ASTM D1160-18
(Test Method)Standard Test Method for Distillation of Petroleum Products at Reduced Pressure
Standard Test Method for Distillation of Petroleum Products at Reduced Pressure
SIGNIFICANCE AND USE
5.1 This test method is used for the determination of the distillation characteristics of petroleum products, biodiesel, and fractions that may decompose if distilled at atmospheric pressure. This boiling range, obtained at conditions designed to obtain approximately one theoretical plate fractionation, can be used in engineering calculations to design distillation equipment, to prepare appropriate blends for industrial purposes, to determine compliance with regulatory rules, to determine the suitability of the product as feed to a refining process, or for a host of other purposes.
5.2 The boiling range is directly related to viscosity, vapor pressure, heating value, average molecular weight, and many other chemical, physical, and mechanical properties. Any of these properties can be the determining factor in the suitability of the product in its intended application.
5.3 Petroleum product specifications often include distillation limits based on data by this test method.
5.4 Many engineering design correlations have been developed on data by this test method. These correlative methods are used extensively in current engineering practice.
SCOPE
1.1 This test method covers the determination, at reduced pressures, of the range of boiling points for petroleum products and biodiesel that can be partially or completely vaporized at a maximum liquid temperature of 400 °C. Both a manual method and an automatic method are specified.
1.2 In cases of dispute, the referee test method is the manual test method at a mutually agreed upon pressure.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 6.1.4, 6.1.8.1, 10.11, and A3.2.1.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1160 − 18
Standard Test Method for
1
Distillation of Petroleum Products at Reduced Pressure
This standard is issued under the fixed designation D1160; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope* ucts by Hydrometer Method
D4052Test Method for Density, Relative Density, and API
1.1 This test method covers the determination, at reduced
Gravity of Liquids by Digital Density Meter
pressures,oftherangeofboilingpointsforpetroleumproducts
D4057Practice for Manual Sampling of Petroleum and
andbiodieselthatcanbepartiallyorcompletelyvaporizedata
Petroleum Products
maximumliquidtemperatureof400°C.Bothamanualmethod
D4177Practice for Automatic Sampling of Petroleum and
and an automatic method are specified.
Petroleum Products
1.2 Incasesofdispute,therefereetestmethodisthemanual
D6300Practice for Determination of Precision and Bias
test method at a mutually agreed upon pressure.
Data for Use in Test Methods for Petroleum Products and
1.3 The values stated in SI units are to be regarded as
Lubricants
standard. The values given in parentheses after SI units are
providedforinformationonlyandarenotconsideredstandard.
3. Terminology
1.4 This standard does not purport to address all of the
3.1 Definitions of Terms Specific to This Standard:
safety concerns, if any, associated with its use. It is the
3.1.1 atmospheric equivalent temperature (AET), n—the
responsibility of the user of this standard to establish appro-
temperature converted from the measured vapor temperature
priate safety, health, and environmental practices and deter-
using EqA7.1. TheAET is the expected distillate temperature
mine the applicability of regulatory limitations prior to use.
if the distillation was performed at atmospheric pressure and
For specific warning statements, see 6.1.4, 6.1.8.1, 10.11, and
there was no thermal decomposition.
A3.2.1.
1.5 This international standard was developed in accor-
3.1.2 end point (EP) or final boiling point (FBP), n—the
dance with internationally recognized principles on standard-
maximum vapor temperature reached during the test.
ization established in the Decision on Principles for the
3.1.3 initial boiling point (IBP), n—the vapor temperature
Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical that is measured at the instant the first drop of condensate falls
Barriers to Trade (TBT) Committee. from the lower end of the condenser section drip tip.
3.1.3.1 Discussion—Whenachainisattachedtothedriptip
2. Referenced Documents
the first drop will form and run down the chain. In automatic
2
2.1 ASTM Standards:
apparatus, the first drop detection device shall be located as
D613Test Method for Cetane Number of Diesel Fuel Oil
near to the lower end of the drip tip as practical.
D1193Specification for Reagent Water
3.1.4 spillover point, n—the highest point of the lower
D1250Guide for Use of the Petroleum MeasurementTables
internal junction of the distillation column and the condensing
D1298Test Method for Density, Relative Density, or API
section of the vacuum-jacketed column assembly.
Gravity of Crude Petroleum and Liquid Petroleum Prod-
4. Summary of Test Method
1
This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of
4.1 The sample is distilled at an accurately controlled
Subcommittee D02.08 on Volatility.
pressure between 0.13kPa and 6.7kPa (1mm and 50 mm Hg)
Current edition approved July 1, 2018. Published August 2018. Originally
under conditions that are designed to provide approximately
approved in 1951. Last previous edition approved in 2015 as D1160–15. DOI:
10.1520/D1160-18.
one theoretical plate fractionation. Data are obtained from
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
which the initial boiling point, the final boiling point, and a
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
distillation curve relating volume percent distilled and atmo-
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. spheric equivalent boiling point temperature can be prepared.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D1160 − 15 D1160 − 18
Standard Test Method for
1
Distillation of Petroleum Products at Reduced Pressure
This standard is issued under the fixed designation D1160; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope*
1.1 This test method covers the determination, at reduced pressures, of the range of boiling points for petroleum products and
biodiesel that can be partially or completely vaporized at a maximum liquid temperature of 400 °C. Both a manual method and
an automatic method are specified.
1.2 In cases of dispute, the referee test method is the manual test method at a mutually agreed upon pressure.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.after
SI units are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use. For specific warning statements, see 6.1.4, 6.1.8.1, 10.11, and A3.2.1.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D613 Test Method for Cetane Number of Diesel Fuel Oil
D1193 Specification for Reagent Water
D1250 Guide for Use of the Petroleum Measurement Tables
D1298 Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by
Hydrometer Method
D4052 Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
D6300 Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
3. Terminology
3.1 Definitions of Terms Specific to This Standard:
3.1.1 atmospheric equivalent temperature (AET), n—the temperature converted from the measured vapor temperature using Eq
A7.1. The AET is the expected distillate temperature if the distillation was performed at atmospheric pressure and there was no
thermal decomposition.
3.1.2 end point (EP) or final boiling point (FBP),n—the maximum vapor temperature reached during the test.
3.1.3 initial boiling point (IBP), n—the vapor temperature that is measured at the instant the first drop of condensate falls from
the lower end of the condenser section drip tip.
1
This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee
D02.08 on Volatility.
Current edition approved Feb. 1, 2015July 1, 2018. Published February 2015August 2018. Originally approved in 1951. Last previous edition approved in 20132015 as
D1160 – 13.D1160 – 15. DOI: 10.1520/D1160-15.10.1520/D1160-18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
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D1160 − 18
3.1.3.1 Discussion—
When a chain is attached to the drip tip the first drop will form and run down the chain. In automatic apparatus, the first drop
detection device shall be located as near to the lower end of the drip tip as practical.
3.1.4 spillover point, n—the highest point of the lower internal junction of the distillation column and the condensing section
of the vacuum-jacketed column assembly.
4. Summary of Test Method
4.1 The
...
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