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ASTM D5505-06

(Practice)

Standard Practice for Classifying Emulsified Recycling Agents

Standard Practice for Classifying Emulsified Recycling Agents

SIGNIFICANCE AND USE
Recycling of deteriorated asphalt pavements is being used as a routine method of maintenance and rehabilitation. Utilization of existing materials as the major component of this procedure may yield benefits in quality, economy, and preservation of natural resources. Recycling takes many forms; hot, cold, in-situ, central plant and surface. This practice may be used for various recycling methods.
SCOPE
1.1 This practice identifies emulsified petroleum products that may be used as recycling agents in recycled mixes. These materials are classified by viscosity or by low temperature penetration after aging.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.2 This practice addresses emulsified materials designed specifically for use in recycling. The use of emulsified materials for recycling shall not be limited to this practice. For instance, the emulsions specified in Specifications D 977 and D 2397 may be used.

General Information

Status
Historical
Publication Date
30-Nov-2006
ICS
75.080 - Petroleum products in general
75.100 - Lubricants, industrial oils and related products
Technical Committee
D04 - Road and Paving Materials
Drafting Committee
D04.41 - Emulsified Asphalt Specifications
Current Stage
Ref Project

Relations

Replaces
ASTM D5505-97(2001) - Standard Practice for Classifying Emulsified Recycling Agents
Effective Date
01-Dec-2006
Referred By
ASTM D8-22a - Standard Terminology Relating to Materials for Roads and Pavements
Effective Date
01-Dec-2006

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ASTM D5505-06 - Standard Practice for Classifying Emulsified Recycling Agents
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D5505 −06
StandardPractice for
1
Classifying Emulsified Recycling Agents
This standard is issued under the fixed designation D5505; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D2397 Specification for Cationic Emulsified Asphalt
D2872 Test Method for Effect of Heat and Air on a Moving
1.1 This practice identifies emulsified petroleum products
Film of Asphalt (Rolling Thin-Film Oven Test)
that may be used as recycling agents in recycled mixes. These
D6930 Test Method for Settlement and Storage Stability of
materials are classified by viscosity or by low temperature
Emulsified Asphalts
penetration after aging.
D6933 Test Method for Oversized Particles in Emulsified
1.2 This standard does not purport to address all of the
Asphalts (Sieve Test)
safety concerns, if any, associated with its use. It is the
D6997 Test Method for Distillation of Emulsified Asphalt
responsibility of the user of this standard to consult and
3. Significance and Use
establish appropriate safety and health practices and deter-
mine the applicability of regulatory limitations prior to use.
3.1 Recycling of deteriorated asphalt pavements is being
1.3 This practice addresses emulsified materials designed
used as a routine method of maintenance and rehabilitation.
specifically for use in recycling. The use of emulsified mate-
Utilization of existing materials as the major component of this
rials for recycling shall not be limited to this practice. For
procedure may yield benefits in quality, economy, and preser-
instance, the emulsions specified in Specfications D977 and
vation of natural resources. Recycling takes many forms; hot,
D2397 may be used.
cold, in-situ, central plant and surface. This practice may be
used for various recycling methods.
2. Referenced Documents
2
4. Classification
2.1 ASTM Standards:
D5 Test Method for Penetration of Bituminous Materials 4.1 This practice describes emulsified recycling (ER) agents
D70 Test Method for Density of Semi-Solid Bituminous
as belonging to three groups; ER-1, ER-2, and ER-3 as shown
Materials (Pycnometer Method) in Table 1. The range of recycling methods demands several
D140 Practice for Sampling Bituminous Materials
emulsified recycling agents. The groups should provide ad-
D244 Test Methods and Practices for Emulsified Asphalts equate freedom of selection for most recycling methods.
D977 Specification for Emulsified Asphalt
4.1.1 ER-1 is a material whose main function is to rejuve-
D1754 Test Method for Effects of Heat andAir onAsphaltic nate aged asphalt. The material is a petroleum derivative, and
Materials (Thin-Film Oven Test)
highly compatible with asphalts. It is classified by viscosity.
D2007 Test Method for Characteristic Groups in Rubber 4.1.2 ER-2 and ER-3 are materials that combine rejuvena-
Extender and Processing Oils and Other Petroleum-
tors and asphalt components in one emulsion. These soft
Derived Oils by the Clay-Gel Absorption Chromato- residues are classified by low temperature penetration after
graphic Method
aging. They are typically used in recycling where there is an
D2042 Test Method for Solubility of Asphalt Materials in increased demand for bitumen as when new aggregates are
Trichloroethylene added, or where immediate cohesiveness is desired.
D2170 Test Method for Kinematic Viscosity of Asphalts
4.2 The choice of ER will be determined by the consistency
(Bitumens)
of the binder in the aged pavement, the methods of recycling
planned, the amount, if any, of new aggregates, and other
1 design needs.
This practice is under the jurisdiction of ASTM Committee D04 on Road and
Paving Materials and is the direct responsibility of Subcommittee D04.41 on
5. Properties
Emulsified Asphalt Specifications.
Current edition approved Dec. 1, 2006. Published December 2006. Originally
5.1 All emulsified recycling agents shall be homogenous,
approved in 1994. Last previous edition approved in 2001 as D5505 – 97 (2001).
free flowing at pumping temperature, and shall conform to the
DOI: 10.1520/D5505-06.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or requirements of Table 1.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
5.2 Emulsified recycling agent residue should be combined
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. with aged asphalts and evaluated to determine proper ER
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5505−06
TABLE 1 Specifica
...

