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ASTM D4762-88(2001)

(Guide)

Standard Guide for Testing Automotive/Industrial Composite Materials

Standard Guide for Testing Automotive/Industrial Composite Materials

SCOPE
1.1 This guide covers the testing of molded automotive/industrial composite materials. It is intended to increase the users awareness of the special considerations necessary for the testing of these materials. In addition, the user is provided with a comparison of some of the more commonly used ASTM International standard test methods that are applicable for evaluating automotive/industrial composites.
1.2 Areas in which current ASTM International standard test methods do not meet the needs for testing of automotive/industrial composites are indicated. This provides direction for future standardization work.
1.3 It is not the intent of this guide to cover all test methods which could possibly be used for automotive/industrial composites. Only the most commonly used and most applicable standards are included.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
28-Jan-1988
ICS
83.140.20 - Laminated sheets
Technical Committee
D30 - Composite Materials
Drafting Committee
D30.04 - Lamina and Laminate Test Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D4762-88(1995)e1 - Standard Guide for Testing Automotive/Industrial Composite Materials
Effective Date
29-Jan-1988
Replaced By
ASTM D4762-04 - Standard Guide for Testing Polymer Matrix Composite Materials
Effective Date
01-May-2004
Referred By
ASTM D8069-17a - Standard Test Method for Determining Flexural Modulus of Full Section Pultruded Fiber Reinforced Polymer (FRP) Composite Members with Doubly Symmetric Cross Sections under Bending
Effective Date
29-Jan-1988
Referred By
ASTM E2533-21 - Standard Guide for Nondestructive Examination of Polymer Matrix Composites Used in Aerospace Applications
Effective Date
29-Jan-1988
Referred By
ASTM D8509/D8509M-23 - Standard Guide for Test Method Selection and Test Specimen Design for Bolted Joint Related Properties
Effective Date
29-Jan-1988

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ASTM D4762-88(2001) - Standard Guide for Testing Automotive/Industrial Composite MaterialsASTM D4762-88(2001) - Standard Guide for Testing Automotive/Industrial Composite Materials
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ASTM D4762-88(2001) - Standard Guide for Testing Automotive/Industrial Composite Materials
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 4762 – 88 (Reapproved 2001)
Standard Guide for
1
Testing Automotive/Industrial Composite Materials
This standard is issued under the fixed designation D 4762; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
A new class of composite materials has been developed to meet the needs of automotive and
industrial mass production applications. This new class of materials, referred to as automotive/
industrial composites, is comprised of filled and unfilled polymers reinforced with chopped or
6
continuous high modulus, or both (greater than 20.7 GPa (3 3 10 psi)) fibers.
Automotive/industrial composites possess some of the same advantages as high-performance
aerospace composites. However, some aspects of performance are traded off for reduced cost, ease of
manufacturing, and high quality appearance. Automotive/industrial composites are also different from
materials classified as plastics. This difference arises from the use of high modulus fiber reinforcement
to provide substantial improvements in structural properties of the base polymer system.
Currently, ASTM International standard test methods developed for high performance composites
or plastics, or both, are used for testing of automotive/industrial composites. In many cases, these
standards are quite adequate if proper attention is given to the special testing considerations for
automotive/industrial composites covered in this guide. However, in some cases, current standards do
not meet the needs for testing of the required properties. In this case, revised standards or new
standards specifically for automotive/industrial composites may be desirable.
In addition to covering the special considerations required for automotive/industrial composites
testing, this guide points out and compares existing ASTM International standards applicable to these
materials. This is done only for some of the more commonly evaluated material properties.
1. Scope responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
1.1 This guide covers the testing of molded automotive/
bility of regulatory limitations prior to use.
industrial composite materials. It is intended to increase the
users awareness of the special considerations necessary for the
2. Referenced Documents
testing of these materials. In addition, the user is provided with
2.1 ASTM Standards:
a comparison of some of the more commonly used ASTM
C 581 Practice for Determining Chemical Resistance of
International standard test methods that are applicable for
Thermosetting Resins Used in Glass-Fiber-Reinforced
evaluating automotive/industrial composites.
2
Structures Intended for Liquid Service
1.2 Areas in which current ASTM International standard
D 256 Test Methods for Determining Izod Pendulum Im-
test methods do not meet the needs for testing of automotive/
3
pact Resistance of Plastics
industrial composites are indicated. This provides direction for
D 543 Practices for Evaluating the Resistance of Plastics to
future standardization work.
3
Chemical Reagents
1.3 It is not the intent of this guide to cover all test methods
3
D 618 Practice for Conditioning Plastics for Testing
which could possibly be used for automotive/industrial com-
3
D 638 Test Method for Tensile Properties of Plastics
posites. Only the most commonly used and most applicable
D 648 Test Method for Deflection Temperature of Plastics
standards are included.
3
Under Flexural Load in the Edgewise Position
1.4 This standard does not purport to address all of the
D 671 Test Method for Flexural Fatigue of Plastics by
safety concerns, if any, associated with its use. It is the
3
Constant-Amplitude-of-Force
1
This guide is under the jurisdiction of ASTM Committee D30 on Composite
Materials and is the direct responsibility of Subcommittee D30.03 on Constituent/
2
Precursor Properties. Annual Book of ASTM Standards, Vol 08.04.
3
Current edition approved Jan. 29, 1988. Published June 1988. Annual Book of ASTM Standards, Vol 08.01.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D 4762 – 88 (2001)
D 695 Test Method for Compressive Properties of Rigid 4. Significance and Use
3
Plastics
4.1 This guide is intended to serve as a reference for the
D 696 Test Method for Coefficient of Linear Thermal Ex-
testing of automotive/industrial composite materials.
3
pansion of Plastics Between − 30°C and 30°C
4.2 The use of this guide assures that proper
...

