-22.
2
UN Recommendations of the Transportation of Dangerous Goods, Chapter 2.2.1.1.
*A Summary of Changes section appears at the end of this standard
© Jointly copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, USA and the American Petroleum Institute (API), 1220 L Street NW, Washington DC 20005, USA
1

---------------------- Page: 1 ----------------------
D8009 − 22
2. Referenced Documents
3
2.1 ASTM Standards:
D3700 Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4175 Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
D6377 Test Method for Determination of Vapor Pressure of Crude Oil: VPCR (Expansion Method)
x
D6378 Test Method for Determination of Vapor Pressure (VP ) of Petroleum Products, Hydrocarbons, and Hydrocarbon-
X
Oxygenate Mixtures (Triple Expansion Method)
D7975 Test Method for Determination of
...

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