ASTM D5213-99
(Specification)Standard Specification for Polymeric Resin Film for Electrical Insulation and Dielectric Applications
Standard Specification for Polymeric Resin Film for Electrical Insulation and Dielectric Applications
SCOPE
1.1 This specification covers requirements for the material, dimensions and tolerances, and property values of film, in sheet or strip form, with or without heat-sealable coatings.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
General Information
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Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
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An American National Standard
Designation: D 5213 – 99
Standard Specification for
Polymeric Resin Film for Electrical Insulation and Dielectric
Applications
This standard is issued under the fixed designation D 5213; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 3.2.1 sheet, n—material greater than 75 mm in width.
3.2.2 strip, n—material 75 mm or less in width.
1.1 This specification covers requirements for the material,
dimensions and tolerances, and property values of film, in sheet
4. Classification
or strip form, with or without heat-sealable coatings.
4.1 This specification covers the following:
1.2 The values stated in SI units are to be regarded as the
4.1.1 Type I—General purpose,
standard. The values given in parentheses are for information
4.1.2 Type II—Heat sealable,
only.
4.1.2.1 Grade 1—One side coated, and
NOTE 1—This document is similar to IEC 60674, Part 3, Sheets 2, 4, 5,
4.1.2.2 Grade 2—Two sides coated.
6, and 7.
4.2 Materials:
4.2.1 Item A—Poly(N,N8-p,p8-oxydiphenylene pyromelliti-
2. Referenced Documents
mide),
2.1 ASTM Standards:
4.2.2 Item B—Poly(N,N8-p,p8-oxydiphenylene biphenyltet-
D 149 Test Method for Dielectric Breakdown Voltage and
racarboxylimide,
Dielectric Strength of Solid Electrical Insulating Materials
4.2.3 Item C—Poly(N,N8-p-phenylene biphenyltetracar-
at Commercial Power Frequencies
boxylimide),
D 883 Terminology Relating to Plastics
4.2.4 Item D—FEP-fluorocarbon, and
D 1711 Terminology Relating to Electrical Insulation
4.2.5 Item E—Polyethylene terephthalate.
D 2305 Test Methods for Polymeric Films Used for Elec-
4.2.6 Item F—Polyethylene naphthalate.
trical Insulation
D 3636 Practice for Sampling and Judging Quality of Solid
5. Ordering Information
Electrical Insulating Materials
5.1 Order the film covered by this specification stating the
D 4088 Practice for Preparation for Shipment of Solid
type, grade, class, thickness, width, and roll dimensions.
Electrical Insulating Materials
2.2 IEC Standards:
6. Materials
Publication 60674-3 Specification for Electrical Films for
6.1 Type I material is flexible, unsupported film.
Electrical Purposes
6.2 Type II material is film meeting all of the requirements
of Type I, and having a heat-sealable coating on one or both
3. Terminology
sides.
3.1 Definitions—Definitions are in accordance with Termi-
nologies D 1711 and D 883 unless otherwise specified.
7. Requirements
3.2 Definitions of Terms Specific to This Standard:
7.1 The film covered by this specification shall meet the
property requirements given in Tables 1-6 and Table 7 when
tested by the methods given in Test Methods D 2305.
This specification is under the jurisdiction of ASTM Committee D-9 on 7.1.1 Type II films, prior to coating, shall meet all of the
Electrical and Electronic Insulating Materials and is the direct responsibility of
requirements given in Table 1 for films of the thicknesses given
Subcommittee D09.07 on Flexible and Rigid Insulating Materials.
in Table 8.
Current edition approved March 10, 1999. Published June 1999. Orginally
7.1.2 Type II films, after coating, shall meet all of the
published as D 5213 – 91. Last previous edition D 5213 – 95.
Annual Book of ASTM Standards, Vol 10.01.
requirements given in Table 1 for elongation, before and after
Annual Book of ASTM Standards, Vol 08.01.
heating, and for shrinkage as given in Table 1 for films of the
Annual Book of ASTM Standards, Vol 10.02.
5 nd
thicknesses given in Table 8.
