ASTM D1900-06(2015)
(Practice)Standard Practice for Carbon Black—Sampling Bulk Shipments
Standard Practice for Carbon Black—Sampling Bulk Shipments
SIGNIFICANCE AND USE
3.1 Sampling of bulk shipments of carbon blacks is of utmost importance since the location and number of samples taken by different laboratories can have a significant effect on the agreement of test values obtained. This practice is for use in obtaining representative samples of carbon black in each compartment or in the entire hopper car or hopper truck. These samples may be used to ascertain the average quality or the uniformity of a shipment, or both.
SCOPE
1.1 This practice covers procedures for the sampling and data reporting of bulk shipments of carbon black in three-compartment hopper rail cars and compartmented bulk hopper trailers.
Note 1: The tests to be made on the samples obtained by this practice, how many samples are taken, where they are taken, and what statistical values (if any) to report shall be determined by agreement between the purchaser and the manufacturer. This practice gives guidance for use in developing such agreements or for use when no formal agreement exists. The specific details of each procedure are described in appropriate ASTM test methods used for testing carbon black.
Note 2: Some purchasers or manufacturers may consider Flexible Intermediate Bulk Containers (FIBC) to be a bulk shipment. See Practice D1799 for guidance on sampling and reporting for this package.
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D1900 − 06 (Reapproved 2015)
Standard Practice for
1
Carbon Black—Sampling Bulk Shipments
This standard is issued under the fixed designation D1900; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope the agreement of test values obtained. This practice is for use
in obtaining representative samples of carbon black in each
1.1 This practice covers procedures for the sampling and
compartment or in the entire hopper car or hopper truck. These
data reporting of bulk shipments of carbon black in three-
samples may be used to ascertain the average quality or the
compartment hopper rail cars and compartmented bulk hopper
uniformity of a shipment, or both.
trailers.
NOTE 1—The tests to be made on the samples obtained by this practice,
4. Sampling Procedure
how many samples are taken, where they are taken, and what statistical
3
4.1 Withdraw approximatelya4dm (1 gal) sample from
values (if any) to report shall be determined by agreement between the
3
purchaser and the manufacturer. This practice gives guidance for use in each sample port, after first withdrawing at least 4 dm (1 gal)
developing such agreements or for use when no formal agreement exists.
of carbon black from each port and discarding it. Sample ports
The specific details of each procedure are described in appropriateASTM
are located on each side of each compartment in a three-
test methods used for testing carbon black.
compartment bulk hopper rail car and on one side of a hopper
NOTE 2—Some purchasers or manufacturers may consider Flexible
truck.
Intermediate Bulk Containers (FIBC) to be a bulk shipment. See Practice
D1799 for guidance on sampling and reporting for this package.
4.2 If sampling from the top ports of a hopper car or hopper
1.2 The values stated in SI units are to be regarded as
truck, approximately 150 mm (6 in.) of surface material should
3
standard. The values given in parentheses are for information
be raked aside before collecting approximately 4 dm (1 gal)
only.
for testing.
1.3 This standard does not purport to address all of the
4.3 Asample thief may be used to sample from the top ports
safety concerns, if any, associated with its use. It is the
of a hopper car or hopper truck. The thief must be able to
responsibility of the user of this standard to establish appro-
sample at least 150 mm (6 in.) below the surface. Collect
3
priate safety and health practices and determine the applica-
approximately 4 dm (1 gal) for testing.
bility of regulatory limitations prior to use.
4.4 If sampling a hopper car or hopper truck during unload-
ing it is recommended that three samples be collected for
2. Referenced Documents
testing from each compartment: one at the beginning of
2
2.1 ASTM Standards:
unloading, one at approximately the middle of unloading, and
D1799 Practice for Carbon Black—Sampling Packaged
one near the end of unloading. The sample size should be
Shipments
3
approximately 4 dm (1 gal).
