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ASTM D4142-89(1996)e1

(Guide)

Standard Guide for Testing Epoxy Resins

Standard Guide for Testing Epoxy Resins

SCOPE
1.1 This guide covers methods for testing epoxy resins as listed in Table 1. All of the methods were tested by interlaboratory participation in accordance with usual ASTM guidelines. Each method specifies a recommended amount of sample for starting a separate analysis, but several of the procedures can be conducted on the same starting material if so desired. For example, viscosity, color, and density could be run on the same specimen.
1.2  This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
27-Apr-1989
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.33 - Polymers and Resins
Current Stage
Ref Project

Relations

Replaced By
ASTM D4142-89(2001) - Standard Guide for Testing Epoxy Resins
Effective Date
28-Apr-1989
Referred By
ASTM D6412/D6412M-99(2020) - Standard Specification for Epoxy (Flexible) Adhesive For Bonding Metallic And Nonmetallic Materials
Effective Date
28-Apr-1989

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ASTM D4142-89(1996)e1 - Standard Guide for Testing Epoxy ResinsASTM D4142-89(1996)e1 - Standard Guide for Testing Epoxy Resins
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ASTM D4142-89(1996)e1 - Standard Guide for Testing Epoxy Resins
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NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
e1
Designation: D 4142 – 89 (Reapproved 1996)
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
Standard Guide for
Testing Epoxy Resins
This standard is issued under the fixed designation D 4142; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
e NOTE—Keywords were added editorially in October 1996.
TABLE 1 Methods for Testing Epoxy Resins
1. Scope
Test Method Section ASTM Designation
1.1 This guide covers methods for testing epoxy resins as
Epoxy content 4 D 1652
listed in Table 1. All of the methods were tested by interlabo-
Hydrolyzable chlorine 5 D 1726
ratory participation in accordance with usual ASTM guide-
Total chlorine 6 D 1847
lines. Each method specifies a recommended amount of sample
Viscosity 7 D 445, D1545
Color 8 D 1544, D1209
for starting a separate analysis, but several of the procedures
Density 9 D 1475
can be conducted on the same starting material if so desired.
Nonvolatile content 10 D 1259
For example, viscosity, color, and density could be run on the
Acid value 11 D 1639
same specimen.
1.2 This standard does not purport to address all of the D 1847 Test Methods for Total Chlorine Content of Epoxy
safety concerns, if any, associated with its use. It is the Resins
responsibility of the user of this standard to establish appro-
3. Significance and Use
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. 3.1 This guide directs the user to test methods that deter-
mine properties generally accepted as standard test items for
2. Referenced Documents
clasification of epoxy resins.
2.1 ASTM Standards:
4. Epoxy Content
D 445 Test Method for Kinematic Viscosity of Transparent
and Opaque Liquids (and the Calculation of Dynamic 4.1 The epoxy content of epoxy resins is determined by
reacting a solution of the resin with a standard solution of
Viscosity)
hydrogen bromide in glacial acetic acid. The quantity of acid
D 1209 Test Method for Color of Clear Liquids (Platinum-
consumed is a measure of the epoxy content. Test Methods
Cobalt Scale)
D 1652 was found to have a repeatability of 2 % of the epoxy
D 1259 Test Methods for Nonvolatile Content of Resin
content and a reproducibility of 6 % of the epoxy content.
Solutions
D 1475 Test Method for Density of Paint, Varnish, Lacquer,
5. Hydrolyzable Chlorine
and Related Products
5.1 Test Method D 1726 covers the determination of the
D 1544 Test Method for Color of Transparent Liquids
easily hydrolyzable chlorine content of liquid epoxy resins in
(Gardner Color Scale)
concentrations below 1 weight %. The specimen is refluxed
D 1545 Test Method for Viscosity of Transparent Liquids
with a known amount of a standard alcoholic potassium
by Bubble Time Method
hydroxide solution. The amount of hydroxide consumed is
D 1639 Test Method for Acid Value of Organic Coating
measured by titration and corresponds to the hydrolyzable
Materials
chlorine content of the resin. By interlaboratory testing, the
D 1652 Test Method for Epoxy Content of Epoxy Resins
repeatability was found to be 0.02 %, and the reproducibility
D 1726 Test Method for Hydrolyzable Chlorine Content of
was found to be 0.05 %, both absolute.
Liquid Epoxy Resins
6. Total Chlorine
This guide is under the jurisdiction of ASTM Committee D-1 on Paint and
6.1 Organic and inorganic chlorine compounds are deter-
Related Coatings, Materials, and Applications and is the direct responsibility of
mined in epoxy resins in accordance with Test Methods
Subcommittee D01.33 on Polymers and Resins.
Current edition approved April 28, 1989. Published June 1989. Originally D 1847. The resin specimen is oxidized by combustion in a
e1
published as D 4142 – 82. Last previous edition D 4142 – 82 .
bomb containing oxygen under pressure. The chlorides formed
Annual Book of ASTM Standards, Vol 05.01.
a
...

