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ASTM F3001-14

(Specification)

Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion

Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion

ABSTRACT
This specification establishes the requirements for additively manufactured titanium-6aluminum-4vanadium with extra low interstitials (Ti-6Al-4V ELI) components using full-melt powder bed fusion such as electron beam melting and laser melting. The standard covers the classification of materials, ordering information, manufacturing plan, feedstock, process, chemical composition, microstructure, mechanical properties, thermal processing, hot isostatic pressing, dimensions and mass, permissible variations, retests, inspection, rejection, certification, product marking and packaging, and quality program requirements.
SCOPE
1.1 This specification covers additively manufactured titanium-6aluminum-4vanadium with extra low interstitials (Ti-6Al-4V ELI) components using full-melt powder bed fusion such as electron beam melting and laser melting. The components produced by these processes are used typically in applications that require mechanical properties similar to machined forgings and wrought products. Components manufactured to this specification are often, but not necessarily, post processed via machining, grinding, electrical discharge machining (EDM), polishing, and so forth to achieve desired surface finish and critical dimensions.  
1.2 This specification is intended for the use of purchasers or producers or both of additively manufactured Ti-6Al-4V ELI components for defining the requirements and ensuring component properties.  
1.3 Users are advised to use this specification as a basis for obtaining components that will meet the minimum acceptance requirements established and revised by consensus of the members of the committee.  
1.4 User requirements considered more stringent may be met by the addition to the purchase order of one or more supplementary requirements, which may include, but are not limited to, those listed in S1-S4 and S1-S16 in Specification F2924.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

General Information

Status
Historical
Publication Date
31-Jan-2014
ICS
77.120.50 - Titanium and titanium alloys
Technical Committee
F42 - Additive Manufacturing Technologies
Drafting Committee
F42.05 - Materials and Processes
Current Stage
Ref Project