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ASTM D5505-14(2020)(Practice)
Standard Practice for Classifying Emulsified Recycling Agents

SIGNIFICANCE AND USE
3.1 Recycling of deteriorated asphalt pavements is being used as a routine method of maintenance and rehabilitation. Utilization of existing materials as the major component of this procedure may yield benefits in quality, economy, and preservation of natural resources. Recycling takes many forms: hot, cold, in-situ, central plant, and surface. This practice may be used for various recycling methods.  
3.2 This practice describes emulsified recycling (ER) agents as belonging to three groups: ER-1, ER-2, and ER-3 as shown in Table 1. The range of recycling methods demands several emulsified recycling agents. The groups should provide adequate freedom of selection for most recycling methods. (A) ER-1 shall be certified for dilution with potable water.(B) This specification allows a variety of emulsified asphalts. The engineer should take the steps necessary to keep incompatible materials from co-mingling in tanks or other vessels. It would be prudent to have the chemical charge nature certified by the supplier.(C) RTFO shall be the referee method. When approved by the engineer, the thin-film oven test (Test Method D1754/D1754M) may be substituted for compliance testing.  
3.2.1 ER-1 is a material whose main function is to rejuvenate aged asphalt. The material is a petroleum derivative, and highly compatible with asphalts. It is classified by viscosity.  
3.2.2 ER-2 and ER-3 are materials that combine rejuvenators and asphalt components in one emulsified asphalt. These soft residues are classified by low temperature penetration after aging. They are typically used in recycling where there is an increased demand for asphalt as when new aggregates are added, or where immediate cohesiveness is desired.  
3.3 The choice of ER will be determined by the properties of the asphalt binder in the aged pavement, the methods of recycling planned, the amount, if any, of new aggregates, and other design needs.
SCOPE
1.1 This practice identifies emulsified petroleum products that may be used as recycling agents in recycled mixes. These materials are classified by viscosity or by low temperature penetration after aging.  
1.2 This practice addresses emulsified materials designed specifically for use in recycling. The use of emulsified materials for recycling shall not be limited to this practice. For instance, the emulsified asphalts specified in Specifications D977 and D2397/D2397M may be used.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D1159-23(Test Method)
Standard Test Method for Bromine Numbers of Petroleum Distillates and Commercial Aliphatic Olefins by Electrometric Titration