Available from American National Standards Institute, 4 W. 42 St., New York,
NY 10036. 7.2 Roll Diameters:
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D 5213
TABLE 1 Property Values for Type I, Class A Film poly(N,N*-p-p*-oxydiphenylene pyromellitimide)
Average Property Value
Nominal Thickness, μm (mils)
7.5 (0.3) 13 (0.5) 20 (0.8) 25 (1.0) 50 (2.0) 75 (3.0) 100 (4.0) 130 (5.0)
Tensile strength, min MPa (psi), 69 97 138 138 138 138 138 138
machine direction and transverse (10 000) (14 000) (20 000) (20 000) (20 000) (20 000) (20 000) (20 000)
direction
Elongation, min percent, machine 10 20 35 35 40 45 45 45
and transverse direction
Shrinkage, max percent, after . . 0.30 0.30 0.35 0.35 0.35 0.35
exposure to 200°C (392°F),
machine and transverse direction
Moisture absorption, max percent, 100 % RH 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0
Dielectric strength, min kV/mm 120 120 180 180 150 140 100 100
A,B
(V/mil), 60 Hz (3000) (3000) (4500) (4500) (3800) (3600) (2500) (2500)
B,C 15 15 15 15 15 15 15 15
Volume resistivity, min V-cm, 10 10 10 10 10 10 10 10
B
Permittivity, max at 1 kHz 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0
B
Dissipation factor, max at 1 kHz 0.007 0.005 0.005 0.004 0.004 0.004 0.004 0.004
A
Use Type 3 electrodes in air of Table 1 of Test Method D 149 (opposing 6.4-mm diameter rods).
B
At 23°C (73.4°F), 50 % RH.
C
The median value of 5 measurements should be used for compliance.
TABLE 2 Property Values for Type I, Class B Film poly(N,N*-p-p*-oxydiphenylene biphenyltetracarboxylimide)
Average Property Value
Nominal Thickness, μm (mils)
7.5 (0.3) 13 (0.5) 20 (0.8) 25 (1.0) 40 (1.6) 50 (2.0) 75 (3.0) 100 (4.0) 130 (5.0)
Tensile strength, min MPa (psi), 110 138 196 196 196 196 196 196 196
machine direction and transverse (15 000) (20 000) (28 000) (28 000) (28 000) (28 000) (28 000) (28 000) (28 000)
direction
Elongation, min percent, machine 24 40 80 80 80 80 80 80 80
and transverse direction
Shrinkage, max percent, after . . 0.30 0.30 0.35 0.35 0.35 0.35 0.35
exposure to 200°C (392°F),
machine and transverse direction
Moisture absorption, max percent, 100 % RH 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0
Dielectric strength, min kV/mm 120 120 180 180 150 140 130 100 95
A,B
(V/mil), 60 Hz (3000) (3000) (4500) (4500) (3800) (3500) (3300) (2500) (2400)
B,C 15 15 15 15 15 15 15 15 15
Volume resistivity, min V-cm, 10 10 10 10 10 10 10 10 10
B
Permittivity, max at 1 kHz 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0
B
Dissipation factor, max at 1 kHz 0.007 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005
A
Use Type 3 electrodes in air of Table 1 of Test Method D 149 (opposing 6.4-mm diameter rods).
B
At 23°C (73.4°F), 50 % RH.
C
The median value of 5 measurements should be used for compliance.
TABLE 3 Property Values for Type I, Class C Film poly(N,N*-p-phenylene biphenyltetracarboxylimide)
Average Property Value
Nominal Thickness, μm (mils)
7.5 (0.3) 13 (0.5) 20 (0.8) 25 (1.0) 40 (1.6) 50 (2.0) 75 (3.0) 100 (4.0) 130 (5.0)
Tensile strength, min MPa (psi), 133 176 241 241 241 241 241 241 241
machine direction and transverse (19 000) (25 000) (34 000) (34 000) (34 000) (34 000) (34 000) (34 000) (34 000)
direction
Elongation, min percent, machine 25 25 25 25 25 25 25 25 25
and transverse direction
Shrinkage, max percent, after . . 0.15 0.15 0.15 0.20 0.20 0.20 0.20
exposure to 200°C (392°F),
machine and transverse direction
Moisture absorption, max percent, 100 % RH 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8
Dielectric strength, min kV/mm 120 120 180 180 150 140 120 100 95
A,B
(V/mil), 60 Hz (3000) (3000) (4500) (4500) (3800) (3500) (3000) (2500) (2400)
B,C 15 15 15 15 15 15 15 15 15
Volume resistivity, min V-cm, 10 10 10 10 10 10 10 10 10
B
Permittivity, max at 1 kHz 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0
B
Dissipation factor, max at 1 kHz 0.007 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005
A
Use Type 3 electrodes in air of Table 1 of Test Method D 149 (opposing 6.4-mm diameter rods).
B
At 23°C (73.4°F), 50 % RH.
C
The median value of 5 measurements should be used for compliance.
7.2.1 The outside diameters of rolls of film shall not vary 7.2.2 The inside diameters of cores of standard rolls of film
from the value specified on the purchase order by more than shall not vary from the value specified on the purchase order by
66 mm (0.25 in.). more than6 1.5 mm (0.060 in.).
