Standard Test Method for Ductility Testing of Metallic Foil

SCOPE
1.1 This test method covers the determination of ductility, that is, the ability to undergo plastic deformation in tension or bending before fracturing, of metallic foil in thicknesses up through 0.150 mm (0.0059 in.).
1.2 Values stated in SI units are to be regarded as the standard. Inch-pound units are provided for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
31-Dec-1999
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ASTM E796-94 - Standard Test Method for Ductility Testing of Metallic Foil
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NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: E 796 – 94 An American National Standard
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
Standard Test Method for
Ductility Testing of Metallic Foil
This standard is issued under the fixed designation E 796; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
true tensile strain at fracture. Elongation and reduction of area represent
1. Scope
the engineering tensile strain after fracture.
1.1 This test method covers the determination of ductility,
NOTE 3—For the purpose of this definition the fatigue ductility expo-
that is, the ability to undergo plastic deformation in tension or 4
nent, c, is defined as c 5 −0.60 (see equation in 9.1).
bending before fracturing, of metallic foil in thicknesses up
4. Summary of Test Method
through 0.150 mm (0.0059 in.).
1.2 Values stated in SI units are to be regarded as the
4.1 The specimen is subjected to a fatigue test which
standard. Inch-pound units are provided for information only.
employs precisely controlled, symmetric, cyclic, constant-
1.3 This standard does not purport to address all of the
amplitude, flexural strains of a magnitude that will cause
safety concerns, if any, associated with its use. It is the
fracture in the low-cycle fatigue regime.
responsibility of the user of this standard to establish appro-
4.2 The fatigue ductility is determined from an equation
priate safety and health practices and determine the applica-
derived from universal, empirical, relationships between ten-
bility of regulatory limitations prior to use.
sile properties and fatigue behavior which utilizes the strain
range employed and the fatigue life obtained in the fatigue test,
2. Referenced Documents
as well as the modulus of elasticity, the tensile strength and the
2.1 ASTM Standards:
fracture strength determined in accordance with Test Method
E 3 Methods of Preparation of Metallographic Specimens
E 111 and Test Methods E 8, with the provisions in Test
E 6 Terminology Relating to Methods of Mechanical Test-
Methods E 345 and in this standard.
ing
5. Significance and Use
E 8 Test Methods for Tension Testing of Metallic Materials
E 111 Test Method for Young’s Modulus, Tangent Modulus,
5.1 For bulk specimens, tension tests provide an adequate
and Chord Modulus
means to determine the ductility of materials either through the
E 345 Test Methods of Tension Testing of Metallic Foil
measurement of elongation or reduction of area. For foil
E 513 Definitions of Terms Relating to Constant-Amplitude
specimens, however, tension tests are not very useful for the
Low-Cycle Fatigue Testing
determination of ductility. This test method, employing low-
E 606 Practice for Strain Controlled Fatigue Testing
cycle fatigue, circumvents the difficulties arising from the
E 1150 Definitions of Terms Relating to Fatigue
continuous application of strain until fracture and determines
the ductility indirectly from empirical low-cycle fatigue rela-
3. Terminology
tionships for metals.
3.1 Definitions:
5.2 The results of ductility tests from selected portions of a
3.1.1 The definitions of terms appearing in Definitions E 6,
metallic foil may not totally represent the ductility of the entire
E 1150, E 513, and Practice E 606, shall be considered as
foil or its in-service behavior in different environments.
applying to the terms used in this test method.
5.3 This test method is considered satisfactory for accep-
3.1.2 fatigue ductility, D —the ability of a material to
f tance testing of commercial shipments, design purposes, ser-
deform plastically before fracturing, determined from a
vice evaluation, manufacturing control, and research and
constant-strain amplitude, low-cycle fatigue test.
development.
NOTE 1—Fatigue ductility is usually expressed in percent in direct
6. Apparatus
analogy with elongation and reduction of area ductility measures.