SIGNIFICANCE AND USE
5.1 The bromine number is useful as a measure of aliphatic unsaturation in petroleum samples. When used in conjunction with the calculation procedure described in Annex A2, it can be used to estimate the percentage of olefins in petroleum distillates boiling up to approximately 315 °C (600 °F).  
5.2 The bromine number of commercial aliphatic monoolefins provides supporting evidence of their purity and identity.
SCOPE
1.1 This test method3 covers the determination of the bromine number of the following materials:  
1.1.1 Petroleum distillates that are substantially free of material lighter than isobutane and that have 90 % distillation points (by Test Method D86) under 327 °C (626 °F). This test method is generally applicable to gasoline (including leaded, unleaded, and oxygenated fuels), kerosine, and distillates in the gas oil range that fall in the following limits:    
90 % Distillation Point, °C (°F)  
Bromine Number, max3    
Under 205 (400)  
175    
205 to 327 (400 to 626)  
10  
1.1.2 Commercial olefins that are essentially mixtures of aliphatic mono-olefins and that fall within the range of 95 to 165 bromine number (see Note 1). This test method has been found suitable for such materials as commercial propylene trimer and tetramer, butene dimer, and mixed nonenes, octenes, and heptenes. This test method is not satisfactory for normal alpha-olefins.  
Note 1: These limits are imposed since the precision of this test method has been determined only up to or within the range of these bromine numbers.  
1.2 The magnitude of the bromine number is an indication of the quantity of bromine-reactive constituents, not an identification of constituents; therefore, its application as a measure of olefinic unsaturation should not be undertaken without the study given in Annex A1.  
1.3 For petroleum hydrocarbon mixtures of bromine number less than 1.0, a more precise measure for bromine-reactive constituents can be obtained by using Test Method D2710. If the bromine number is less than 0.5, then Test Method D2710 or the comparable bromine index methods for industrial aromatic hydrocarbons, Test Methods D1492 or D5776 must be used in accordance with their respective scopes. The practice of using a factor of 1000 to convert bromine number to bromine index is not applicable for these lower values of bromine number.  
1.4 The values stated in SI units are to be regarded as the standard.  
1.4.1 Exception—The values given in parentheses are for information only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Sections 7, 8, and 9.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D6792-23c(Practice)
Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories

SIGNIFICANCE AND USE
4.1 A petroleum products, liquid fuels, and lubricants testing laboratory plays a crucial role in product quality management and customer satisfaction. It is essential for a laboratory to provide quality data. This document provides guidance for establishing and maintaining a quality management system in a laboratory.  
4.1.1 The word ‘customer’ can refer to both customers internal and external to the laboratory or organization.
SCOPE
1.1 This practice covers the establishment and maintenance of the essentials of a quality management system in laboratories engaged in the analysis of petroleum products, liquid fuels, and lubricants. It is designed to be used in conjunction with Practice D6299.
Note 1: This practice is based on the quality management concepts and principles advocated in ANSI/ISO/ASQ Q9000 standards, ISO/IEC 17025, ASQ Manual,2 and ASTM standards such as D3244, D4182, D4621, D6299, D6300, D7372, E29, E177, E456, E548, E882, E994, E1301, E1323, STP 15D,3 and STP 1209.4  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory requirements prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D3235-23(Test Method)
Standard Test Method for Solvent Extractables in Petroleum Waxes

SIGNIFICANCE AND USE
5.1 The solvent extractables in a wax may have significant effects on several of its properties such as strength, hardness, flexibility, scuff resistance, coefficient of friction, coefficient of expansion, melting point, and staining characteristics. Whether these effects are desirable or undesirable depends on the intended use of the wax.
SCOPE
1.1 This test method covers the determination of solvent extractables in petroleum waxes.  
1.2 The values stated in SI units are to be regarded as standard.  
1.2.1 Exception—The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D7873-22a(Test Method)
Standard Test Method for Determination of Oxidation Stability and Insolubles Formation of Inhibited Turbine Oils at 120 °C Without the Inclusion of Water (Dry TOST Method)

