ASTM F1097-91(1996)
(Specification)Standard Specification for Mortar, Refractory (High-Temperature, Air-Setting)
Standard Specification for Mortar, Refractory (High-Temperature, Air-Setting)
SCOPE
1.1 This specification covers dry air-setting refractory mortar for use in laying and bonding refractory brick in ship boiler furnaces; and wet air-setting refractory mortar for use in laying refractory brick in stationary boiler furnaces, bright annealing furnaces, controlled atmosphere furnaces, and furnaces heated by electric elements.
1.2 The values stated in inch-pound units are to be regarded as standard. The SI units in parentheses are for information purposes only and may be approximate.
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
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Designation: F 1097 – 91 (Reapproved 1996) An American National Standard
Standard Specification for
Mortar, Refractory (High-Temperature, Air-Setting)
This standard is issued under the fixed designation F 1097; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope specified in the contract or purchase order (see 4.1.3):
MIL-STD-105 Sampling Procedures and Tables for Inspec-
1.1 This specification covers dry air-setting refractory mor-
tion by Attributes
tar for use in laying and bonding refractory brick in ship boiler
MIL-STD-129 Marking for Shipment and Storage
furnaces and wet air-setting refractory mortar for use in laying
refractory brick in stationary boiler furnaces, bright annealing
3. Classification
furnaces, controlled atmosphere furnaces, and furnaces heated
3.1 The refractory mortar shall be of the following types:
by electric elements.
3.1.1 Type 1—Dry.
1.2 The values stated in inch-pound units are to be regarded
3.1.2 Type 2—Wet.
as standard. The SI units in parentheses are for information
purposes only and may be approximate.
4. Ordering Information
1.3 This standard does not purport to address all of the
4.1 Orders for material under this specification shall include
safety concerns, if any, associated with its use. It is the
the following information, as necessary to adequately describe
responsibility of the user of this standard to establish appro-
the material:
priate safety and health practices and determine the applica-
4.1.1 ASTM designation and year of issue,
bility of regulatory limitations prior to use.
4.1.2 Type required (see 3.1), and
2. Referenced Documents 4.1.3 Optional requirements, if any (see S1).
2.1 ASTM Standards:
5. Material
C 24 Test Method for Pyrometric Cone Equivalent (PCE) of
2 5.1 The mortar shall be composed of finely ground heat-
Fireclay and High Alumina Refractory Materials
resistant clays, minerals, or a mixture of clays and minerals in
C 27 Classification of Fire Clay and High-Alumina Refrac-
2 either a dry or wet condition.
tory Brick
5.1.1 Type 1, Dry—Mortar shall be furnished dry and shall
C 92 Test Methods for Sieve Analysis and Water Content of
2 be ready for use as soon as mixed with water. Mortar, after
Refractory Materials
being mixed with water and then dried, shall be capable of
C 133 Test Methods for Cold Crushing Strength and Modu-
2 being remixed with water.
lus of Rupture of Refractories
5.1.2 Type 2, Wet—Mortar shall be furnished ready for use
C 198 Test Method for Cold Bonding Strength of Refrac-
2 at a trowelling consistency and shall be easily mixed with
tory Mortar
2 water to a dipping consistency.
C 199 Test Method for Pier Test for Refractory Mortars
2.2 Federal Specifications —The following documents
6. Performance Requirements
shall apply only when one or more of the requirements of S1
6.1 Resistance to Heat Soaking—Mortar shall not soften nor
are specified in the contract or purchase order (see 4.1.3):
show any evidence of fusion, and the shrinkage shall not be
UU-S-48 Sacks, Shipping, Paper
greater than hairline cracks when tested as specified in 11.2.
PPP-B-35 Bags: Textile, Shipping, Burlap, Cotton and Wa-
6.2 Bonding Strength—The average modulus of rupture at
terproof Laminated
the brick joint when tested as specified in 11.3 shall be not less
PPP-B-704 Pails: Shipping, Steel (1 through 12 gallon)
than shown in Table 1.