NOTE 2—The fatigue ductility corresponds to the fracture ductility, the 6.1 Fatigue Ductility Flex Tester as schematically shown in
Fig. 1. A photograph of the tester is shown in Fig. 2. The tester
consists of a juxtaposed pair of precision test mandrels moving
This test method is under the jurisdiction of ASTM Committee E-28 on
Mechanical Testing and is the direct responsibility of Subcommittee E28.02 on
Ductility and Flexure Testing. Engelmaier, W., “A Method for the Determination of Ductility for Thin Metallic
Current edition approved Feb. 15, 1994. Published April 1994. Originally Materials,” Formability 2000 A.D., ASTM STP 753, ASTM, 1981, in press.
published as E 796–81. Last previous edition E 796–88 (1993). Model 2 FDF Flex Ductility Tester, manufactured in accordance with the
Annual Book of ASTM Standards, Vol 03.01. original Bell Laboratories design, available from Universal Tool and Machine, Inc.,
Discontinued—See 1986 Annual Book of ASTM Standards, Vol 03.01. 171 Coit St., Irvington, NJ 07111, has been found satisfactory.
E 796
of the yield strength (0.2 % offset, determined in accordance
with Test Methods E 8 with the provisions in Test Methods
E 345) of the material. A 100-g (3-oz) tension weight is
suitable for most specimens; however, for very thin foil
specimens it might be necessary to use a lighter tension weight.
6.2 Double-Bladed Specimen Cutter, as required in Test
Methods E 345, but capable of cutting specimens to the width
required herein (Section 7).
7. Test Specimens
7.1 Specimen Preparation—Test specimens shall be pre-
pared in accordance with Test Methods E 345, Type B speci-
mens, with the dimensions as specified herein. The specimens
may be prepared individually by use of a double-bladed cutter.
The cutting edges of the blades should be lubricated with a
material such as stearic acid in alcohol or other suitable
material. The finished specimens shall be examined under
about 20 3 magnification to ascertain that the edges are
smooth and that there are no surface scratches or creases.
FIG. 1 Schematic of Fatigue Ductility Flex Tester Showing
Specimens showing discernible surface scratches, creases, or
Principle of Operation
edge discontinuities shall be rejected.
7.2 Specimen Thickness—Specimen thickness shall be de-
termined in accordance with Test Methods E 345. The thick-
ness of each specimen may be determined by any suitable
means, provided that the thickness of each specimen is
measured to an accuracy of 2 %.
NOTE 4—For specimens for which the density is not known, for
example, plated foil, the thickness of the specimens will have to be
measured directly even for soft materials or materials thinner than 0.025
mm (0.001 in.).
NOTE 5—For specimens with rough surfaces, it is necessary to deter-
mine the minimum core thickness, that is, the specimen thickness without
the rough surface features, from a metallographic cross section, prepared
in accordance with Methods E 3.
7.3 Specimen Dimensions—The test specimens shall have
the following dimensions:
7.3.1 Width—2.5 to 7.5 mm (0.1 to 0.3 in.) with 3.2 mm
(0.125 in.) the preferred width.
7.3.2 Length—30 mm (1.2 in.) minimum.
7.4 Number of Specimens—It is recommended that at least
three specimens in both the main orientation direction (direc-
tion of rolling for wrought foil, direction of plating solution
FIG. 2 Fatigue Ductility Flex Tester, Model 2 FDF
agitation for plated foil) and the orthogonal direction be tested.
7.5 Mechanical Properties—For purposes of performing the
1 1
vertically a total of 38 63mm(1 ⁄2 6 ⁄8 in.) at 50 cycles/min.
test and calculating the fatigue ductility, it is desirable to have
The specimen, held in a horizontal position by six rollers and
available in both the main orientation direction and the
positioned between the two test mandrels, is subjected to cyclic
orthogonal direction the following mechanical properties, ob-
flexural strains by being bent alternately around the two test
tained in accordance with the applicable standards such as Test
mandrels. The precision test mandrels shall have uniform
Methods E 8, Test Method E 111, and Methods E 345: tensile
roundness, a maximum surface roughness height of 0.25 μm
yield strength, tensile strength, tensile fracture strength, and
(10 μin.), and a minimum surface hardness of 60 HRC. The
modulus of elasticity.
diamet
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