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ASTM D3479/D3479M-19(2023)(Test Method)
Standard Test Method for Tension-Tension Fatigue of Polymer Matrix Composite Materials

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5.1 This test method is designed to yield tensile fatigue data for material specifications, research and development, quality assurance, and structural design and analysis. The primary test result is the fatigue life of the test specimen under a specific loading and environmental condition. Replicate tests may be used to obtain a distribution of fatigue life for specific material types, laminate stacking sequences, environments, and loading conditions. Guidance in statistical analysis of fatigue life data, such as determination of linearized stress life (S-N) or strain-life (ε-N) curves, can be found in Practice E739.  
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1.1 This test method determines the fatigue behavior of polymer matrix composite materials subjected to tensile cyclic loading. The composite material forms are limited to continuous-fiber or discontinuous-fiber reinforced composites for which the elastic properties are specially orthotropic with respect to the test direction. This test method is limited to unnotched test specimens subjected to constant amplitude uniaxial in-plane loading where the loading is defined in terms of a test control parameter.  
1.2 This test method presents two procedures where each defines a different test control parameter.  
1.2.1 Procedure A—A system in which the test control parameter is the load (stress) and the machine is controlled so that the test specimen is subjected to repetitive constant amplitude load cycles. In this procedure, the test control parameter may be described using either engineering stress or applied load as a constant amplitude fatigue variable.  
1.2.2 Procedure B—A system in which the test control parameter is the strain in the loading direction and the machine is controlled so that the test specimen is subjected to repetitive constant amplitude strain cycles. In this procedure, the test control parameter may be described using engineering strain in the loading direction as a constant amplitude fatigue variable.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3.1 Within the text the inch-pound units are shown in brackets.  
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ASTM D4762-23(Guide)
Standard Guide for Testing Polymer Matrix Composite Materials

SIGNIFICANCE AND USE
4.1 This guide is intended to aid in the selection of standards for polymer matrix composite materials. It specifically summarizes the application of standards from ASTM Committee D30 on Composite Materials that apply to continuous-fiber reinforced polymer matrix composite materials. For reference and comparison, many commonly used or applicable ASTM standards from other ASTM Committees are also included.
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1.1 This guide summarizes the application of ASTM standard test methods (and other supporting standards) to continuous-fiber reinforced polymer matrix composite materials. The most commonly used or most applicable ASTM standards are included, emphasizing use of standards of Committee D30 on Composite Materials.  
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1.3 This guide does not specify a system of measurement; the systems specified within each of the referenced standards shall apply as appropriate. Note that the referenced standards of ASTM Committee D30 are either SI-only or combined-unit standards with SI units listed first.  
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ASTM D8387/D8387M-23(Test Method)
Standard Test Method for High Bypass – Low Bearing Interaction Response of Polymer Matrix Composite Laminates

SIGNIFICANCE AND USE
5.1 Refer to Guide D8509.
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1.1 This test method determines the uniaxial high bypass - low bearing interaction response of multi-directional polymer matrix composite laminates reinforced by high-modulus fibers using a two-fastener hard point joint specimen. The scope of this test method is limited to net section (bypass) failure modes. Standard specimen configurations using fixed values of test parameters are described for this procedure. A number of test parameters may be varied within the scope of the standard, provided that the parameters are fully documented in the test report. The composite material forms are limited to continuous-fiber or discontinuous-fiber (tape or fabric, or both) reinforced composites for which the laminate is balanced and symmetric with respect to the test direction. The range of acceptable test laminates and thicknesses are described in 8.2.1. This test method was previously published under Test Method D7248/D7248M-17 Procedure C.  
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ASTM D6873/D6873M-23(Practice)
Standard Practice for Bearing Fatigue Response of Polymer Matrix Composite Laminates

