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75.040 - Crude petroleum

ICS 75.040 Details

Crude petroleum

Rohol

Pétrole brut

Surova nafta

General Information

Parent
75 - PETROLEUM AND RELATED TECHNOLOGIES

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Standardization Organization
Technical Committee
Directive
Mandate
50
SIST
SIST EN ISO 12185:2024(Main)
Crude petroleum, petroleum products and related products - Determination of density - Laboratory density meter with an oscillating U tube sensor (ISO 12185:2024)
EN ISO 12185:2024

This document specifies a method for the determination, using an oscillating U-tube density meter, of the density of crude petroleum and related products within the range 600 kg/m3 to 1 100 kg/m3, which can be handled as single-phase liquids at the test temperature and pressure.
This document is applicable to liquids of any vapour pressure as long as suitable precautions are taken to ensure that they remain in single phase. Loss of light components leads to changes in density during both the sample handling and the density determination.
This method is not intended for use with in-line density meters.

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SIST
SIST EN ISO 3838:2004/A1:2024(Amendment)
Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods - Amendment 1 (ISO 3838:2004/Amd 1:2023)
EN ISO 3838:2004/A1:2023
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EN ISO 3838:2004/A1:2023(Amendment)
Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods - Amendment 1 (ISO 3838:2004/Amd 1:2023)
SIST EN ISO 3838:2004/A1:2024
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SIST
SIST EN 15199-3:2021(Main)
Petroleum products - Determination of boiling range distribution by gas chromatography method - Part 3: Crude oil
EN 15199-3:2020

This European Standard describes a method for the determination of the boiling range distribution of petroleum products by capillary gas chromatography using flame ionisation detection. The standard is applicable to crude oils. The boiling range distribution and recovery to C100 or C120 can be determined.
Two procedures are described: single and dual analysis mode. The basis of each is the calculation procedure as described in Annex A.
NOTE 1   This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations.
NOTE 2   For the purposes of this European Standard, the terms "% (m/m)" and "% (V/V)" are used to represent respectively the mass fraction and the volume fraction.
WARNING : Use of this European Standard may involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

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SIST
SIST EN 14639:2006(Main)
Crude tar and crude benzole - Characteristics and test methods
EN 14639:2005

This European Standard defines the methods of tests for the determination of the characteristics of crude tar and crude benzole.

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CEN
EN ISO 3838:2004(Main)
Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods (ISO 3838:2004)
SIST EN ISO 3838:2004

ISO 3838:2004 specifies methods for the determination of the density or relative density of crude petroleum and of petroleum products handled as liquids.
The capillary-stoppered pyknometer method is also for use with solids and this method may also be used for coal tar products, including road tars, creosote and tar pitches, or for mixtures of these with petroleum products. This method is not suitable for the determination of the density or relative density of highly volatile liquids having Reid vapour pressures greater than 50 kPa according to ISO 3007 or having an initial boiling point below 40 degrees Celsius.
The graduated bicapillary pyknometer method is recommended for the accurate determination of the density or relative density of all except the more viscous products, and is particularly useful when only small amounts of samples are available. The method is restricted to liquids having Reid vapour pressures of 130 kPa or less according to ISO 3007 and having kinematic viscosities less than 50 mm2/s (50 centistokes (cSt)) at the test temperature.
Special precautions are specified for the determination of the density or relative density of highly volatile liquids.

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SIST
SIST EN ISO 3838:2004(Main)
Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods (ISO 3838:2004)
EN ISO 3838:2004

ISO 3838:2004 specifies methods for the determination of the density or relative density of crude petroleum and of petroleum products handled as liquids.
The capillary-stoppered pyknometer method is also for use with solids and this method may also be used for coal tar products, including road tars, creosote and tar pitches, or for mixtures of these with petroleum products. This method is not suitable for the determination of the density or relative density of highly volatile liquids having Reid vapour pressures greater than 50 kPa according to ISO 3007 or having an initial boiling point below 40 degrees Celsius.
The graduated bicapillary pyknometer method is recommended for the accurate determination of the density or relative density of all except the more viscous products, and is particularly useful when only small amounts of samples are available. The method is restricted to liquids having Reid vapour pressures of 130 kPa or less according to ISO 3007 and having kinematic viscosities less than 50 mm2/s (50 centistokes (cSt)) at the test temperature.
Special precautions are specified for the determination of the density or relative density of highly volatile liquids.