2.3 Military Standards —The following documents shall
6.3 Pyrometric Cone Equivalent (PCE)—The PCE shall be
apply only when one or more of the requirements of S1 are
not less than cone 32 (see 11.4).
1 7. Requirements
This specification is under the jurisdiction of ASTM Committee F-25 on Ships
and Marine Technology and is the direct responsibility of Subcommittee F25.07 on
7.1 Fineness—Mortar shall be ground to such fineness that
General Requirements.
not more than 5 % shall be retained on a No. 40 ASTM sieve,
Current edition approved Feb. 22, 1991. Published July 1991.
and not more than 0.5 % shall be held on a No. 30 ASTM sieve
Annual Book of ASTM Standards, Vol 15.01.
Standardization Documents Order Desk, Building 4, Section D, 700 Robbins
(see 11.1).
Ave., Philadelphia, PA 19111-5094, ATTN: NPODS.
Copyright © ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
F 1097
TABLE 1 Bonding Strength of Mortar
9.2.1 The test sample shall be a 45-lbs (20-kg) composite of
the randomly selected sample units. Two or more determina-
Average Modulus of Rupture,
tions as applicable (see Table 2) shall be performed on the
Temperatures, °F (°C)
psi (kPa), min
composite. There shall be no evidence of failure to meet the
230 (110) 200 (1400)
specified unit or average requirements.
1000 (538) 100 (700)
2000 (1093) 100 (700)
9.3 The PCE shall be determined on two cones of different
samples from each lot. If both cones fail, this shall be cause for
rejection without retest. If either cone fails, three additional
7.2 Shelf Life, Type 1—Mortar shall show no deterioration
cones shall be made, each from a different sample. If any one
after 1 year’s storage.
of the three retest cones fail, this shall be cause for rejection.
7.3 Shelf Life, Type 2—At any time within one year of
shipment from the supplier, the mortar in a previously un- 10. Specimen Preparation
opened container shall not have stiffened to such an extent as
10.1 The entire mortar sample for testing shall be thor-
to interfere with its easy removal and mixing.
oughly mixed to ensure uniformity before any portion is taken
7.4 Consistency—Mortar, when tempered with water, shall
for tests. The selected portion of Type 1 (dry) mortar shall be
be of such consistency that it will be suitable for spreading
mixed with water to a trowelling consistency for the tests of
easily with a trowel or for dipping and for laying refractory
11.2 and 11.3.
brick and bonding them together upon drying and upon
10.2 For the test specified in 11.3, brick-mortar joints shall
subsequent heating at furnace temperatures. Mortar shall retain
be prepared in accordance with Test Method C 198, except that
this degree of workability for 2 h.
refractory bricks, conforming to Classification C 27, super-
7.4.1 The mixed mortar shall have sufficient water retention
duty, shall be used and shall be cut in half. The two halves of
to permit a ⁄16-in. (2-mm) joint to be made with a trowelling
each brick shall be placed in a device suitable for bringing,
consistency, but not allow the newly laid brick to float out of
with a straight motion, the molded ends together with the faces
position.
parallel at all times to form a bond.
10.2.1 A small quantity of mortar shall be spread by a trowel
8. Workmanship
on the upper face forming the bond to ensure intimate contact.
8.1 Workmanship shall be first class in every respect. There
Sufficient mortar to give a ⁄8-in. (3-mm) thick layer shall be
shall be no foreign material or caked aggregate lumps in the
spread evenly on the lower bond forming face and the upper
mortar. Wet mortar shall be easily removed from the container
half shall be lowered until it is ⁄16 in. (2 mm) from the lower
and shall mix easily to a uniform trowelling consistency.
half. The excess mortar shall be cut from the joint, flush with
the sides of the brick. The unit thus formed shall be removed
9. Sampling
at once from the bond-forming machine. The bond specimens
9.1 An inspection lot for tests and inspections shall consist
shall be allowed to air-dry for 24 h.
of all material manufactured at essentially the same time and of
the same type offered for delivery at one time.
11. Test Methods
9.2 For the tests specified in 11.1 through 11.4, the sample
11.1 Fineness—The fineness test shall be made in accor-
unit shall be 15 lbs (7 kg) of mortar. No
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