ASTM D2359-17
(Specification)Standard Specification for Refined Benzene-535
Standard Specification for Refined Benzene-535
ABSTRACT
This specification covers a grade of benzene known as refined benzene-535. Different tests shall be performed in order to determine the following properties of refined benzene-535: minimum purity, maximum toluene content, maximum sulfur content, maximum thiophene content, maximum nonaromatic hydrocarbon content, maximum nitrogen content, water content, maximum acid wash color, appearance, maximum color, 1,4 dioxane content, and minimum solidification point with anhydrous basis.
SCOPE
1.1 This specification covers a grade of benzene known as refined benzene-535.
1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 Consult current OSHA regulations, supplier’s Safety Data Sheets, and local regulations for all materials used in this specification.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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Designation: D2359 −17
Standard Specification for
1
Refined Benzene-535
This standard is issued under the fixed designation D2359; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
3
1. Scope Spectrophotometry (Withdrawn 2009)
D3437 Practice for Sampling and Handling Liquid Cyclic
1.1 This specification covers a grade of benzene known as
Products
refined benzene-535.
D4492 Test Method for Analysis of Benzene by Gas Chro-
1.2 The following applies to all specified limits in this
matography
standard: for purposes of determining conformance with this
D4735 Test Method for Determination of Trace Thiophene
standard, an observed value or a calculated value shall be
in Refined Benzene by Gas Chromatography
rounded off “to the nearest unit” in the last right-hand digit
D5194 Test Method for Trace Chloride in Liquid Aromatic
used in expressing the specification limit, in accordance with
Hydrocarbons
the rounding-off method of Practice E29.
D5386 Test Method for Color of Liquids Using Tristimulus
1.3 The values stated in SI units are to be regarded as Colorimetry
D5808 Test Method for Determining Chloride in Aromatic
standard. No other units of measurement are included in this
standard. Hydrocarbons and Related Chemicals by Microcoulom-
etry
1.4 Consult current OSHA regulations, supplier’s Safety
D6304 Test Method for Determination of Water in Petro-
Data Sheets, and local regulations for all materials used in this
leum Products, Lubricating Oils, and Additives by Cou-
specification.
lometric Karl Fischer Titration
1.5 This international standard was developed in accor-
D6875 Test Method for Solidification Point of Industrial
dance with internationally recognized principles on standard-
Organic Chemicals by Thermistor
ization established in the Decision on Principles for the
D7011 Test Method for Determination of Trace Thiophene
Development of International Standards, Guides and Recom-
in Refined Benzene by Gas Chromatography and Sulfur
mendations issued by the World Trade Organization Technical
Selective Detection
Barriers to Trade (TBT) Committee.
D7183 Test Method for Determination of Total Sulfur in
Aromatic Hydrocarbons and Related Chemicals by Ultra-
2. Referenced Documents
violet Fluorescence
2
2.1 ASTM Standards:
D7184 Test Method for Ultra Low Nitrogen in Aromatic
D848 Test Method for Acid Wash Color of Industrial Aro-
Hydrocarbons by Oxidative Combustion and Reduced
matic Hydrocarbons
Pressure Chemiluminescence Detection
D852 Test Method for Solidification Point of Benzene
D7359 Test Method for Total Fluorine, Chlorine and Sulfur
D1209 Test Method for Color of Clear Liquids (Platinum-
in Aromatic Hydrocarbons and Their Mixtures by Oxida-
Cobalt Scale)
tive Pyrohydrolytic Combustion followed by Ion Chroma-
D1685 Test Method for Traces of Thiophene in Benzene by
tography Detection (Combustion Ion Chromatography-
CIC)
D7360 Test Method for Analysis of Benzene by Gas Chro-
matography with External Calibration
D7375 Test Method for Trace Quantities of Water in Aro-
1
This specification is under the jurisdiction of ASTM Committee D16 on
matic Hydrocarbons and Their Mixtures by Coulometric
Aromatic, Industrial, Specialty and Related Chemicals and is the direct responsi-
3
bility of Subcommittee D16.01 on Benzene, Toluene, Xylenes, Cyclohexane and Karl Fischer Titration (Withdrawn 2017)
Their Derivatives.
D7457 Test Method for Determining Chloride in Aromatic
Current edition approved June 1, 2017. Published June 2017. Originally
Hydrocarbons and Related Chemicals by Microcoulom-
approved in 1966. Last previous edition approved in 2016 as D2359 – 16. DOI:
etry
10.1520/D2359-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D2359 − 17
A
D7504 Test Method for Trace Impurities in Monocyclic
Property Specification ASTM Test Method
Purity, min, weight % 99.80 D4492 or D7360
Aromatic Hydrocarbons by Gas Chromatography and
Toluene, max, weight % 0.10 D4492 or D7360
Effective Carbon Number
Thiophene, max, mg/kg 1 D1685 or D4735 or
D7536 Test Method for Chlorine in Aromatics by Mono- D7011
Nonaromatic hydrocarbons, max, 0.15 D4492 or D7360
chromatic Wavelength Dispersive X-ray
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D2359 − 16 D2359 − 17
Standard Specification for
1
Refined Benzene-535
This standard is issued under the fixed designation D2359; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*Scope
1.1 This specification covers a grade of benzene known as refined benzene-535.
1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard,
an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing
the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 Consult current OSHA regulations, supplier’s Safety Data Sheets, and local regulations for all materials used in this
specification.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D848 Test Method for Acid Wash Color of Industrial Aromatic Hydrocarbons
D852 Test Method for Solidification Point of Benzene
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
3
D1685 Test Method for Traces of Thiophene in Benzene by Spectrophotometry (Withdrawn 2009)
D3437 Practice for Sampling and Handling Liquid Cyclic Products
D4492 Test Method for Analysis of Benzene by Gas Chromatography
D4735 Test Method for Determination of Trace Thiophene in Refined Benzene by Gas Chromatography
D5194 Test Method for Trace Chloride in Liquid Aromatic Hydrocarbons
D5386 Test Method for Color of Liquids Using Tristimulus Colorimetry
D5808 Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
D6304 Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl
Fischer Titration
D6875 Test Method for Solidification Point of Industrial Organic Chemicals by Thermistor
D7011 Test Method for Determination of Trace Thiophene in Refined Benzene by Gas Chromatography and Sulfur Selective
Detection
D7183 Test Method for Determination of Total Sulfur in Aromatic Hydrocarbons and Related Chemicals by Ultraviolet
Fluorescence
D7184 Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure
Chemiluminescence Detection
D7359 Test Method for Total Fluorine, Chlorine and Sulfur in Aromatic Hydrocarbons and Their Mixtures by Oxidative
Pyrohydrolytic Combustion followed by Ion Chromatography Detection (Combustion Ion Chromatography-CIC)
D7360 Test Method for Analysis of Benzene by Gas Chromatography with External Calibration
1
This specification is under the jurisdiction of ASTM Committee D16 on Aromatic Hydrocarbons Aromatic, Industrial, Specialty and Related Chemicals and is the direct
responsibility of Subcommittee D16.01 on Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives.
Current edition approved June 1, 2016June 1, 2017. Published June 2016June 2017. Originally approved in 1966. Last previous edition approved in 20122016 as
D2359 – 12.D2359 – 16. DOI: 10.1520/D2359-16.10.1520/D2359-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
The last approved version of this historical standard is referenced on www.astm.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D2359 − 17
D7375 Test Method for Trace Quantities of Water in Aromatic Hydrocarbons and Their Mixtures by Coulometric Karl Fischer
3
Titration (Withdrawn 2017)
D7457 Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
D7504 Test Method for Trace Impurit
...
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