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ASTM D802-97

(Test Method)

Standard Test Methods for Sampling and Testing Pine Oils

Standard Test Methods for Sampling and Testing Pine Oils

SCOPE
1.1 These test methods cover procedures for sampling and testing pine oils, and are applicable to both natural pine oils derived from pine stumps either by the steam and solvent process or by destructive distillation, and also to synthetic pine oils obtained by the chemical hydration of terpene hydrocarbons.
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.>

General Information

Status
Historical
Publication Date
09-Nov-1997
ICS
67.200.10 - Animal and vegetable fats and oils
87.060.20 - Binders
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.34 - Pine Chemicals and Hydrocarbon Resins
Current Stage
Ref Project

Relations

Replaced By
ASTM D802-02 - Standard Test Methods for Sampling and Testing Pine Oils
Effective Date
10-May-2002

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ASTM D802-97 - Standard Test Methods for Sampling and Testing Pine OilsASTM D802-97 - Standard Test Methods for Sampling and Testing Pine Oils
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ASTM D802-97 - Standard Test Methods for Sampling and Testing Pine Oils
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Standards Content (Sample)

Designation: D 802 – 97
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
Standard Test Methods for
1
Sampling and Testing Pine Oils
This standard is issued under the fixed designation D 802; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope chromatography is the accepted method for determining the
chemical composition of pine oil. An ASTM test method based
1.1 These test methods cover procedures for sampling and
on capillary gas chromatography can be used for the major
testing pine oils, and are applicable to both natural pine oils
components of pine oil. A capillary GC procedure is currently
derived from pine stumps either by the steam and solvent
being written which is suitable for both major and minor
process or by destructive distillation, and also to synthetic pine
components.
oils obtained by the chemical hydration of terpene hydrocar-
bons.
4. Sampling
1.2 The procedures given in these test methods appear in the
4.1 Sample the material in accordance with the procedure
following order:
described in Guide D 268 and Practice E 300.
Section
Sampling 4
5. Appearance
Appearance 5
Color 6
5.1 Examine a portion of the sample after agitation to
Specific Gravity 7
determine its clarity and freedom from foreign matter and
Refractive Index 8
Composition 9
separated water.
Moisture 10
6. Color
1.3 This standard does not purport to address all of the
6.1 Compare the color of the sample in any suitable or
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro- designated apparatus with the accepted or specified color
standard.
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
7. Specific Gravity
2. Referenced Documents
7.1 Determine the specific gravity at 15.6/15.6°C by any
convenient method, reporting the value to the nearest 0.0005.
2.1 ASTM Standards:
(A pycnometer or specific gravity balance is recommended. A
D 268 Guide for Sampling and Testing Volatile Solvents
hydrometer should not be used, on account of errors caused by
and Chemical Intermediates for Use in Paint and Related
2
surface tension on the hydrometer stem.) Correct determina-
Coatings and Materials
3
tions made at any other temperature, using apparatus standard-
D 803 Test Methods for Testing Tall Oil
3
ized at 15.6°C by adding to or subtracting from the observed
D 890 Test Method for Water in Liquid Naval Stores
reading 0.00080 for each degree Celsius that the temperature of
D 3009 Test Method for Compositon of Turpentine by Gas
3
the liquid is above or below 15.6°C.
Chromatography
4
E 300 Practice for Sampling Industrial Chemicals
8. Refractive Index
3. Significance and Use
8.1 Determine the refractive index with an instrument hav-
ing a resolution of 6 0.0001 at 20°C, if possible. If tested at
3.1 The testing procedures described in these test methods
have been in use for many years and emphasize the physical any other temperature, correct the reading obtained to 20°C
...

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3.1 The testing procedures described in these test methods have been in use for many years and emphasize the physical properties of pine oil rather than its chemical composition. Test Methods D6387 describe a capillary gas chromatography method which is suitable for determining both the major and minor components found in pine oils.
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1.1 These test methods cover procedures for sampling and testing pine oils, and are applicable to both natural pine oils derived from pine stumps either by the steam and solvent process or by destructive distillation, and also to synthetic pine oils obtained by the chemical hydration of terpene hydrocarbons.  
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1.1 These test methods cover procedures for sampling and testing pine oils, and are applicable to both natural pine oils derived from pine stumps either by the steam and solvent process or by destructive distillation, and also to synthetic pine oils obtained by the chemical hydration of terpene hydrocarbons.  
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