ASTM D1579-01(2008)
(Test Method)Standard Test Method for Filler Content of Phenol, Resorcinol, and Melamine Adhesives
Standard Test Method for Filler Content of Phenol, Resorcinol, and Melamine Adhesives
SIGNIFICANCE AND USE
It is possible to modify the properties of phenol, resorcinol, and melamine-based adhesives by adding fillers to the adhesive and in doing so affect the way the adhesive performs. This test method makes possible accurate determination of these filler levels for purposes of quality control and characterization of the adhesive.
SCOPE
1.1 This test method is suitable for measuring the filler content of phenol, resorcinol, and melamine resin-base adhesives mixed with hardener or catalyst, that set at room, intermediate, and high temperatures. Results are expressed on the basis of the nonvolatile content of the mixed, liquid adhesive.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
General Information
Relations
Buy Standard
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1579 − 01(Reapproved 2008)
Standard Test Method for
Filler Content of Phenol, Resorcinol, and Melamine
1
Adhesives
This standard is issued under the fixed designation D1579; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense. as part of Federal Test Method Standard No.
175a.
1. Scope* performs. This test method makes possible accurate determi-
nation of these filler levels for purposes of quality control and
1.1 This test method is suitable for measuring the filler
characterization of the adhesive.
content of phenol, resorcinol, and melamine resin-base adhe-
sives mixed with hardener or catalyst, that set at room,
5. Apparatus
intermediate, and high temperatures. Results are expressed on
5.1 Erlenmeyer Flask, or beaker, of 100-mL capacity.
the basis of the nonvolatile content of the mixed, liquid
adhesive.
5.2 Analytical Balance, accurate to 0.001 g.
1.2 The values stated in SI units are to be regarded as the
5.3 Circulating-Air Oven, capable of maintaining a tem-
standard. The values given in parentheses are for information
perature of 105 6 1°C (221 6 1.8°F).
only.
5.4 Desiccator, with drying agent and tray.
1.3 This standard does not purport to address all of the
5.5 Sintered Glass Crucible, of coarse or medium porosity.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
6. Sampling
priate safety and health practices and determine the applica-
6.1 Except in special cases, take a sample from each
bility of regulatory limitations prior to use.
component of the adhesive. When possible, use a composite
2. Referenced Documents
sample of each component chosen from three or more separate
2
containers, chosen at random.Also take samples from contain-
2.1 ASTM Standards:
ers which appear to be nonrepresentative and test such samples
D907 Terminology of Adhesives
separately.Placethesamplesimmediatelyinclean,dry,airtight
D1582 Test Method for Nonvolatile Content of Liquid
containers, filled to prevent excessive air space above the
Phenol, Resorcinol, and Melamine Adhesives
adhesive and transported to the testing laboratory. Take pre-
3. Terminology
cautions to reduce evaporation or drying of the adhesive to a
minimum. Mix the adhesive in the can thoroughly if there is a
3.1 Definitions—Many terms used in this test method are
tendency for the materials to separate before a sample is taken.
defined in Terminology D907.
6.2 Test three specimens of each sample, unless otherwise
4. Significance and Use
required.
4.1 It is possible to modify the properties of phenol,
7. Procedure
resorcinol, and melamine-based adhesives by adding fillers to
the adhesive and in doing so affect the way the adhesive
7.1 Mix the adhesive in accordance with the instructions of
the manufacturer.
1
This test method is under the jurisdiction of ASTM Committee D14 on
7.2 Phenol and Resorcinol Base—Accurately weigh to the
Adhesives and is the direct responsibility of Subcommittee D14.30 on Wood
nearest 1 mg approximately2gofthe freshly mixed adhesive
Adhesives.
(cut film adhesives into small pieces approximately 13-mm
Current edition approved April 1, 2008. Published April 2008. Originally
(0.5-in) square before weighing) in a 100-mL beaker or
approved in 1958. Last previous edition approved in 2001 as D1579 – 01. DOI:
10.1520/D1579-01R08.