SIGNIFICANCE AND USE
5.1 Insoluble material may form in oils that are subjected to oxidizing conditions.  
5.2 Significant formation of oil insolubles or metal corrosion products, or both, during this test may indicate that the oil will form insolubles or corrode metals, or both, resulting in varnish formation during field service. The level of varnish formation in service will be dependent on many factors (turbine design, reservoir temperature, duty-cycle, for example. peaking, cycling, or base-load duty, maintenance, and so forth) and a direct correlation between results in this test and field varnish formation are yet to be established.  
5.3 Oxidation condition at 120 °C under accelerated oxidation environment of Test Method D4310 and measurement of sludge and RPVOT value could reflect a practical oil quality in actual turbine operations. Results from this test should be used together with other key lubricant performance indicators (including other established oxidation and corrosion tests) to indicate suitability for service.
SCOPE
1.1 This test method is used to evaluate the sludging tendencies of steam and gas turbine lubricants during the oxidation process in the presence of oxygen and metal catalyst (copper and iron) at an elevated temperature. This test method may be used to evaluate industrial oils (for example, circulating oils and so forth).  
1.2 This test method is a modification of Test Method D4310 where the sludging and corrosion tendencies of the same kinds of oils are determined after 1000 h at 95 °C in the presence of water. Water is omitted in this modification.  
1.3 The values stated in SI units are to be regarded as standard.  
1.3.1 Exception—The values in parentheses in some of the figures are provided for information only for those using old equipment based on non-SI units.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.  
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ASTM D974-22(Test Method)
Standard Test Method for Acid and Base Number by Color-Indicator Titration

SIGNIFICANCE AND USE
5.1 New and used petroleum products can contain basic or acidic constituents that are present as additives or as degradation products formed during service, such as oxidation products. The relative amount of these materials can be determined by titrating with acids or bases. This number, whether expressed as acid number or base number, is a measure of this amount of acidic or basic substances, respectively, in the oil—always under the conditions of the test. This number is used as a guide in the quality control of lubricating oil formulations. It is also sometimes used as a measure of lubricant degradation in service; however, any condemning limits must be empirically established.  
5.2 Since a variety of oxidation products contribute to the acid number and the organic acids vary widely in corrosive properties, the test cannot be used to predict corrosiveness of an oil under service conditions. No general correlation is known between acid number and the corrosive tendency of oils toward metals. Compounded engine oils can and usually do have both acid and base numbers in this test method.
SCOPE
1.1 This test method covers the determination of acidic or basic constituents (Note 1) in petroleum products3 and lubricants soluble or nearly soluble in mixtures of toluene and isopropyl alcohol. It is applicable for the determination of acids or bases whose dissociation constants in water are larger than 10−9; extremely weak acids or bases whose dissociation constants are smaller than 10−9 do not interfere. Salts react if their hydrolysis constants are larger than 10−9.
Note 1: In new and used oils, the constituents considered to have acidic characteristics include organic and inorganic acids, esters, phenolic compounds, lactones, resins, salts of heavy metals, and addition agents such as inhibitors and detergents. Similarly, constituents considered to have basic properties include organic and inorganic bases, amino compounds, salts of weak acids (soaps), basic salts of polyacidic bases, salts of heavy metals, and addition agents such as inhibitors and detergents.
Note 2: This test method is not suitable for measuring the basic constituents of many basic additive-type lubricating oils. Test Method D4739 can be used for this purpose.  
1.2 This test method can be used to indicate relative changes that occur in an oil during use under oxidizing conditions. Although the titration is made under definite equilibrium conditions, the method does not measure an absolute acidic or basic property that can be used to predict performance of an oil under service conditions. No general relationship between bearing corrosion and acid or base numbers is known.  
Note 3: Oils, such as many cutting oils, rustproofing oils, and similar compounded oils, or excessively dark-colored oils, that cannot be analyzed for acid number by this test method due to obscurity of the color-indicator end point, can be analyzed by Test Method D664. The acid numbers obtained by this color-indicator test method need not be numerically the same as those obtained by Test Method D664, the base numbers obtained by this color indicator test method need not be numerically the same as those obtained by Test Method D4739, but they are generally of the same order of magnitude.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations...