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SIST
SIST ISO 3007:2002(Main)
Petroleum products and crude petroleum -- Determination of vapour pressure -- Reid method
ISO 3007:1999

This International Standard specifies a method for the determination of the vapour pressure of liquid petroleum
products consisting of essentially or wholly of hydrocarbon components, or containing oxygenated hydrocarbons of
specific types and at specified maximum concentrations. The method does not apply outside these concentration
levels, nor to any blends containing methanol or other oxygenated hydrocarbons not covered in note 1.
NOTE 1 The maximum concentration of ethers containing 5 or more carbon atoms is 15 % (V/V), and for ethanol is 10 %
(V/V). For higher alcohols, the maximum concentration is 7 % (V/V).
NOTE 2 For the purposes of this International Standard, the term "%(V/V)" is used to represent the volume fraction of a
material.
For petroleum products containing methanol, or other oxygenated hydrocarbons outside the scope of note 1, a dry
vapour-pressure test method should be used. For liquefied petroleum gases, ISO 4256 should be used. The test
method may be applied to volatile crude petroleum with a vapour pressure exceeding 10 kPa, although the
precision has not been evaluated.
Four procedures are described in this International Standard. Procedures A and B are alternative apparatus
configurations for products with a Reid vapour pressure up to 180 kPa, Procedure C is applied to liquid products
with a Reid vapour pressure above 180 kPa, and Procedure D applies to aviation gasolines with a Reid vapour
pressure of approximately 50 kPa.
Vapour pressure is an important physical property of volatile liquids, and has critical performance implications for
automotive and aviation gasolines. Vapour pressure is also one of the properties affecting atmospheric evaporation,
and is therefore increasingly used in regulations relating to emissions and air quality control. Vapour pressure is
also a critical property limiting the performance and safety of operation of equipment during transfer operations.
NOTE Because the external atmospheric pressure is counteracted by the atmospheric pressure initially in the vapour
chamber, the Reid vapour pressure is approximately the "absolute" vapour pressure at 37,8 °C. The Reid vapour pressure
differs from the true vapour pressure of the sample owing to slight vaporization of the sample and the pressure of water vapour
and air in the confined space.

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SIST
SIST EN ISO 3735:1999(Main)
Crude petroleum and fuel oils - Determination of sediment - Extraction method (ISO 3735:1999)
EN ISO 3735:1999

Migrated from Progress Sheet (TC Comment) (2000-07-10): Updating of existing EN implementations of ISO standards (standing resolution); ++ Will go to VA.

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SIST
SIST EN ISO 3675:1999(Main)
Crude petroleum and liquid petroleum products - Laboratory determination of density - Hydrometer method (ISO 3675:1998)
EN ISO 3675:1998

Migrated from Progress Sheet (TC Comment) (2000-07-10): Revision of EN ISO 3675:1995

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ISO 3735:1999(Main)
Crude petroleum and fuel oils — Determination of sediment — Extraction method
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EN ISO 3735:1999(Main)
Crude petroleum and fuel oils - Determination of sediment - Extraction method (ISO 3735:1999)
SIST EN ISO 3735:1999

Migrated from Progress Sheet (TC Comment) (2000-07-10): Updating of existing EN implementations of ISO standards (standing resolution); ++ Will go to VA.

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SIST
SIST EN ISO 9029:1998(Main)
Crude petroleum - Determination of water - Distillation method (ISO 9029:1990)
EN ISO 9029:1995

The precision data of this procedure have only been determined for water contents up to 1 % (V/V). Includes principle, apparatus, solvent, calibration and recovery test, sampling, procedure, expression of results, precision and test report. The distillation apparatus is shown in figures 1 and 2. The precision of the method is shown in figure 3. The sample handling is described in annex A.

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ISO
ISO 10337:1997(Main)
Crude petroleum — Determination of water — Coulometric Karl Fischer titration method
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ISO
ISO 9114:1997(Main)
Crude petroleum — Determination of water content by hydride reaction — Field method
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ISO
ISO 10336:1997(Main)
Crude petroleum — Determination of water — Potentiometric Karl Fischer titration method
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SIST
SIST ISO 9030:1996(Main)
Crude petroleum -- Determination of water and sediment -- Centrifuge method
ISO 9030:1990

Specifies a method for the laboratory determination. The precision data of this procedure have only been determined for water contents up to 1 % (V/V). Includes principle, apparatus, reagents, sampling, procedure, expression of results, precision and test report. A centrifuge tube is shown in figure 1. The procedure for reading the volume of water and sediment is shown in figure 2. The precision of the method is shown in figure 3. The sample handling is described in annex A.