Erlenmeyer flask, add 50-mL of absolute methyl alcohol, and
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
stir the mixture thoroughly for 3 min. Filter the mixture
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
promptly through a previously weighed, sintered glass crucible
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. of coarse or medium porosity and wash the contents of the
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D1579 − 01 (2008)
beaker onto the filter with another 50-mL portion of methyl where:
alcohol.Wash the residue in the crucible with at least 50-mLof
r = weight of insoluble residue,
boiling distilled water, dry to approximately constant weight at
a = weight of adhesive sample, and
n = % nonvolatile content/100.
105 6 1°C (221 6 1.8°F), cool in a desiccator, and weigh
accurately.
8.2 Melamine Base Adhesives—Consider the insoluble resi-
due
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D1579–97 Designation: D 1579 – 01 (Reapproved 2008)
Standard Test Method for
Filler Content of Phenol, Resorcinol, and Melamine
1
Adhesives
This standard is issued under the fixed designation D 1579; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense. , as part of Federal Test Method Standard No. 175a.
1. Scope*
1.1 This test method is suitable for measuring the filler content of phenol, resorcinol, and melamine resin-base adhesives mixed
with hardener or catalyst, that set at room, intermediate, and high temperatures. Results are expressed on the basis of the
nonvolatile content of the mixed, liquid adhesive.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D 907 Terminology of Adhesives
D 1582 Test Method for Nonvolatile Content of Liquid Phenol, Resorcinol, and Melamine Adhesives
3. Terminology
3.1 Definitions—Many of the terms used in this test method are defined in Terminology D 907.
3.1.1filler, n—a relatively nonadhesive substance added to an adhesive to improve its working properties, permanence, strength,
or other qualities. (See also binder and extender.)
4. Significance and Use
4.1 It is possible to modify the properties of phenol, resorcinol, and melamine-based adhesives by adding fillers to the adhesive
and in doing so affect the way the adhesive performs. This test method makes possible accurate determination of these filler levels
for purposes of quality control and characterization of the adhesive.
5. Apparatus
5.1 Erlenmeyer Flask, or beaker, of 100-mL capacity.
5.2 Analytical Balance, accurate to 0.001 g.
5.3 Circulating-Air Oven, capable of maintaining a temperature of 105 6 1°C (221 6 1.8°F).
5.4 Desiccator, with drying agent and tray.
5.5 Sintered Glass Crucible, of coarse or medium porosity.
6. Sampling
6.1 Exceptinspecialcases,takeasamplefromeachcomponentoftheadhesive.Whenpossible,useacompositesampleofeach
component chosen from three or more separate containers, chosen at random.Also take samples from containers which appear to
be nonrepresentative and test such samples separately. Place the samples immediately in clean, dry, airtight containers, filled to
prevent excessive air space above the adhesive and transported to the testing laboratory. Take precautions to reduce evaporation
1
This test method is under the jurisdiction of the ASTM Committee D-14 on Adhesives and is the direct responsibility of Subcommittee D14.30 on Wood Adhesives.
Current edition approved March 10, 1997. Published April 1998. Originally published as D1579–58. Last previous edition D1579–92.
1
This test method is under the jurisdiction of ASTM Committee D14 on Adhesives and is the direct responsibility of Subcommittee D14.30 on Wood Adhesives.
Current edition approved April 1, 2008. Published April 2008. Originally approved in 1958. Last previous edition approved in 2001 as D 1579 – 01.
2
Annual Book of ASTM Standards, Vol 15.06.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
---------------------- Page: 1 ----------------------
D 1579 – 01 (2008)
or drying of the adhesive to a minimum. Mix the adhesive in the can thoroughly if there is a tendency for the materials to separate
before a sample is taken.
6.2 Test three specimens of each sample, unless otherwise required.
7. Procedure
7.1 Mix the adhesive in accordance with the instructions of the manufacturer.
7.2 Phenol and Resorcinol Base—Accurately weigh to the nearest 1 mg approximately2gofthe freshly mixed adhesi
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.