ASTM D4339-01(2018)
(Test Method)Standard Test Method for Determination of the Odor of Adhesives
Standard Test Method for Determination of the Odor of Adhesives
SIGNIFICANCE AND USE
4.1 The results from this determination are useful in determining the suitability of adhesives in applications where the odor level associated with the end use is critical.
SCOPE
1.1 This test method describes a procedure for evaluating the odor of adhesives. It is intended to replace Federal Standard 175A, Method 4051.
1.2 This test method provides a means of comparing the odor of an adhesive sample to a reference sample. It is not intended to give an absolute value for the odor of a sample. It can be used for wet or dry samples.
1.3 Warning—Do not use this test method with adhesives containing hazardous components such as solvent residues and unreacted monomeric materials.
1.4 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See 1.3 for specific precautionary statements.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
Relations
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D4339 − 01 (Reapproved 2018)
Standard Test Method for
Determination of the Odor of Adhesives
This standard is issued under the fixed designation D4339; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope (Dilution Method) (Withdrawn 1986)
1.1 This test method describes a procedure for evaluating
3. Terminology
the odor of adhesives. It is intended to replace Federal
Standard 175A, Method 4051.
3.1 Definitions—Several terms in this test method are de-
fined in accordance with Terminology D907.
1.2 This test method provides a means of comparing the
odor of an adhesive sample to a reference sample. It is not
3.2 Definitions of Terms Specific to This Standard:
intended to give an absolute value for the odor of a sample. It
3.2.1 odor, n—that property of a substance which affects the
can be used for wet or dry samples.
sense of smell.
1.3 Warning—Do not use this test method with adhesives
4. Significance and Use
containing hazardous components such as solvent residues and
unreacted monomeric materials.
4.1 The results from this determination are useful in deter-
mining the suitability of adhesives in applications where the
1.4 The values stated in inch-pound units are to be regarded
odor level associated with the end use is critical.
as the standard. The values given in parentheses are for
information only.
5. Apparatus
1.5 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 5.1 Glass Bottles, 1-qt (1-L), wide-mouth, straight sided,
responsibility of the user of this standard to establish appro- with screw caps.
priate safety, health, and environmental practices and deter-
NOTE 1—It is important that the bottles and caps be kept clean and
mine the applicability of regulatory limitations prior to use.
odor-free. Discard any bottle which cannot be made visibly clean or
See 1.3 for specific precautionary statements.
odor-free. Wash bottles and caps with a suitable cleaning powder, rinse
1.6 This international standard was developed in accor- thoroughly with tap water, then rinse with distilled water, drain, and dry
in an oven. Do all cleaning in an odor-free atmosphere.
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
5.2 Oven or Incubator, for aging samples at elevated tem-
Development of International Standards, Guides and Recom-
peratures.
mendations issued by the World Trade Organization Technical
5.3 Aluminum Foil.
Barriers to Trade (TBT) Committee.
5.4 Balance, capable of measuring to nearest 0.1 g.
2. Referenced Documents
6. Test Sample and Test Specimen
2.1 ASTM Standards:
D907 Terminology of Adhesives
6.1 Select a test sample representative of the adhesive being
D1391 Method for Measurement of Odor in Atmospheres
tested. It may be liquid or solid. Keep in a tightly closed
container until used (5.1).
6.2 For the test specimen, place 20.0 6 0.1 g of the test
This test method is under the jurisdiction of ASTM Committee D14 on
sample into the glass bottle (5.1), cover with aluminum foil,
Adhesives and is the direct responsibility of Subcommittee D14.10 on Working
place the cap on the bottle and tighten.
Properties.
Current edition approved Nov. 1, 2018. Published November 2018. Originally
NOTE 2—Always use new aluminum foil, never reuse it.
approved in 1984. Last previous edition approved in 2013 as D4339 – 01 (2013).
DOI: 10.1520/D4339-01R18.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
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D4339 − 01 (2018)
7. Reference Sample and Reference Specimen 10.2 Remove the cap and foil and immediately sniff the
odor. Keep the bottle closed except for the short period
7.1 Select a reference sample, that from prior experience or
necessary to sniff the specimen. (Warning—See 1.3.)
knowledge,orbyagreementbetweensupplierandpurchaserof
adhesive, has acceptable odor. 10.3 Indicate for each pair of samples whether the odor of
7.1.1 Store the reference sample in a tightly closed the adhesive specimen is less than, equal to, or greater than the
container, specified in 5.1
...
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