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Standard Test Method for Iron Chip Corrosion for Water–Miscible Metalworking Fluids

SIGNIFICANCE AND USE
5.1 The results obtained by this test are a useful guideline in determining the ability of water-miscible metalworking fluids to prevent or minimize rust under specific conditions. There is usually a relationship between the results of this test and a similar ability of the subject coolant to prevent rust on nested parts or in drilled holes containing chips, etc. It must be understood, however, that conditions, metal types, etc. found in practice will not correlate quantitatively with these controlled laboratory conditions. The procedure may not be able to differentiate between two products with poor rust control due to the wide spacing between test dilutions.
SCOPE
1.1 This test method covers evaluation of the ferrous corrosion control characteristics of water–miscible metalworking fluids.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exception—Note 1 contains inch-pound units since the drill sizes and feed rates do not have readily available metric equivalents.  
1.2.2 Exception—U.S. Standard sieve sizes include mesh values.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4177-22e1(Practice)
Standard Practice for Automatic Sampling of Petroleum and Petroleum Products

SIGNIFICANCE AND USE
4.1 Representative samples of petroleum and petroleum products are required for the determination of chemical and physical properties, which are used to establish standard volumes, prices, and compliance with commercial terms and regulatory requirements. This practice does not cover sampling of electrical insulating oils and hydraulic fluids. This practice does not address how to sample crude at temperatures below the freezing point of water.
PART I—General
This part is applicable to all petroleum liquid sampling whether it be crude oil or refined products. Review this section before designing or installing any automatic sampling system.
SCOPE
1.1 This practice describes general procedures and equipment for automatically obtaining samples of liquid petroleum and petroleum products, crude oils, and intermediate products from the sample point into the primary container. This practice also provides additional specific information about sample container selection, preparation, and sample handling. If sampling is for the precise determination of volatility, use Practice D5842 (API MPMS Chapter 8.4) in conjunction with this practice. For sample mixing and handling, refer to Practice D5854 (API MPMS Chapter 8.3). This practice does not cover sampling of electrical insulating oils and hydraulic fluids.  
1.2 Table of Contents:    
Section  
INTRODUCTION  
Scope  
1  
Referenced Documents  
2  
Terminology  
3  
Significance and Use  
4  
PART I–GENERAL  
Representative Sampling Components  
5  
Design Criteria  
6  
Automatic Sampling Systems  
7  
Sampling Location  
8  
Mixing of the Flowing Stream  
9  
Proportionality  
10  
Sample Extractor Grab Volume  
11  
Containers  
12  
Sample Handling and Mixing  
13  
Control Systems  
14  
Sample System Security  
15  
System Proving (Performance Acceptance Tests)  
16  
Performance Monitoring  
17  
PART II–CRUDE OIL  
Crude Oil  
18  
PART III–REFINED PRODUCTS  
Refined Products  
19  
KEYWORDS  
Keywords  
20  
ANNEXES  
Calculations of the Margin of Error based on Number of Sample Grabs  
Annex A1  
Theoretical Calculations for Selecting the Sampler Probe Location  
Annex A2  
Portable Sampling Units  
Annex A3  
Profile Performance Test  
Annex A4  
Sampler Acceptance Test Data  
Annex A5  
APPENDIXES  
Design Data Sheet for Automatic Sampling System  
Appendix X1  
Comparisons of Percent Sediment and Water versus Unloading Time Period  
Appendix X2  
Sampling Frequency and Sampling System Monitoring Spreadsheet  
Appendix X3  
Sampling System Monitoring—Additional Diagnostics  
Appendix X4  
1.3 Units—The values stated in either SI units or US Customary (USC) units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Except where there is no direct SI equivalent, such as for National Pipe Threads/diameters, or tubing.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4057-22(Practice)
Standard Practice for Manual Sampling of Petroleum and Petroleum Products

