Standard Specification for Fully-Formulated Glycol Base Engine Coolant for Heavy-Duty Engines

ABSTRACT
This specification covers the requirements for fully-formulated glycol base coolants for cooling systems of heavy-duty engines. When concentrates are used at 40 to 60 % glycol concentration by volume in water of suitable quality, or when prediluted glycol base engine coolants (50 volume % minimum) are used without further dilution, they will function effectively during both winter and summer to provide protection against corrosion, cavitation, freezing, and boiling. The coolant concentrate mixed with water or the prediluted coolant, when maintained with maintenance doses of supplemental coolant additives (SCA), shall be suitable for use in a properly maintained cooling system in normal service for a minimum of two years. In addition, the coolant concentrate or prediluted coolant shall provide protection in operating engines against cavitation corrosion (also termed liner pitting) and against scaling of internal engine hot surfaces. Hot surfaces typically are within the engine head, head spacer, upper cylinder liner, or liquid cooled exhaust manifold.
SCOPE
1.1 This specification covers the requirements for fully-formulated glycol base coolants for cooling systems of heavy-duty engines. When concentrates are used at 40 to 60 % glycol concentration by volume in water of suitable quality, (see ), or when prediluted glycol base engine coolants (50 volume % minimum) are used without further dilution, they will function effectively during both winter and summer to provide protection against corrosion, cavitation, freezing, and boiling.
1.2 This specification is intended to cover the requirements for engine coolants prepared from virgin or recycled ethylene or propylene glycol.
Committee D15 has not substantially studied the impact of using recycled glycols from sources such as:  glycol bottoms polyester manufacturing waste aircraft and runway deicers medical waste to prepare engine coolants. However, several serious cases of very poor performance have been reported and substantiated in heavy duty fleets when recycled glycols from sources such as above have been used to prepare engine coolants. Efforts are underway to more clearly define the purity requirements for glycols used to prepare engine coolants meeting this specification, whether from recycled engine coolants or other sources.
1.3 The coolants governed by this specification are categorized as follows:Coolant TypeDescriptionI-FFEthylene glycol base concentrateII-FFPropylene glycol base concentrateIII-FFEthylene glycol predilute (50 vol %)IV-FFPropylene glycol predilute (50 vol %)
1.4 Coolant concentrates meeting this specification do not require any addition of Supplemental Coolant Additive (SCA) until the first maintenance interval when a maintenance dose of SCA is required to continue protection in certain heavy duty engine cooling systems, particularly those of the wet cylinder liner-in-block design. The SCA additions are defined by and are the primary responsibility of the engine manufacturer or vehicle manufacturer. If they provide no instructions, follow the SCA supplier's instructions.
1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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ASTM D6210-06 - Standard Specification for Fully-Formulated Glycol Base Engine Coolant for Heavy-Duty Engines
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 6210 – 06
Standard Specification for
Fully-Formulated Glycol Base Engine Coolant for Heavy-
,
1 2
Duty Engines
This standard is issued under the fixed designation D6210; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope liner-in-block design. The SCA additions are defined by and
are the primary responsibility of the engine manufacturer or
1.1 This specification covers the requirements for fully-
vehicle manufacturer. If they provide no instructions, follow
formulated glycol base coolants for cooling systems of heavy-
the SCA supplier’s instructions.
duty engines.When concentrates are used at 40 to 60% glycol
1.5 The values stated in SI units are to be regarded as
concentration by volume in water of suitable quality, (see
standard. The values given in parentheses are for information
Appendix X1), or when prediluted glycol base engine coolants
only.
(50 volume% minimum) are used without further dilution,
1.6 This standard does not purport to address all of the
theywillfunctioneffectivelyduringbothwinterandsummerto
safety concerns, if any, associated with its use. It is the
provide protection against corrosion, cavitation, freezing, and
responsibility of the user of this standard to establish appro-
boiling.
priate safety and health practices and determine the applica-
1.2 This specification is intended to cover the requirements
bility of regulatory limitations prior to use.
for engine coolants prepared from virgin or recycled ethylene
or propylene glycol.
2. Referenced Documents
3
NOTE 1—Committee D15 has not substantially studied the impact of
2.1 ASTM Standards:
using recycled glycols from sources such as:
D1126 Test Method for Hardness in Water
• glycol bottoms
D1293 Test Methods for pH of Water
• polyester manufacturing waste
D3306 Specification for Glycol Base Engine Coolant for
• aircraft and runway deicers
Automobile and Light-Duty Service
• medical waste
D4327 Test Method for Anions in Water by Chemically
to prepare engine coolants. However, several serious cases of very poor perfor-
Suppressed Ion Chromatography
mance have been reported and substantiated in heavy duty fleets when recycled
D5828 Test Method for Compatibility of Supplemental
glycols from sources such as above have been used to prepare engine coolants.
Efforts are underway to more clearly define the purity requirements for glycols
Coolant Additives (SCAs) and Engine Coolant Concen-
used to prepare engine coolants meeting this specification, whether from recycled
trates
engine coolants or other sources.
4
2.2 Other Standards:
1.3 The coolants governed by this specification are catego-
Federal Method 2540B Total Dissolved Solids Dried at
rized as follows:
103–105°C
Coolant Type Description
3. General Requirements
I-FF Ethylene glycol base concentrate
II-FF Propylene glycol base concentrate
3.1 Concentrated and prediluted coolants shall meet all of
III-FF Ethylene glycol predilute (50 vol %)
the respective requirements of Specification D3306.
IV-FF Propylene glycol predilute (50 vol %)
3.2 The coolant concentrate mixed with water or the predi-
1.4 Coolant concentrates meeting this specification do not
luted coolant, when maintained with maintenance doses of
require any addition of Supplemental CoolantAdditive (SCA)
SCAinaccordancewiththeenginemanufacturer’srecommen-
untilthefirstmaintenanceintervalwhenamaintenancedoseof
dations,andthoseontheproductlabel,shallbesuitableforuse
SCA is required to continue protection in certain heavy duty
in a properly maintained cooling system in normal service for
engine cooling systems, particularly those of the wet cylinder
a minimum of two years (see Appendix X1).
1 3
ThisspecificationisunderthejurisdictionofASTMCommitteeD15onEngine For referenced ASTM standards, visit the ASTM website, www.astm.org, or
CoolantsandisthedirectresponsibilityofSubcommitteeD15.07onSpecifications. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Current edition approved Aug. 1, 2006. PublishedAugust 2006. Originally Standards volume information, refer to the standard’s Document Summary page on
approved in 1998. Last previous edition approved in 2004 as D6210-04. the ASTM website.
2 4
Aresearch report is available fromASTM International Headquarters. Request Standard Method for the Examination of Water and Wastewater, American
RR:D15–1023. Public Health Association, et al, 1015 15th Street, N.W. Washington, DC 20005
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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