D 5213
TABLE 4 Property Values for Type I, Class D Film (FEP—Fluorocarbon)
Average Property Value
Nominal Thickness, μm (mils)
13 25 51 76 102 127 254 356 508 762 1016 1524 2413
(0.50) (1.0) (2.0) (3.0) (4.0) (5.0) (10.0) (14.0) (20.0) (30.0) (40.0) (60.0) (95.0)
Tensile strength, min MPa (psi), 13.8 17.25 17.25 17.25 17.25 17.25 17.25 17.25 17.25 17.25 17.25 17.25 17.25
machine direction and transverse (2000) (2500) (2500) (2500) (2500) (2500) (2500) (2500) (2500) (2500) (2500) (2500) (2500)
direction
Elongation, min, %, machine 175 250 250 250 250 250 250 250 250 250 250 250 250
direction and transverse
direction
Shrinkage, max percent, after 5.0 5.0 3.0 2.0 2.0 2.0 2.0 2.0 2.0 4.0 4.0 4.0 5.0
exposure to 200°C (392°F)
Moisture absorption, max percent, 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1
100 %, RH
Dielectric strength, min at 60 Hz 160 160 140 120 110 100 72 64 56 . . . .
A,B
kV/mm (V/mil) (4000) (4000) (3500) (3000) (2750) (2500) (1800) (1600) (1400)
B,C 17 17 17 17 17 17 17 17 17 17 17 17 17
Volume resistivity, min, V-cm 10 10 10 10 10 10 10 10 10 10 10 10 10
B
Permittivity, max at 1 kHz 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15
B
Dissipation factor, max at 1 kHz 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003
A
Use Type 3 electrodes in air of Table 1 of Test Method D 149 (opposing 6.4-mm diameter rods).
B
At 23°C (73.4°F), 50 % RH.
C
The median value of 5 measurements should be used for compliance.
TABLE 5 Property Values for Type I, Class E Film (Polyethylene Terephthalate)
Average Property Value
Nominal Thickness, μm (mils)
12 (0.48) 15 (0.60) 23 (0.92) 36 (1.42) 75 (3.00) 100 (4.00) 190 (7.50) 250 (10.00)
19 (0.75) 50 (2.00) 125 (5.00) 225 (9.00) >250
Tensile strength, min MPa (psi), 145 (21 000) 145 (21 000) 138 (20 000) 138 (20 000) 138 (20 000) 138 (20 000) 138 (20 000) 110
machine direction and transverse (16 000)
direction
Elongation, min % machine 60 60 65 70 70 70 70 70
direction and transverse direction
Shrinkage, max percent after 3.5 3.0 3.0 3.0 3.0 3.0 3.0 2.0
exposure to 150°C (302°F), 30 min
Moisture absorption, max %, 100 % RH 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8
Dielectric strength, min at 60 Hz, 208 (5300) 190 (4800) 174 (4400) 130 (3300) 105 (2700) 80 (2000) 60 (1500) 50 (1300)
A,B
kV/mm (V/mil)
B,C 15 15 15 15 15 15 15 15
Volume resistivity, min, V-cm 10 10 10 10 10 10 10 10
B
Permittivity, max at 1 kHz 3.5 3.5 3.5 3.5 3.5 3.5 3.5 3.5
B
Dissipation factor, max at 1 kHz 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006
A
Use Type 3 electrodes in air of Table 1 of Test Method D 149 (opposing 6.4-mm diameter rods).
B
At 23°C (73.4°F), 50 % RH.
C
The median value of 5 measurements should be used for compliance.
TABLE 6 Property Values for Type I, Class F Film (Polyethylene Naphthalate) Average Property Value
Nominal Thickness, μm (mils)
12 (0.48) 16 (0.65) 25 (1.00) 38 (1.50) 50 (2.00) 75 (3.00) 100 (4.00) - 250 (10.00)
Tensile strength, min MPa (psi), 172 (25 000) 172 (25 000) 172 (25 000) 172 (25 000) 172 (25 000) 172 (25 000) 172 (25 000)
machine direction and transverse
direction
Elongation, min percent, machine 50 50 50 50 50 50 50
and transverse direction
Shrinkage, max percent, after 2.00 2.00 2.00 2.00 2.00 2.00 2.00
exposure to 150°C (302°F), 30 min
Moisture absorption, max %, 0.6 0.6 0.6 0.6 0.6 0.6 0.6
at 100 % RH
Dielectric strength, min at 60 Hz, 215 (5500) 215 (5500) 195 (5000) 145 (3700) 145 (3700) 120 (3000) 120 (3000)
A,B
kV/mm (V/mil)
B,C 15 15 15 15 15 15 15
Volume resistivity, min, V-cm 10 10 10 10 10 10 10
ohm-cm
B
Permittivity, max at 1 kHz 3.4 3.4 3.4 3.4 3.4 3.4 3.4
B
Dissipation factor, max at 1 kHz 0.006 0.006 0.006 0.006 0.006 0.006 0.006
A
Use Type 3 electrodes in air of Table 1 of Test Method D 149 (opposing 6.4-mm diameter rods).