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ASTM F3001-14 - Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed FusionASTM F3001-14 - Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion
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REDLINE ASTM F3001-14 - Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed FusionREDLINE ASTM F3001-14 - Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion
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REDLINE ASTM F3001-14 - Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:F3001 −14
Standard Specification for
Additive Manufacturing Titanium-6 Aluminum-4 Vanadium
1
ELI (Extra Low Interstitial) with Powder Bed Fusion
This standard is issued under the fixed designation F3001; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope B243 Terminology of Powder Metallurgy
B600 Guide for Descaling and Cleaning Titanium and Tita-
1.1 This specification covers additively manufactured
nium Alloy Surfaces
titanium-6aluminum-4vanadium with extra low interstitials
B769 Test Method for Shear Testing of Aluminum Alloys
(Ti-6Al-4V ELI) components using full-melt powder bed
D3951 Practice for Commercial Packaging
fusion such as electron beam melting and laser melting. The
E3 Guide for Preparation of Metallographic Specimens
components produced by these processes are used typically in
E8/E8M Test Methods for Tension Testing of Metallic Ma-
applications that require mechanical properties similar to
terials
machined forgings and wrought products. Components manu-
E9 Test Methods of Compression Testing of Metallic Mate-
factured to this specification are often, but not necessarily, post
rials at Room Temperature
processed via machining, grinding, electrical discharge ma-
E11 Specification for Woven Wire Test Sieve Cloth and Test
chining (EDM), polishing, and so forth to achieve desired
Sieves
surface finish and critical dimensions.
E29 Practice for Using Significant Digits in Test Data to
1.2 This specification is intended for the use of purchasers
Determine Conformance with Specifications
or producers or both of additively manufactured Ti-6Al-4V
E238 Test Method for Pin-Type Bearing Test of Metallic
ELI components for defining the requirements and ensuring
Materials
component properties.
E407 Practice for Microetching Metals and Alloys
1.3 Users are advised to use this specification as a basis for
E539 TestMethodforAnalysisofTitaniumAlloysbyX-Ray
obtaining components that will meet the minimum acceptance
Fluorescence Spectrometry
requirements established and revised by consensus of the
E1409 Test Method for Determination of Oxygen and Nitro-
members of the committee.
gen in Titanium and TitaniumAlloys by Inert Gas Fusion
1.4 User requirements considered more stringent may be E1447 Test Method for Determination of Hydrogen in Tita-
met by the addition to the purchase order of one or more nium and Titanium Alloys by Inert Gas Fusion Thermal
supplementary requirements, which may include, but are not Conductivity/Infrared Detection Method
limited to, those listed in S1-S4 and S1-S16 in Specification E1820 Test Method for Measurement of Fracture Toughness
F2924.
E1941 Test Method for Determination of Carbon in Refrac-
tory andReactive Metals andTheirAlloys byCombustion
1.5 The values stated in SI units are to be regarded as
Analysis
standard. No other units of measurement are included in this
E2371 Test Method for Analysis of Titanium and Titanium
standard.
Alloys by Direct Current Plasma and Inductively Coupled
2. Referenced Documents
Plasma Atomic Emission Spectrometry (Performance-
2
Based Test Methodology)
2.1 ASTM Standards:
F136 Specification for Wrought Titanium-6Aluminum-
B214 Test Method for Sieve Analysis of Metal Powders
4Vanadium ELI (Extra Low Interstitial)Alloy for Surgical
Implant Applications (UNS R56401)
1
This specification is under the jurisdiction of ASTM Committee F42 on
F2792 Terminology for Additive Manufacturing
Additive Manufacturing Technologies and is the direct responsibility of Subcom-
,
mittee F42.05 on Materials and Processes.
Technologies
Current edition approved Feb. 1, 2014. Published March 2014. Originally
F2924 Specification for Additive Manufacturing Titanium-6
approved in 2013. Last previous edition approved in 2013 as F3001-13. DOI:
Aluminum-4 Vanadium with Powder Bed Fusion
10.1520/F3001-14
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 2
2.2 ISO/ASTM Standards:
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
52915 Specification forAdditive Manufacturing File Format
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. (AMF) Version 1.1
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
F3001−14
52921 Terminology for Additive Manufacturing— 4.1.6 Class F components shall be stress relieved or an-
Coordinate Systems and Test Methodologies nealed per Section 12.
3
2.3 ASQ Standard:
ASQ C1 Specification of General Requirements for a Qual- 5.
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: F3001 − 13 F3001 − 14
Standard Specification for
Additive Manufacturing Titanium-6 Aluminum-4 Vanadium
1
ELI (Extra Low Interstitial) with Powder Bed Fusion
This standard is issued under the fixed designation F3001; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers additively manufactured titanium-6aluminum-4vanadium with extra low interstitials (Ti-6Al-4V
ELI) components using full-melt powder bed fusion such as electron beam melting and laser melting. The components produced
by these processes are used typically in applications that require mechanical properties similar to machined forgings and wrought
products. Components manufactured to this specification are often, but not necessarily, post processed via machining, grinding,
electrical discharge machining (EDM), polishing, and so forth to achieve desired surface finish and critical dimensions.
1.2 This specification is intended for the use of purchasers or producers or both of additively manufactured Ti-6Al-4V ELI
components for defining the requirements and ensuring component properties.
1.3 Users are advised to use this specification as a basis for obtaining components that will meet the minimum acceptance
requirements established and revised by consensus of the members of the committee.
1.4 User requirements considered more stringent may be met by the addition to the purchase order of one or more
supplementary requirements, which may include, but are not limited to, those listed in S1-S4 and S1-S12S1-S16 in Specification
F2924.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
2. Referenced Documents
2
2.1 ASTM Standards:
B214 Test Method for Sieve Analysis of Metal Powders
B243 Terminology of Powder Metallurgy
B600 Guide for Descaling and Cleaning Titanium and Titanium Alloy Surfaces
B769 Test Method for Shear Testing of Aluminum Alloys
D3951 Practice for Commercial Packaging
E3 Guide for Preparation of Metallographic Specimens
E8/E8M Test Methods for Tension Testing of Metallic Materials
E9 Test Methods of Compression Testing of Metallic Materials at Room Temperature
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E238 Test Method for Pin-Type Bearing Test of Metallic Materials
E407 Practice for Microetching Metals and Alloys
E539 Test Method for Analysis of Titanium Alloys by X-Ray Fluorescence Spectrometry
E1409 Test Method for Determination of Oxygen and Nitrogen in Titanium and Titanium Alloys by Inert Gas Fusion
E1447 Test Method for Determination of Hydrogen in Titanium and Titanium Alloys by Inert Gas Fusion Thermal
Conductivity/Infrared Detection Method
E1820 Test Method for Measurement of Fracture Toughness
E1941 Test Method for Determination of Carbon in Refractory and Reactive Metals and Their Alloys by Combustion Analysis
1
This specification is under the jurisdiction of ASTM Committee F42 on Additive Manufacturing Technologies and is the direct responsibility of Subcommittee F42.05
on Materials and Processes.
Current edition approved April 1, 2013Feb. 1, 2014. Published April 2013March 2014. Originally approved in 2013. Last previous edition approved in 2013 as F3001-13.
DOI: 10.1520/F3001-1310.1520/F3001-14
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
F3001 − 14
E2371 Test Method for Analysis of Titanium and Titanium Alloys by Direct Current Plasma and Inductively Coupled Plasma
Atomic Emission Spectrometry (Performance-Based Test Methodology)
F136 Specification for Wrought Titanium-6Aluminum-4Vanadium ELI (Extra Low Interstitial) Alloy for Surgical Implant
Applications (UNS R56401)
,
F2792 Terminology for Additive Manufacturing Technologies
F2921 Terminology for Additive Manufacturing—Coordinate Systems and Test Methodologies
F2924 Specification for Addi
...

