Standard Practice for Separation of Vehicle From Solvent-Reducible Paints

SIGNIFICANCE AND USE
Separation of the vehicle from the pigment in solvent-reducible paints is required in order to characterize paint vehicles by chemical, spectroscopic, or chromatographic techniques. Characterization of vehicles is important since they play a major role in the performance of coatings.
SCOPE
1.1 This practice covers the procedure for the separation of the vehicle from the pigment in solvent-reducible paint.
1.2 In the development of the practice the following materials were tested: white soya and white fish oil isophthalic alkyd semi-gloss enamels, white linseed oil paint, white soya and white linseed o-phthalic alkyd enamels. It is considered to be applicable to similar materials.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-May-2010
Current Stage
Ref Project

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ASTM D2372-85(2010) - Standard Practice for Separation of Vehicle From Solvent-Reducible Paints
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D2372 − 85 (Reapproved2010)
Standard Practice for
Separation of Vehicle From Solvent-Reducible Paints
This standard is issued under the fixed designation D2372; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 3. Significance and Use
1.1 This practice covers the procedure for the separation of 3.1 Separation of the vehicle from the pigment in solvent-
the vehicle from the pigment in solvent-reducible paint. reducible paints is required in order to characterize paint
vehicles by chemical, spectroscopic, or chromatographic tech-
1.2 In the development of the practice the following mate-
niques. Characterization of vehicles is important since they
rials were tested: white soya and white fish oil isophthalic
play a major role in the performance of coatings.
alkyd semi-gloss enamels, white linseed oil paint, white soya
and white linseed o-phthalic alkyd enamels. It is considered to
4. Apparatus
be applicable to similar materials.
4.1 Centrifuge, high-speed, capable of developing in excess
1.3 The values stated in SI units are to be regarded as
of 10 000 g.
standard. No other units of measurement are included in this
NOTE 1—Calculate the gravity developed by the centrifuge as follows:
standard.
26 2
g 5 1.118 310 3r 3n (1)
1.4 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
where:
responsibility of the user of this standard to establish appro-
r = rotating radius, mm, and
priate safety and health practices and determine the applica- n = rotating speed, r/min.
bility of regulatory limitations prior to use.
5. Procedure
NOTE 2—If the percent of pigment is desired, see Test Method D2371
2. Referenced Documents
and Test Method D2698.
2.1 ASTM Standards:
5.1 Mix the sample until it is homogeneous, preferably on a
D2371 Test Method for Pigment Content of Solvent-
mechanical shaker.
Reducible Paints
5.2 Centrifuge about 20 mL of the whole paint on a
D2698 Test Method for Determination of the Pigment Con-
high-speed centrifuge in excess of 10 000 g (Note 1) for 30
tent of Solvent-Reducible Paints by High-Speed Centri-
min or until separation is completed. If difficulty is
fuging
encountered, add 10 mL of a suitab
...

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