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EN ISO 9029:1995(Main)
Crude petroleum - Determination of water - Distillation method (ISO 9029:1990)
SIST EN ISO 9029:1998

The precision data of this procedure have only been determined for water contents up to 1 % (V/V). Includes principle, apparatus, solvent, calibration and recovery test, sampling, procedure, expression of results, precision and test report. The distillation apparatus is shown in figures 1 and 2. The precision of the method is shown in figure 3. The sample handling is described in annex A.

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ISO
ISO 9029:1990(Main)
Crude petroleum — Determination of water — Distillation method
SIST ISO 9029:1996

The precision data of this procedure have only been determined for water contents up to 1 % (V/V). Includes principle, apparatus, solvent, calibration and recovery test, sampling, procedure, expression of results, precision and test report. The distillation apparatus is shown in figures 1 and 2. The precision of the method is shown in figure 3. The sample handling is described in annex A.

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ISO
ISO 9030:1990(Main)
Crude petroleum — Determination of water and sediment — Centrifuge method
SIST ISO 9030:1996

Specifies a method for the laboratory determination. The precision data of this procedure have only been determined for water contents up to 1 % (V/V). Includes principle, apparatus, reagents, sampling, procedure, expression of results, precision and test report. A centrifuge tube is shown in figure 1. The procedure for reading the volume of water and sediment is shown in figure 2. The precision of the method is shown in figure 3. The sample handling is described in annex A.

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SIST
SIST EN ISO 12185:1998(Main)
Crude petroleum and petroleum products - Determination of density - Oscillating U-tube method (ISO 12185:1996)
EN ISO 12185:1996

Gives a method for the determination, using an oscillation U-tube densitometer, of the density of crude petroleum and related products within the range 600 kg/m^3 to 1 100 kg/m^3 which can be handled as single-phase liquids at the test temperature and pressure.

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SIST
SIST EN 15199-3:2008(Main)
Petroleum products - Determination of boiling range distribution by gas chromatography method - Part 3: Crude oil
EN 15199-3:2008

This European standard describes a method for the determination of the boiling range distribution of petroleum products by capillary gas chromatography using flame ionisation detection. The standard is applicable to crude oils. The boiling range distribution and recovery to C100 or C120 can be determined.Two procedures are described: single and dual analysis mode. The basis of each is the calculation procedure as described in Annex A.

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SIST
SIST EN ISO 3838:1998(Main)
Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods (ISO 3838:1983)
EN ISO 3838:1995

Migrated from Progress Sheet (TC Comment) (2000-07-10): Decision of BT to submit this ISO document to UAP procedure.

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CEN
EN ISO 3838:1995(Main)
Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods (ISO 3838:1983)
SIST EN ISO 3838:1998

Migrated from Progress Sheet (TC Comment) (2000-07-10): Decision of BT to submit this ISO document to UAP procedure.

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SIST
SIST EN ISO 3735:1998(Main)
Crude petroleum and fuel oils - Determination of sediment - Extraction method (ISO 3735:1975)
EN ISO 3735:1995

Migrated from Progress Sheet (TC Comment) (2000-07-10): Decision of BT to submit this ISO document to UAP procedure.

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CEN
EN ISO 3735:1995(Main)
Crude petroleum and fuel oils - Determination of sediment - Extraction method (ISO 3735:1975)
SIST EN ISO 3735:1998

Migrated from Progress Sheet (TC Comment) (2000-07-10): Decision of BT to submit this ISO document to UAP procedure.

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SIST
SIST ISO 9029:1996(Main)
Crude petroleum -- Determination of water -- Distillation method
ISO 9029:1990

The precision data of this procedure have only been determined for water contents up to 1 % (V/V). Includes principle, apparatus, solvent, calibration and recovery test, sampling, procedure, expression of results, precision and test report. The distillation apparatus is shown in figures 1 and 2. The precision of the method is shown in figure 3. The sample handling is described in annex A.

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SIST
SIST ISO 3735:1996(Main)
Crude petroleum and fuel oils -- Determination of sediment -- Extraction method
ISO 3735:1975
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SIST
SIST ISO 3675:1996(Main)
Crude petroleum and liquid petroleum products -- Laboratory determination of density or relative density -- Hydrometer method
ISO 3675:1993
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ISO
ISO 3734:1976(Main)
Crude petroleum and fuel oils — Determination of water and sediment — Centrifuge method
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ISO
ISO 3735:1975(Main)
Crude petroleum and fuel oils — Determination of sediment — Extraction method
SIST ISO 3735:1996
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