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5.1 Refer to Guide D8509.
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1.1 This practice provides instructions for modifying static bearing test methods to determine the fatigue behavior of composite materials subjected to cyclic bearing forces. The composite material forms are limited to continuous-fiber reinforced polymer matrix composites in which the laminate is both symmetric and balanced with respect to the test direction. The range of acceptable test laminates and thicknesses are described in 8.2.  
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5.1.4 Poisson's ratio in compression.  
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ASTM D8131/D8131M-23(Practice)
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5.1 This test practice is designed to produce tensile property data for material specifications, research and development, quality assurance, and structural design and analysis. Factors that influence the tensile response and should therefore be reported include the following: materials (laminates and adhesive), methods of material preparation including surface preparation prior to bonding, lay-ups, specimen stacking sequence, joint taper ratio or step length, ply overlap length, material relative thicknesses and stiffness of the parent and repair laminates, adhesive bond stiffness, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, time at temperature, void content, and volume percent reinforcement. Properties in the test direction, which may be obtained from this test practice, include the following:  
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5.1.2 Ultimate tensile strength (based on the nominal repair material thickness), (Frtu).  
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1.1 This test practice defines the procedure for determination of the tensile strength of a tapered or stepped joint of polymer matrix composite materials. It is applicable to secondary bonded or co-bonded laminates with either unidirectional plies or woven fabric reinforcements. The materials to be bonded may be different material systems. In the bondline, a separate adhesive material may or may not be used (example: adhesives may be used with a prepreg system or may not be used with a wet lay-up repair system). The range of acceptable test laminates and thicknesses is described in 8.2.1.  
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1.3 Unidirectional (0° ply orientation) tape composites, textile composites, as well as multidirectional composite laminates, can be tested.  
1.4 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
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ASTM D2344/D2344M-22(Test Method)
Standard Test Method for Short-Beam Strength of Polymer Matrix Composite Materials and Their Laminates

SIGNIFICANCE AND USE
5.1 In most cases, because of the complexity of internal stresses and the variety of failure modes that can occur in this specimen, it is not generally possible to relate the short-beam strength to any one material property. However, failures are normally dominated by resin and interlaminar properties, and the test results have been found to be repeatable for a given specimen geometry, material system, and stacking sequence  (4).  
5.2 Short-beam strength determined by this test method can be used for quality control and process specification purposes. It can also be used for comparative testing of composite materials, provided that failures occur consistently in the same mode (5) .  
5.3 This test method is not limited to specimens within the range specified in Section 8, but is limited to the use of a loading span length-to-specimen thickness ratio of 4.0 and a minimum specimen thickness of 2.0 mm [0.08 in.].
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1.1 This test method determines the short-beam strength of high-modulus fiber-reinforced composite materials. The specimen is a short beam machined from a curved or a flat laminate up to 6.00 mm [0.25 in.] thick. The beam is loaded in three-point bending.  
1.2 Application of this test method is limited to continuous- or discontinuous-fiber-reinforced polymer matrix composites, for which the elastic properties are balanced and symmetric with respect to the longitudinal axis of the beam.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3.1 Within the text, the inch-pound units are shown in brackets.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D5449/D5449M-22(Test Method)
Standard Test Method for Transverse Compressive Properties of Hoop Wound Polymer Matrix Composite Cylinders

SIGNIFICANCE AND USE
5.1 This test method is designed to produce transverse compressive property data for material specifications, research and development, quality assurance, and structural design and analysis. Factors that influence the transverse compressive response and should therefore be reported are: material, method of material preparation, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, void content, and fiber volume fraction. Properties in the test direction that may be obtained from this test method are:  
5.1.1 Transverse compressive strength, σ22uc,  
5.1.2 Transverse compressive strain at failure, ε22uc,  
5.1.3 Transverse compressive modulus of elasticity, E22, and  
5.1.4 Poisson's ratio, γ21.
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1.1 This test method determines the transverse compressive properties of wound polymer matrix composites reinforced by high-modulus continuous fibers. It describes testing of hoop wound (90°) cylinders in axial compression for determination of transverse compressive properties.  
1.2 The technical content of this test method has been stable since 1993 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this test method, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards, including editorial changes and incorporation of updated guidance on specimen preconditioning and environmental testing. The test method, therefore, should not be considered to include any significant changes in approach and practice since 1993. Future maintenance of the test method will only be in response to specific requests and performed only as technical support allows.  
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1.3.1 Within the text, the inch-pound units are shown in brackets.  
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ASTM D5450/D5450M-22(Test Method)
Standard Test Method for Transverse Tensile Properties of Hoop Wound Polymer Matrix Composite Cylinders