SIGNIFICANCE AND USE
4.1 Samples of petroleum and petroleum products are obtained for many reasons, including the determination of chemical and physical properties. These properties may be used for: calculating standard volumes; establishing product value; and often safety and regulatory reporting.  
4.2 There are inherent limitations when performing any type of sampling, any one of which may affect the representative nature of the sample. As examples, a spot sample provides a sample from only one particular point in the tank, vessel compartment, or pipeline. In the case of running or all-level samples, the sample only represents the column of material from which it was taken.  
4.3 Based on the product, and testing to be performed, this practice provides guidance on sampling equipment, container preparation, and manual sampling procedures for petroleum and petroleum products of a liquid, semi-liquid, or solid state, from the storage tanks, flowlines, pipelines, marine vessels, process vessels, drums, cans, tubes, bags, kettles, and open discharge streams into the primary sample container.
SCOPE
1.1 This practice covers procedures and equipment for manually obtaining samples of liquid petroleum and petroleum products, crude oils, and intermediate products from the sample point into the primary container are described. Procedures are also included for the sampling of free water and other heavy components associated with petroleum and petroleum products.  
1.2 This practice also addresses the sampling of semi-liquid or solid-state petroleum products. For the sampling of green petroleum coke, see Practice D8145. For the sampling of calcined petroleum coke, see Practice D6970.  
1.3 This practice provides additional specific information about sample container selection, preparation, and sample handling.  
1.4 This practice does not cover sampling of electrical insulating oils and hydraulic fluids. If sampling is for the precise determination of volatility, use Practice D5842 (API MPMS Chapter 8.4) in conjunction with this practice. For sample mixing and handling, refer to Practice D5854 (API MPMS Chapter 8.3).  
1.5 The procedures described in this practice may also be applicable in sampling most non-corrosive liquid industrial chemicals provided that all safety precautions specific to these chemicals are followed. Also, refer to Practice E300. The procedures described in this practice are also applicable to sampling liquefied petroleum gases and chemicals. Also refer to Practices D1265 and D3700. The procedure for sampling bituminous materials is described in Practice D140. Practice D4306 provides guidance on sample containers and preparation for sampling aviation fuel.  
1.6 Units—The values stated in SI units are to be regarded as the standard. USC units are reflected in parentheses.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D5291-21(Test Method)
Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants

SIGNIFICANCE AND USE
5.1 This is the first ASTM standard covering the simultaneous determination of carbon, hydrogen, and nitrogen in petroleum products and lubricants.  
5.2 Carbon, hydrogen, and particularly nitrogen analyses are useful in determining the complex nature of sample types covered by this test method. The CHN results can be used to estimate the processing and refining potentials and yields in the petrochemical industry.  
5.3 The concentration of nitrogen is a measure of the presence of nitrogen containing additives. Knowledge of its concentration can be used to predict performance. Some petroleum products also contain naturally occurring nitrogen. Knowledge of hydrogen content in samples is helpful in addressing their performance characteristics. Hydrogen to carbon ratio is useful to assess the performance of upgrading processes.
SCOPE
1.1 These test methods cover the instrumental determination of carbon, hydrogen, and nitrogen in laboratory samples of petroleum products and lubricants. Values obtained represent the total carbon, the total hydrogen, and the total nitrogen.  
1.2 These test methods are applicable to samples such as crude oils, fuel oils, additives, and residues for carbon and hydrogen and nitrogen analysis. These test methods were tested in the concentration range of at least 75 % to 87 % by mass for carbon, at least 9 % to 16 % by mass for hydrogen, and  
1.3 The nitrogen test method is not applicable to light materials or those containing  
1.3.1 However, using Test Method D levels of 0.1 % by mass nitrogen in lubricants could be determined.  
1.4 These test methods are not recommended for the analysis of volatile materials such as gasoline, gasoline-oxygenate blends, or gasoline type aviation turbine fuels.  
1.5 The results of these tests can be expressed as mass % carbon, hydrogen or nitrogen.  
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
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    English language
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  • Standard
    8 pages
    English language
    sale 15% off