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ASTM D5325-03(2021)

(Test Method)

Standard Test Method for Determination of Weight Percent Volatile Content of Water-Borne Aerosol Paints

Standard Test Method for Determination of Weight Percent Volatile Content of Water-Borne Aerosol Paints

SIGNIFICANCE AND USE
4.1 Calculation of the weight percent volatile organic content of water-borne paints, requires that the water content be known. This test method provides a direct way to determine the weight percent volatile organic matter of water-borne aerosol paints minus the matter content. This test method is modeled after Method 36.4
SCOPE
1.1 This test method is for the determination of the weight percent volatile content of water-borne paints in aerosols.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Jan-2021
ICS
87.040 - Paints and varnishes
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.21 - Chemical Analysis of Paints and Paint Materials
Current Stage
Ref Project

Relations

Refers
ASTM D2369-24 - Standard Test Method for Volatile Content of Coatings
Effective Date
01-Feb-2024
Refers
ASTM D2369-10(2015)e1 - Standard Test Method for Volatile Content of Coatings
Effective Date
01-Jun-2015
Refers
ASTM D3792-05(2015) - Standard Test Method for Water Content of Coatings by Direct Injection Into a Gas Chromatograph
Effective Date
01-Jun-2015
Refers
ASTM D2369-10e1 - Standard Test Method for Volatile Content of Coatings
Effective Date
01-Jul-2011
Refers
ASTM D2369-10 - Standard Test Method for Volatile Content of Coatings
Effective Date
01-Jul-2010
Refers
ASTM D3792-05(2009) - Standard Test Method for Water Content of Coatings by Direct Injection Into a Gas Chromatograph
Effective Date
01-Jun-2009
Refers
ASTM D4017-02(2008)e1 - Standard Test Method for Water in Paints and Paint Materials by Karl Fischer Method
Effective Date
01-Feb-2008
Refers
ASTM D2369-07 - Standard Test Method for Volatile Content of Coatings
Effective Date
01-Jul-2007
Refers
ASTM D3792-05 - Standard Test Method for Water Content of Coatings by Direct Injection Into a Gas Chromatograph
Effective Date
01-Jan-2005
Refers
ASTM D2369-04 - Standard Test Method for Volatile Content of Coatings
Effective Date
01-Mar-2004
Refers
ASTM D2369-03 - Standard Test Method for Volatile Content of Coatings
Effective Date
10-Jan-2003
Refers
ASTM D4017-02 - Standard Test Method for Water in Paints and Paint Materials by Karl Fischer Method
Effective Date
10-Jan-2002
Refers
ASTM D4017-96a - Standard Test Method for Water in Paints and Paint Materials by Karl Fischer Method
Effective Date
10-Jan-2002
Refers
ASTM D2369-01 - Standard Test Method for Volatile Content of Coatings
Effective Date
10-Jan-2001
Refers
ASTM D2369-98 - Standard Test Method for Volatile Content of Coatings
Effective Date
10-Jan-2001

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ASTM D5325-03(2021) - Standard Test Method for Determination of Weight Percent Volatile Content of Water-Borne Aerosol PaintsASTM D5325-03(2021) - Standard Test Method for Determination of Weight Percent Volatile Content of Water-Borne Aerosol Paints
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ASTM D5325-03(2021) - Standard Test Method for Determination of Weight Percent Volatile Content of Water-Borne Aerosol Paints
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D5325 − 03 (Reapproved 2021)
Standard Test Method for
Determination of Weight Percent Volatile Content of Water-
Borne Aerosol Paints
This standard is issued under the fixed designation D5325; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2.2 Other Standard:
Method36 DeterminationofPercentVolatileOrganicCom-
1.1 This test method is for the determination of the weight
pounds (VOC) in Water Based Aerosol Paints
percent volatile content of water-borne paints in aerosols.
3. Summary of Test Method
1.2 The values stated in SI units are to be regarded as
standard. No other units of measurement are included in this 3.1 The propellant is released from the can and the content
remaining is tested for percent water and nonvolatiles.
standard.
1.3 This standard does not purport to address all of the
4. Significance and Use
safety concerns, if any, associated with its use. It is the
4.1 Calculation of the weight percent volatile organic con-
responsibility of the user of this standard to establish appro-
tent of water-borne paints, requires that the water content be
priate safety, health, and environmental practices and deter-
known.Thistestmethodprovidesadirectwaytodeterminethe
mine the applicability of regulatory limitations prior to use.
weight percent volatile organic matter of water-borne aerosol
1.4 This international standard was developed in accor-
paints minus the matter content. This test method is modeled
dance with internationally recognized principles on standard-
after Method36.
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom- 5. Apparatus
mendations issued by the World Trade Organization Technical
5.1 Freezer.
Barriers to Trade (TBT) Committee.
5.2 Ice Pick.
5.3 Hammer.
2. Referenced Documents
5.4 Applicator Sticks.
2.1 ASTM Standards:
D2369Test Method for Volatile Content of Coatings 5.5 Masking Tape.
D3792TestMethodforWaterContentofCoatingsbyDirect
5.6 Tin Snips or Metal Cutter.
Injection Into a Gas Chromatograph
5.7 Shaker, similar to Eberbach shaker in Fig. 1.
D4017Test Method for Water in Paints and Paint Materials
by Karl Fischer Method
6. Procedure
E180Practice for Determining the Precision of ASTM
6.1 Preparation of Aerosol Contents for Analysis:
Methods for Analysis and Testing of Industrial and Spe-
3 6.1.1 Mix the aerosol paint container thoroughly for about
cialty Chemicals (Withdrawn 2009)
15min,usingashakersimilartotheEberbachshakershownin
Fig. 1, at the low speed setting. It is essential that the samples
be well mixed to obtain valid results.
This test method is under the jurisdiction of ASTM Committee D01 on Paint
6.1.2 Removethecapandactuatorfromthecan.Putthecap
and Related Coatings, Materials, andApplications and is the direct responsibility of
on the can and weigh the can to 0.01 g.
Subcommittee D01.21 on Chemical Analysis of Paints and Paint Materials.
6.1.3 Place the can in an upside down position in a freezer
Current edition approved Feb. 1, 2021. Published February 2021. Originally
approved in 1992. Last previous edition approved in 2014 as D5325–03 (2014).
for2hata temperature that is 0°C.
DOI: 10.1520/D5325-03R21.
6.1.4 Put the can upside down in a fume hood. Puncture the
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
bottom of the can near the edge with a very sharp ice pick.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
3 4
The last approved version of this historical standard is referenced on Bay Area Air Quality Management District, (BAAQMD) Manual of
www.astm.org. Procedures, Vol III, 939 Ellis St., San Francisco, CA 94109.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D5325 − 03 (2021)
W =W −W ,
5 2 3
W = total weight of aerosol container plus contents, g,
W = total weight of aerosol
...

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SCOPE
1.1 This test method is a standardized brushout procedure for comparing the brush drag of architectural type solvent-borne paints.  
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5.1 Coatings attached to substrates are subjected to damaging impacts during the manufacture of articles and their use in service. In its use over many years, this test method for impact resistance has been found to be useful in predicting the performance of organic coatings for their ability to resist cracking caused by impacts.
SCOPE
1.1 This test method covers a procedure for rapidly deforming by impact a coating film and its substrate and for evaluating the effect of such deformation.  
1.2 This test method should be restricted to testing in only one laboratory when numerical values are used because of the poor reproducibility of the method. Interlaboratory agreement is improved when ranking is used in place of numerical values.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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