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ASTM D3520-04

(Test Method)

Standard Test Method for Quenching Time of Heat-Treating Fluids (Magnetic Quenchometer Method) (Withdrawn 2008)

Standard Test Method for Quenching Time of Heat-Treating Fluids (Magnetic Quenchometer Method) (Withdrawn 2008)

SIGNIFICANCE AND USE
The results obtained by the test method described are useful as guides in selecting fluids with respect to quenching speed characteristics desired for metal quenching applications.
Note 3—Although this test method has been found useful for some water-based fluids, the statistical significance of the test has been established only by round-robin testing of petroleum-based fluids.
These results will provide a measure of quenching speed (cooling rate) from approximately 885°C (1625°F) to 354°C (670°F) and are not directly proportional to hardness obtainable on metals quenched therein as many other factors are involved in the quenching process in actual plant operation with production parts.
Note 4—Test Method D 6200 describes the equipment and procedure for characterizing the time-temperature performance of a quenching oil through the entire cooling process.
FIG. 1 Magnetic Quenchometer
FIG. 2 Test Sequence in Beaker
SCOPE
1.1 This test method covers a procedure for making a comparative evaluation of the quenching speed characteristics of petroleum fluids used in the quenching of metals by means of the Magnetic Quenchometer.
Note 1—A comparison method for testing the hardenability of steel is Test Method A 255.
Note 2—An additional comparison method for evaluation of the quenching speed characteristics of petroleum fluids used in the quenching of metals is Test Method D 6200.
1.2 This test method provides a measure of changes in oil chemistry due to contamination, base oil degradation, and additive drag-out during use. This test measures changes in the quenching speed characteristics of petroleum fluids at the high temperature (>354°C). This test method does not reliably predict metallurgical performance.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to use.
WITHDRAWN RATIONALE
This test method covers a procedure for making a comparative evaluation of the quenching speed characteristics of petroleum fluids used in the quenching of metals by means of the Magnetic Quenchometer.
Formerly under the jurisdiction of Committee D02 on Petroleum Products and Lubricants, this test method was withdrawn in November 2008.
This test method is being withdrawn without replacement since equipment and materials used in the standard are no longer available from any commercial supplier.

General Information

Status
Historical
Publication Date
30-Apr-2004
ICS
75.100 - Lubricants, industrial oils and related products
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.L0.06 - Non-Lubricating Process Fluids
Current Stage
Ref Project

Relations

Replaces
ASTM D3520-88(1998) - Standard Test Method for Quenching Time of Heat-Treating Fluids (Magnetic Quenchometer Method) (Withdrawn 2008)
Effective Date
01-May-2004

