ASTM D1583-01(2008)
(Test Method)Standard Test Method for Hydrogen Ion Concentration of Dry Adhesive Films
Standard Test Method for Hydrogen Ion Concentration of Dry Adhesive Films
SIGNIFICANCE AND USE
The pH of an adhesive may be a factor whereby the adherends or the adhesive itself may be adversely affected in time by the acidity or alkalinity.
SCOPE
1.1 This test method covers determination of the hydrogen ion concentration (pH), acidity, or alkalinity, of organic adhesives in the cured dry film form. This test method is not designed to apply to pressure-sensitive adhesives.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
General Information
Relations
Buy Standard
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1583 − 01 (Reapproved2008)
Standard Test Method for
Hydrogen Ion Concentration of Dry Adhesive Films
This standard is issued under the fixed designation D1583; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 4.4 The pH is determined using a pH meter in accordance
with Test Method E70.
1.1 This test method covers determination of the hydrogen
ion concentration (pH), acidity, or alkalinity, of organic adhe-
5. Significance and Use
sives in the cured dry film form. This test method is not
designed to apply to pressure-sensitive adhesives. 5.1 The pH of an adhesive may be a factor whereby the
adherends or the adhesive itself may be adversely affected in
1.2 The values stated in SI units are to be regarded as the
time by the acidity or alkalinity.
standard. The values given in parentheses are for information
only.
6. Apparatus
1.3 This standard does not purport to address all of the
6.1 pH Meter, capable of making measurements to 60.05
safety concerns, if any, associated with its use. It is the
pH.
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
6.2 Glass Vial, capable of properly immersing the electrode
bility of regulatory limitations prior to use.
of the pH meter when filled with the specified test solution.
6.3 Distilled Water, with a pH between 5.6 and 7.0 at 23 6
2. Referenced Documents
1°C (73.4 6 1.8°F).
2.1 ASTM Standards:
6.4 Glass Sheet, free from scratches, approximately 200 by
D907 Terminology of Adhesives
250 mm (8 by 10 in.) in size for use in oven.
E70 Test Method for pH of Aqueous Solutions With the
6.5 Circulating-Air Oven, capable of maintaining tempera-
Glass Electrode
tures of 23 6 1°C (73.4 6 1.8°F) to 150 6 1°C (302 6 1.8°F).
3. Terminology
7. Sampling
3.1 Definitions—Many of the terms in this test method are
defined in Terminology D907. 7.1 Except in special cases, take a composite sample when
possible from three or more separate containers, chosen at
4. Summary of Test Method random.Also take samples from containers which appear to be
nonrepresentative, and test such samples separately. Place the
4.1 Collect samples of the adhesive to be tested with any
samples immediately in airtight glass containers filled to
hardener necessary.
prevent excessive air space above the adhesive and transport
4.2 Dry adhesive films are prepared.
them to the testing laboratory in these containers. Take
precautions to reduce evaporation or drying to a minimum.
4.3 The adhesive films are ground and mixed with distilled
Thoroughly mix the adhesive in the container if there is a
water.
tendency for the materials to separate before a sample is taken.
Use the required catalysts and hardeners from the same
shipment as the other adhesive components if the components
This test method is under the jurisdiction of ASTM Committee D14 on
are furnished as a unit by the adhesive manufacturer.
Adhesives and is the direct responsibility of Subcommittee D14.30 on Wood
Adhesives
Current edition approved April 1, 2008. Published April 2008. Originally
8. Test Specimens
approved in 1958. Last previous edition approved in 2001 as D1583 – 01. DOI:
10.1520/D1583-01R08.
8.1 Room-Temperature Setting Adhesives—Use adhesives
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
that form dry films at room temperature and mix in accordance
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
with the recommendations of the adhesive manufacturer.
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. Spread the adhesive on glass or other inert material to which
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D1583 − 01 (2008)
the adhesive does not adhere to a film thickness of less than instructions of the manufacturer of the i
...
This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D1583–00 Designation: D 1583 – 01 (Reapproved 2008)
Standard Test Method for
Hydrogen Ion Concentration of Dry Adhesive Films
This standard is issued under the fixed designation D 1583; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope
1.1 This test method covers determination of the hydrogen ion concentration (pH), acidity, or alkalinity, of organic adhesives
in the cured dry film form. This test method is not designed to apply to pressure-sensitive adhesives.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
D 907 Terminology of Adhesives
E 70 Test Method for pH of Aqueous Solutions withWith the Glass Electrode
3. Terminology
3.1 Definitions— Many of the terms in this test method are defined in Terminology D 907.
4. Summary of Test Method
4.1 Collect samples of the adhesive to be tested with any hardener necessary.
4.2 Dry adhesive films are prepared.
4.3 The adhesive films are ground and mixed with distilled water.
4.4 The pH is determined using a pH meter in accordance with Test Method E 70.
5. Significance and Use
5.1 The pH of an adhesive may be a factor whereby the adherends or the adhesive itself may be adversely affected in time by
the acidity or alkalinity.
6. Apparatus
6.1 pH Meter, capable of making measurements to 60.05 pH.
6.2 Glass Vial, capable of properly immersing the electrode of the pH meter when filled with the specified test solution.
6.3 Distilled Water, with a pH between 5.6 and 7.0 at 23 6 1°C (73.4 6 1.8°F).
6.4 Glass Sheet, free from scratches, approximately 200 by 250 mm (8 by 10 in.) in size for use in oven.
6.5 Circulating-Air Oven, capable of maintaining temperatures of 23 6 1°C (73.4 6 1.8°F) to 150 6 1°C (302 6 1.8°F).
7. Sampling
7.1 Except in special cases, take a composite sample when possible from three or more separate containers, chosen at random.
Also take samples from containers which appear to be nonrepresentative, and test such samples separately. Place the samples
immediately in airtight glass containers filled to prevent excessive air space above the adhesive and transport them to the testing
laboratory in these containers. Take precautions to reduce evaporation or drying to a minimum. Thoroughly mix the adhesive in
This test method is under the jurisdiction of ASTM Committee D-14 on Adhesives and is the direct responsibility of Subcommittee D14.30 on Wood Adhesives.
Current edition approved May 10, 2000. Published August 2000. Originally published as D1583–58. Last previous edition D1583–96.
This test method is under the jurisdiction of ASTM Committee D14 on Adhesives and is the direct responsibility of Subcommittee D14.30 on Wood Adhesives
Current edition approved April 1, 2008. Published April 2008. Originally approved in 1958. Last previous edition approved in 2001 as D 1583 – 01.
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
, Vol 15.06.volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D 1583 – 01 (2008)
the container if there is a tendency for the materials to separate before a sample is taken. Use the required catalysts and hardeners
from the same shipment as the other adhesive components if the components are furnished as a unit by the adhesive manufacturer.
8. Test Specimens
8.1 Room-Temperature Set
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.