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5.1 This test method for the chemical analysis of titanium and titanium alloys is primarily intended to test material for compliance with specifications of chemical composition such as those under the jurisdiction of ASTM Committee B10. It may also be used to test compliance with other specifications that are compatible with the test method.  
5.2 It is assumed that all who use this test method will be trained analysts capable of performing common laboratory procedures skillfully and safely and that the work will be performed in a properly equipped laboratory.  
5.3 This is a performance-based test method that relies more on the demonstrated quality of the test result than on strict adherence to specific procedural steps. It is expected that laboratories using this test method will prepare their own work instructions. These work instructions will include detailed operating instructions for the specific laboratory, the specific reference materials used, and performance acceptance criteria. It is also expected that, when applicable, each laboratory will participate in proficiency test programs, such as described in Practice E2027, and that the results from the participating laboratory will be satisfactory.
SCOPE
1.1 This method describes the analysis of titanium and titanium alloys, such as specified by committee B10, by inductively coupled plasma atomic emission spectrometry (ICP-AES) and direct current plasma atomic emission spectrometry (DCP-AES) for the following elements:    
Element  
Application
Range (wt.%)  
Quantitative
Range (wt.%)  
Aluminum  
0–8  
0.009 to 8.0  
Boron  
0–0.04  
0.0008 to 0.01  
Cobalt  
0-1  
0.006 to 0.1  
Chromium  
0–5  
0.005 to 4.0  
Copper  
0–0.6  
0.004 to 0.5  
Iron  
0–3  
0.004 to 3.0  
Manganese  
0–0.04  
0.003 to 0.01  
Molybdenum  
0–8  
0.004 to 6.0  
Nickel  
0–1  
0.001 to 1.0  
Niobium  
0-6  
0.008 to 0.1  
Palladium  
0-0.3  
0.02 to 0.20  
Ruthenium  
0-0.5  
0.004 to 0.10  
Silicon  
0–0.5  
0.02 to 0.4  
Tantalum  
0-1  
0.01 to 0.10  
Tin  
0–4  
0.02 to 3.0  
Tungsten  
0-5  
0.01 to 0.10  
Vanadium  
0–15  
0.01 to 15.0  
Yttrium  
0–0.04  
0.001 to 0.004  
Zirconium  
0–5  
0.003 to 4.0  
1.2 This test method has been interlaboratory tested for the elements and ranges specified in the quantitative range part of the table in 1.1. It may be possible to extend this test method to other elements or broader mass fraction ranges as shown in the application range part of the table above provided that test method validation is performed that includes evaluation of method sensitivity, precision, and bias. Additionally, the validation study shall evaluate the acceptability of sample preparation methodology using reference materials or spike recoveries, or both. Guide E2857 provides information on validation of analytical methods for alloy analysis.  
1.3 Because of the lack of certified reference materials (CRMs) containing bismuth, hafnium, and magnesium, these elements were not included in the scope or the interlaboratory study (ILS). It may be possible to extend the scope of this test method to include these elements provided that method validation includes the evaluation of method sensitivity, precision, and bias during the development of the testing method.  
1.4 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific safety hazards statements are given in Section 9.  
1.6 This international standard was developed in accordance with internationally recognized principle...

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ASTM
ASTM D6906-12a(2021)(Test Method)
Standard Test Method for Determination of Titanium Treatment Weight on Metal Substrates by Wavelength Dispersive X-Ray Fluorescence

SIGNIFICANCE AND USE
4.1 The procedure described in this test method is designed to provide a method by which the coating weight of titanium treatments on metal substrates may be determined.  
4.2 This test method is applicable for determination of the total coating weight and the titanium coating weight of a titanium-containing treatment.
SCOPE
1.1 This test method covers the use of wavelength dispersive X-ray fluorescence (WDXRF) techniques for determination of the coating weight of titanium treatments on metal substrates. These techniques are applicable for determination of the coating weight as titanium or total coating weight of a titanium containing treatment, or both, on a variety of metal substrates.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM F3001-14(2021)(Specification)
Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion

ABSTRACT
This specification establishes the requirements for additively manufactured titanium-6aluminum-4vanadium with extra low interstitials (Ti-6Al-4V ELI) components using full-melt powder bed fusion such as electron beam melting and laser melting. The standard covers the classification of materials, ordering information, manufacturing plan, feedstock, process, chemical composition, microstructure, mechanical properties, thermal processing, hot isostatic pressing, dimensions and mass, permissible variations, retests, inspection, rejection, certification, product marking and packaging, and quality program requirements.
SCOPE
1.1 This specification covers additively manufactured titanium-6aluminum-4vanadium with extra low interstitials (Ti-6Al-4V ELI) components using full-melt powder bed fusion such as electron beam melting and laser melting. The components produced by these processes are used typically in applications that require mechanical properties similar to machined forgings and wrought products. Components manufactured to this specification are often, but not necessarily, post processed via machining, grinding, electrical discharge machining (EDM), polishing, and so forth to achieve desired surface finish and critical dimensions.  
1.2 This specification is intended for the use of purchasers or producers or both of additively manufactured Ti-6Al-4V ELI components for defining the requirements and ensuring component properties.  
1.3 Users are advised to use this specification as a basis for obtaining components that will meet the minimum acceptance requirements established and revised by consensus of the members of the committee.  
1.4 User requirements considered more stringent may be met by the addition to the purchase order of one or more supplementary requirements, which may include, but are not limited to, those listed in S1-S4 and S1-S16 in Specification F2924.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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