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ASTM D3520-04 - Standard Test Method for Quenching Time of Heat-Treating Fluids (Magnetic Quenchometer Method) (Withdrawn 2008)ASTM D3520-04 - Standard Test Method for Quenching Time of Heat-Treating Fluids (Magnetic Quenchometer Method) (Withdrawn 2008)
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ASTM D3520-04 - Standard Test Method for Quenching Time of Heat-Treating Fluids (Magnetic Quenchometer Method) (Withdrawn 2008)
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation:D3520–04
Standard Test Method for
Quenching Time of Heat-Treating Fluids (Magnetic
1
Quenchometer Method)
This standard is issued under the fixed designation D3520; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope Petroleum Products (Hydrometer Method)
D445 Test Method for Kinematic Viscosity of Transparent
1.1 This test method covers a procedure for making a
and Opaque Liquids (the Calculation of Dynamic Viscos-
comparative evaluation of the quenching speed characteristics
ity)
of petroleum fluids used in the quenching of metals by means
D484 Specification for Hydrocarbon Drycleaning Sol-
of the Magnetic Quenchometer.
3
vents
NOTE 1—Acomparison method for testing the hardenability of steel is
D1218 Test Method for Refractive Index and Refractive
Test Method A255.
Dispersion of Hydrocarbon Liquids
NOTE 2—An additional comparison method for evaluation of the
D1744 Test Method for Water in Liquid Petroleum Prod-
quenching speed characteristics of petroleum fluids used in the quenching
3
ucts by Karl Fischer Reagent
of metals is Test Method D6200.
D6200 Test Method for Determining Cooling Characteris-
1.2 This test method provides a measure of changes in oil
tics of Quench Oils by Cooling Curve Analysis
chemistry due to contamination, base oil degradation, and
additivedrag-outduringuse.Thistestmeasureschangesinthe
3. Summary of Test Method
quenching speed characteristics of petroleum fluids at the high
3.1 This test method determines the time for cooling a
temperature (>354°C). This test method does not reliably
chromized nickel ball from approximately 885°C (1625°F) to
predict metallurgical performance.
approximately 354°C (670°F) when quenched in 200 mL of
1.3 This standard does not purport to address all of the
test fluid in a metal beaker at 21 to 27°C (70 to 81°F). The
safety concerns, if any, associated with its use. It is the
quenching time is recorded by a digital timer which is
responsibility of the user of this standard to establish appro-
energized by a photoelectric cell from light produced by the
priate safety and health practices and determine the applica-
ball at 885°C (1625°F) and which is stopped when the ball
bility of regulatory requirements prior to use.
becomes magnetic (Curie Point, approximately 354°C) and is
attracted by a magnet to the side of the beaker, tripping a relay
2. Referenced Documents
to stop the timer.
2
2.1 ASTM Standards:
A255 Test Method for End-Quench Test for Hardenability
4. Significance and Use
of Steel
4.1 The results obtained by the test method described are
D91 Test Method for Precipitation Number of Lubricating
useful as guides in selecting fluids with respect to quenching
Oils
speed characteristics desired for metal quenching applications.
D92 Test Method for Flash and Fire Points by Cleveland
NOTE 3—Although this test method has been found useful for some
Open Cup Tester
water-based fluids, the statistical significance of the test has been
D97 Test Method for Pour Point of Petroleum Products
established only by round-robin testing of petroleum-based fluids.
D287 TestMethodforAPIGravityofCrudePetroleumand
4.2 Theseresultswillprovideameasureofquenchingspeed
(cooling rate) from approximately 885°C (1625°F) to 354°C
1
This test method is under the jurisdiction of ASTM Committee D02 on
(670°F) and are not directly proportional to hardness obtain-
PetroleumProductsandLubricantsandisthedirectresponsibilityofSubcommittee
able on metals quenched therein as many other factors are
D02.L0 on Industrial Lubricants.
involved in the quenching process in actual plant operation
Current edition approved May 1, 2004. Published June 2004. Originally
with production parts.
approved in 1976. Withdrawn November 2003 and reinstated as D3520–04.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
3
the ASTM website. Withdrawn.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D3520–04
FIG. 1 Magnetic Quenchometer
connected controller near the heating elements can be used to minimize
temperature overrides, or both may be used. Further, 1 by 2 by 3-in. heat
sinks can be placed next to the area where the ball is to be placed to act
as heat shields and provide a more uniform temperature in this particular
area.
6. Materials
4
6.1 Ball, Chromized N
...

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Standard Test Method for Determination of Glycol for In-Service Engine Oils by Gas Chromatography

SIGNIFICANCE AND USE
5.1 Some glycol/antifreeze dilution of in-service engine oil is normal under typical operating conditions. However, excessive glycol dilution can lead to decreased performance, premature wear, or sudden engine failure. This test method provides a means of quantifying the level of glycol based antifreeze dilution, allowing the user to take necessary action.
SCOPE
1.1 This test method covers the determination of glycol based antifreeze for in-service engine oil by derivative headspace/gas chromatography.  
1.2 Sample is derivatized in-situ directly in a headspace sampling vial prior to vapor phase extraction and injection into a gas chromatograph.  
1.3 The chemistry of the derivatization is unique to the detection of the molecules of ethylene glycol and 1,2-propylene glycol. 1,3-propylene glycol could also be detected but is not used in any known anti-freeze at this time. Other coolant analyses are beyond the scope of this test method.  
1.4 The derivatization process does not affect glycol breakdown products such as glycolate and formate and hence the presence of these compounds in the oil will not be quantified.  
1.5 The test method concentration range is from 50 µg/g to 1000 µg/g. Lower levels are possible by method modifications. Higher levels are possible through sample dilution.  
1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
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  • Standard
    8 pages
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ASTM
ASTM D7918-23(Test Method)
Standard Test Method for Measurement of Flow Properties and Evaluation of Wear, Contaminants, and Oxidative Properties of Lubricating Grease by Die Extrusion Method and Preparation

SIGNIFICANCE AND USE
5.1 Trending the wear, contamination, consistency, and oxidative properties of a lubricating grease is a crucial part of condition-monitoring programs. Changes in these properties or deviations from the new grease can be indicative of problems within the lubricated component, such as the mixing of incompatible thickener types, excessive wear or contaminant levels, or significant depletion of antioxidant levels. These test methods also makes it possible to develop trends that can be used to predict failures before they occur and allow for corrective action to be taken.
SCOPE
1.1 This test method covers the determination and evaluation of flow properties, wear levels, contaminants, and oxidative condition of new and in-service lubricating grease.  
1.2 This test method provides guidance on evaluating in-service grease samples, NLGI grades 00 to 3, for wear, consistency, contamination, and oxidation.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3.1 Exception—The exception to this will be where units of references were developed by the developers of the test equipment and necessary to report the results of the test.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    9 pages
    English language
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  • Standard
    9 pages
    English language
    sale 15% off