SIGNIFICANCE AND USE
5.1 This test method is used to produce transverse tensile property data for material specifications, research and development, quality assurance, and structural design and analysis. Factors which influence the transverse tensile response and should, therefore, be reported are: material, methods of material preparation, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, void content, and fiber volume fraction. Properties, in the test direction, which may be obtained from this test method include:  
5.1.1 Transverse Tensile Strength,    
5.1.2 Transverse Tensile Strain at Failure,    
5.1.3 Transverse Tensile Modulus of Elasticity,  E22, and  
5.1.4 Poisson's Ratio,  υ21.
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1.1 This test method determines the transverse tensile properties of wound polymer matrix composites reinforced by high-modulus continuous fibers. It describes testing of hoop wound (90°) cylinders in axial tension for determination of transverse tensile properties.  
1.2 The technical content of this test method has been stable since 1993 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this test method, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards, including editorial changes and incorporation of updated guidance on specimen preconditioning and environmental testing. The test method, therefore, should not be considered to include any significant changes in approach and practice since 1993. Future maintenance of the test method will only be in response to specific requests and performed only as technical support allows.  
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1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM
ASTM E1922/E1922M-22(Test Method)
Standard Test Method for Translaminar Fracture Toughness of Laminated and Pultruded Polymer Matrix Composite Materials

SIGNIFICANCE AND USE
5.1 The parameter KTL  determined by this test method is a measure of the resistance of a polymer matrix composite laminate to notch-tip damage and effective translaminar crack growth under opening mode loading. The result is valid only for conditions in which the damage zone at the notch tip is small compared with the notch length and the in-plane specimen dimensions. Alternately, for materials exhibiting distributed damage in a larger volume, observed force-displacement and discrete damage events are still valid structural responses for certain specific engineering applications.  
5.2 This test method can serve the following purposes. In research and development, (a) KTL data can quantitatively establish the effects of fiber and matrix variables and stacking sequence of the laminate on the translaminar fracture resistance of composite laminates; and (b) quantified distributed damage measurements can be used to validate progressive composite damage models. In structural design, KTL data can, within the constraints of the specimen geometry and loading, be used to assess composite laminate resistance to damage growth from edge flaws and notches.  
5.3 The translaminar fracture toughness,  KTL, as well as distributed damage observations, determined by this test method may be a function of the testing speed and temperature. This test method is intended for room temperature and quasi-static conditions, but it can apply to other test conditions provided that the requirements of 13.2 and 13.3 are met. Application of KTL in the design of service components should be made with awareness that the test parameters specified by this test may differ from service conditions, possibly resulting in a different material response than that seen in service. Distributed damage observations are also limited to the material and geometry tested, but may be more generally applied to a variety of structural analysis validation applications.  
5.4 Not all types of laminated polymer matrix...
SCOPE
1.1 This test method covers the determination of translaminar fracture toughness, KTL, for laminated, molded, or pultruded polymer matrix composite materials of various fiber orientations using test results from monotonically loaded notched specimens. If the material response is such that the KTL calculation is not valid, alternate reporting methods are provided.  
1.2 This test method is applicable to room temperature laboratory air environments.  
1.3 Composite materials that can be tested by this test method are not limited by thickness or by type of polymer matrix or fiber, provided that the specimen sizes and the test results meet the requirements of this test method. This test method was developed primarily from test results of various carbon fiber – epoxy matrix laminates and from additional results of glass fiber – epoxy matrix, glass fiber-polyester matrix pultrusions and carbon fiber – bismaleimide matrix laminates (1-4, 5, 6).2  
1.4 A range of eccentrically loaded, single-edge-notch tension, ESE(T), specimen sizes with proportional planar dimensions is provided, but planar size may be variable and adjusted, with associated changes in the applied test load. Specimen thickness is a variable, independent of planar size.  
1.5 Specimen configurations other than those contained in this test method may be used. It is particularly important that the requirements discussed in 5.1 and 5.4 regarding contained notch-tip damage be met when using alternative specimen configurations in conjunction with the KTL calculation.  
1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.6.1 Within the text, the inch-pound units are shown ...

  • Standard
    8 pages
    English language
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  • Standard
    8 pages
    English language
    sale 15% off