D5817 Practice for Carbon Black, Pelleted—Reduction,
4.5 If sampling a hopper car or hopper truck during loading
Blending, and Drying of Gross Samples for Testing
it is recommended that three samples be collected for testing
3. Significance and Use
from each compartment: one at the beginning of loading, one
at approximately the middle of loading and one near the end of
3.1 Sampling of bulk shipments of carbon blacks is of
3
loading. The sample size should be approximately 4 dm
utmost importance since the location and number of samples
(1 gal).
taken by different laboratories can have a significant effect on
4.6 Samples collected as described in 4.1 – 4.5 may be
tested singly or composited. See Practice D5817 for guidance
1
This practice is under the jurisdiction of ASTM Committee D24 on Carbon
Black and is the direct responsibility of Subcommittee D24.61 on Carbon Black on preparing composited samples. When disputed test results
Sampling and Statistical Analysis.
arise reasonable efforts should be made for all parties to test
Current edition approved Nov. 1, 2015. Published December 2015. Originally
samples taken from the same location.
approved in 1961. Last previous edition approved in 2011 as D1900 – 06(2011).
DOI: 10.1520/D1900-06R15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 5. Sample Preparation and Handling
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
5.1 Store the samples in airtight containers until the mate-
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. rials are needed for sample preparation or te
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D1900 − 06 (Reapproved 2011) D1900 − 06 (Reapproved 2015)
Standard Practice for
1
Carbon Black—Sampling Bulk Shipments
This standard is issued under the fixed designation D1900; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice covers procedures for the sampling and data reporting of bulk shipments of carbon black in three-compartment
hopper rail cars and compartmented bulk hopper trailers.
NOTE 1—The tests to be made on the samples obtained by this practice, how many samples are taken, where they are taken, and what statistical values
(if any) to report shall be determined by agreement between the purchaser and the manufacturer. This practice gives guidance for use in developing such
agreements or for use when no formal agreement exists. The specific details of each procedure are described in appropriate ASTM test methods used for
testing carbon black.
NOTE 2—Some purchasers or manufacturers may consider Flexible Intermediate Bulk Containers (FIBC) to be a bulk shipment. See Practice D1799
for guidance on sampling and reporting for this package.
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D1799 Practice for Carbon Black—Sampling Packaged Shipments
D5817 Practice for Carbon Black, Pelleted—Reduction, Blending, and Drying of Gross Samples for Testing
3. Significance and Use
3.1 Sampling of bulk shipments of carbon blacks is of utmost importance since the location and number of samples taken by
different laboratories can have a significant effect on the agreement of test values obtained. This practice is for use in obtaining
representative samples of carbon black in each compartment or in the entire hopper car or hopper truck. These samples may be
used to ascertain the average quality or the uniformity of a shipment, or both.
4. Sampling Procedure
3 3
4.1 Withdraw approximately a 4 dm (1 gal) sample from each sample port, after first withdrawing at least 4 dm (1 gal) of
carbon black from each port and discarding it. Sample ports are located on each side of each compartment in a three-compartment
bulk hopper rail car and on one side of a hopper truck.
4.2 If sampling from the top ports of a hopper car or hopper truck, approximately 150 mm (6 in.) of surface material should
3
be raked aside before collecting approximately 4 dm (1 gal) for testing.
4.3 A sample thief may be used to sample from the top ports of a hopper car or hopper truck. The thief must be able to sample
3
at least 150 mm (6 in.) below the surface. Collect approximately 4 dm (1 gal) for testing.
4.4 If sampling a hopper car or hopper truck during unloading it is recommended that three samples be collected for testing from
each compartment: one at the beginning of unloading, one at approximately the middle of unloading, and one near the end of
3
unloading. The sample size should be approximately 4 dm (1 gal).
1
This practice is under the jurisdiction of ASTM Committee D24 on Carbon Black and is the direct responsibility of Subcommittee D24.61 on Carbon Black Sampling
and Statistical Analysis.
Current edition approved May 1, 2011Nov. 1, 2015. Published July 2011December 2015. Originally approved in 1961. Last previous edition approved in 20062011 as
D1900 – 06.D1900 – 06(2011). DOI: 10.1520/D1900-06R11.10.1520/D1900-06R15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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D1900 − 06 (2015)
4.5 If sampling a hopper car or hopper truck during loading it is recommended that three samples be collected for testing from
each compartment: one at the beginning of loadin
...
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