ASTM D1796-97
(Test Method)Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
SCOPE
1.1 This test method covers the laboratory test for determination of water and sediment in fuel oils by using the centrifuge method in the range from 0 to 30% volume. This chapter, along with API Chapter 10.3 (Test Method D 4007, IP 359), supersedes the previous edition of ASTM Test Method D 1796 (API Standard D 2548, IP75).
Note 1-With some types of fuel oils such as residual fuel oils or distillate fuel oils containing residual components, it is difficult to obtain water or sediment contents with this test method. When this situation is encountered, Method D 95 (API MPMS Chapter 10.5) or Test Method D 473 (API MPMS Chapter 10.1) may be used.
1.2 annex A2 contains a procedure for saturating toluene with water.
1.3 the values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific precautionary statement see 5.1.
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Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D 1796 – 97 An American National Standard
Designation: MPMS Chapter 10.6
Standard Test Method for
Water and Sediment in Fuel Oils by the Centrifuge Method
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(Laboratory Procedure)
This standard is issued under the fixed designation D 1796; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This test method has been approved by the sponsoring committees and accepted by the cooperating organizations in accordance with
established procedures. This test method has been adopted for use by government agencies to replace Method 3000 of Federal Test
Method Standard No. 7916.
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1. Scope Oils by the Extraction Method
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D 4006 Test Method for Water in Crude Oil by Distillation
1.1 This test method covers the laboratory test for determi-
D 4007 Test Method for Water and Sediment in Crude Oil
nation of water and sediment in fuel oils by using the
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by the Centrifuge Method (Laboratory Procedure)
centrifuge method in the range from 0 to 30 % volume. This
D 4057 Practice for Manual Sampling of Petroleum and
chapter, along with API Chapter 10.3 (Test Method D 4007, IP
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Petroleum Products
359), supersedes the previous edition of Test Method D 1796
D 4177 Practice for Automatic Sampling of Petroleum and
(API Standard D 2548, IP 75).
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Petroleum Products
NOTE 1—With some types of fuel oils such as residual fuel oils or
D 4377 Test Method for Water in Crude Oils by Volumetric
distillate fuel oils containing residual components, it is difficult to obtain
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Karl Fischer Titration
water or sediment contents with this test method. When this situation is
D 4928 Test Method for Water in Crude Oils by Coulom-
encountered, Method D 95 (API MPMS Chapter 10.5) or Test Method
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etric Karl Fischer Titration
D 473 (API MPMS Chapter 10.1) may be used.
D 5854 Practice for Mixing and Handling Liquid Samples
1.2 Annex A2 contains a procedure for saturating toluene
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of Petroleum and Petroleum Products
with water.
E 542 Practice for Calibration of Laboratory Volumetric
1.3 The values stated in SI units are to be regarded as the
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Apparatus
standard. The values in parentheses are for information only.
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2.2 API Manual of Petroleum Measurement Standards:
1.4 This standard does not purport to address all of the
Chapter 8.1, Manual Sampling of Petroleum and Petroleum
safety concerns, if any, associated with its use. It is the
Products ( Practice D 4057)
responsibility of the user of this standard to establish appro-
Chapter 8.2, Automatic Sampling of Petroleum and Petro-
priate safety and health practices and determine the applica-
leum Products (Test Method D 4177)
bility of regulatory limitations prior to use. For a specific
Chapter 8.3, Mixing and Handling Liquid Samples of Pe-
precautionary statement see 6.1.
troleum and Petroleum Products (Test Method D 5854)
Chapter 10.1, Determination of Sediment in Crude Oil by
2. Referenced Documents
the Extraction Method (Test Method D 473)
2.1 ASTM Standards:
Chapter 10.2, Determination of Water in Crude Oil by the
D 95 Test Method for Water in Petroleum Products and
Distillation Method (Test Method D 4006)
Bituminous Materials by Distillation (API MPMS Chapter
Chapter 10.3, Determination of Water and Sediment in
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10.5)
Crude Oils by the Centrifuge Method (Laboratory Proce-
3
D 362 Specification for Industrial Grade Toluene
dure) (Test Method D 1796)
D 473 Test Method for Sediment in Crude Oils and Fuel
Chapter 10.5, Determination of Water in Petroleum Prod-
ucts and Other Bituminous Materials (Test Method D 95)
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This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products and Lubricantsand is the direct responsibility of Subcommittee
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D02.02on Static Petroleum Measurement. Annual Book of ASTM Standards, Vol 05.02.
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Current edition approved Jan. 10, 1997. Published October 1997. Originally Annual Book of ASTM Standards, Vol 05.03.
e1 6
published as D 1796 – 60. Last previous edition D 1796 – 83 (1990). Annual Book of ASTM Standards, Vol 14.02.
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Annual Book of ASTM Standards, Vol 05.01. Available from the American Petroleum Institute, 1220 L St., N.W., Washing-
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Discontinued—See 1988 Annual Book of ASTM Standards, Vol 06.03. ton, DC 20005.
Copyright © ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
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NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
D 1796
Chapter 10.7, Determination of Water in Crude Oils (Karl
Fischer) Titration (Test Method D 43
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