B
At 23°C (73.4°F), 50 % RH.
C
The median value of 5 measurements should be used for compliance.
D 5213
TABLE 7 Additional Property Values for Type II, Class A, B and C TABLE 9 Splice Tolerances for Standard Rolls of Type I Film
Films
Roll Diameter,
Nominal Thickness, μm (mils)
mm (in.)
Heat Seal Strength, min at
350°C 6 2°C (662 6 3.6°F)
Dielectric
7.5 13 20 25 40 50 75 100 130
Total Nominal
g/25 mm (in.) width ID OD
Strength, min
(0.3) (0.5) (0.8) (1.0) (1.6) (2.0) (3.0) (4.0) (5.0)
Grade Thickness
kV/mm
A Coated Side Coated Side
μm (mils)
Number of Splices per Roll, max
(V/mil)
to Uncoated to Coated
76 124 9 . . . . . . . .
Side Side
(3) (4.88)
1 25 (1.0) 120 (3000) 450 450 76 152 . 52221111
(3) (6)
1 38 (1.5) 140 (3500) 450 800
1 50 (2.0) 120 (3000) 450 800 76 241 . . 7755444
(3) (9.5)
1 60 (2.5) 100 (2500) 450 800
152 241 40 10 5553322
1 75 (3.0) 100 (2500) 450 800
B
(6) (9.5)
1 100 (4.0) 80 (2000) 450 800
C
Length Between Splices or From End of Roll, m (ft), min
1 100 (4.0) 105 (2700) 450 800
76 152 . 30 30 30 30 30 30 23 23
1 150 (6.0) 85 (2100) 450 800
(3) (6) (100) (100) (100) (100) (100) (100) (75) (75)
2 30 (1.2) 155 (3900) . 500
2 38 (1.5) 120 (3000) . 800 76 241 . . 30 30 30 30 30 23 23
(3) (9.5) (100) (100) (100) (100) (100) (75) (75)
2 50 (2.0) 120 (3000) . 800
D
2 75 (3.0) 100 (2500) . 800 152 241 23 30 30 30 30 30 30 23 23
C
(6) (9.5) (75) (100) (100) (100) (100) (100) (100) (75) (75)
2 75 (3.0) 80 (2000) . 600
A
Average Splice-Free Length per Roll, m (ft) , min
2 130 (5.0) 90 (2200) . 800
76 152 . 150 150 150 115 115 75 45 45
A
See Table 3A for nominal thicknesses of polyimide and FEP-Fluorocarbon
(3) (6) (500) (500) (500) (380) (380) (250) (150) (150)
layers.
76 241 . . 195 195 130 130 105 60 60
B
FEP-Fluorocarbon coating is 50 μm (2.0 mils) in nominal thickness.
(3) (9.5) (640) (640) (425) (425) (340) (200) (200)
C
FEP-Fluorocarbon coating is 25 μm (1.0 mils) in nominal thickness.
152 241 90 170 150 150 115 115 75 60 60
D
FEP-Fluorocarbon coating is 12 μm (0.5 mils) in nominal thickness.
(6) (9.5) (300) (550) (500) (500) (380) (380) (250) (200) (200)
A
Divide the length of the roll by the total number of splice-free segments.
TABLE 8 Thicknesses and Tolerances for Type II Class A, B and
C Films
TABLE 10 Splice Tolerances for Standard Rolls of Type II,
Nominal Thickness,μ m (mils) Tolerances
Grade 1 Film
on Total
Grade A
First FEP Polyimide Second
Thickness, Roll Diameter,
Total
Nominal Thickness, μm (mils)
A
Layer Layer FEP Layer
6μm (mils) mm (in.)
1 25 (1) None 13 (0.5) 13 (0.5) 6 (0.25) 25 38 50 63 75 100 150
ID OD
1 38 (1.5) None 25 (1) 13 (0.5) 6 (0.25) (1) (1.5) (2) (2.5) (3) (4) (6)
1 50 (2) None 25 (1) 25
...
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