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4.1 Flash X-ray facilities provide intense bremsstrahlung radiation environments, usually in a single sub-microsecond pulse, which often fluctuates in amplitude, shape, and spectrum from shot to shot. Therefore, appropriate dosimetry must be fielded on every exposure to characterize the environment, see ICRU Report 34. These intense bremsstrahlung sources have a variety of applications which include the following:
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1.3 Assistance is provided to relate the measured dose to the response of a device under test (DUT). The device is assumed to be a semiconductor electronic part or system.  
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ASTM D396-24(Specification)
Standard Specification for Fuel Oils

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This specification covers grades of fuel oil intended for use in various types of fuel-oil-burning equipment under various climatic and operating conditions. These grades include the following: Grades No. 1 S5000, No. 1 S500, No. 2 S5000, and No. 2 S500 for use in domestic and small industrial burners; Grades No. 1 S5000 and No. 1 S500 adapted to vaporizing type burners or where storage conditions require low pour point fuel; Grades No. 4 (Light) and No. 4 (Heavy) for use in commercial/industrial burners; and Grades No. 5 (Light), No. 5 (Heavy), and No. 6 for use in industrial burners. Preheating is usually required for handling and proper atomization. The grades of fuel oil shall be homogeneous hydrocarbon oils, free from inorganic acid, and free from excessive amounts of solid or fibrous foreign matter. Grades containing residual components shall remain uniform in normal storage and not separate by gravity into light and heavy oil components outside the viscosity limits for the grade. The grades of fuel oil shall conform to the limiting requirements prescribed for: (1) flash point, (2) water and sediment, (3) physical distillation or simulated distillation, (4) kinematic viscosity, (5) Ramsbottom carbon residue, (6) ash, (7) sulfur, (8) copper strip corrosion, (9) density, and (10) pour point. The test methods for determining conformance to the specified properties are given.
SCOPE
1.1 This specification (see Note 1) covers grades of fuel oil intended for use in various types of fuel-oil-burning equipment under various climatic and operating conditions. These grades are described as follows:  
1.1.1 Grades No. 1 S5000, No. 1 S500, No. 1 S15, No. 2 S5000, No. 2 S500, and No. 2 S15 are middle distillate fuels for use in domestic and small industrial burners. Grades No. 1 S5000, No. 1 S500, and No. 1 S15 are particularly adapted to vaporizing type burners or where storage conditions require low pour point fuel.  
1.1.2 Grades B6–B20 S5000, B6–B20 S500, and B6–B20 S15 are middle distillate fuel/biodiesel blends for use in domestic and small industrial burners.  
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1.1.4 Grades No. 5 (Light), No. 5 (Heavy), and No. 6 are residual fuels of increasing viscosity and boiling range, used in industrial burners. Preheating is usually required for handling and proper atomization.  
Note 1: For information on the significance of the terminology and test methods used in this specification, see Appendix X1.
Note 2: A more detailed description of the grades of fuel oils is given in X1.3.  
1.2 This specification is for the use of purchasing agencies in formulating specifications to be included in contracts for purchases of fuel oils and for the guidance of consumers of fuel oils in the selection of the grades most suitable for their needs.  
1.3 Nothing in this specification shall preclude observance of federal, state, or local regulations which can be more restrictive.  
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1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D8165-24(Test Method)
Standard Test Method for Evaluation of Load-Carrying Capacity of Lubricants Used in Hypoid Final-Drive Axles Operated under Low-Speed and High-Torque Conditions

SIGNIFICANCE AND USE
5.1 This test method measures a lubricant's ability to protect hypoid final drive axles from abrasive wear, adhesive wear, plastic deformation, and surface fatigue when subjected to low-speed, high-torque conditions. Lack of protection can lead to premature gear or bearing failure, or both.  
5.2 This test method is used, or referred to, in specifications and classifications of rear-axle gear lubricants such as:  
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1.2.1 Exceptions—Where there is no direct SI equivalent such as National Pipe threads/diameters, tubing size, or where there is a sole source supply equipment specification.
1.2.1.1 The drawing in Annex A6 is in inch-pound units.  
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Standard Practice for Ultrasonic Examination of Turbine and Generator Steel Rotor Forgings

SIGNIFICANCE AND USE
4.1 This practice shall be used when ultrasonic inspection is required by the order or specification for inspection purposes where the acceptance of the forging is based on limitations of the number, amplitude, or location of discontinuities, or a combination thereof, which give rise to ultrasonic indications.  
4.2 The acceptance criteria shall be clearly stated as order requirements.
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1.1 This practice for ultrasonic examination covers turbine and generator steel rotor forgings covered by Specifications A469/A469M, A470/A470M, A768/A768M, and A940/A940M. This practice shall be used for contact testing only.  
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1.3 This practice is intended to provide a means of inspecting cylindrical forgings so that the inspection sensitivity at the forging center line or bore surface is constant, independent of the forging or bore diameter. To this end, inspection sensitivity multiplication factors have been computed from theoretical analysis, with experimental verification. These are plotted in Fig. 1 (bored rotors) and Fig. 2 (solid rotors), for a true inspection frequency of 2.25 MHz, and an acoustic velocity of 2.30 in./s × 105 in./s [5.85 cm/s × 105 cm/s]. Means of converting to other sensitivity levels are provided in Fig. 3. (Sensitivity multiplication factors for other frequencies may be derived in accordance with X1.1 and X1.2 of Appendix X1.)  
FIG. 1 Bored Forgings
Note 1: Sensitivity multiplication factor such that a 10 % indication at the forging bore surface will be equivalent to a 1/8 in. [3 mm] diameter flat bottom hole. Inspection frequency: 2.0 MHz or 2.25 MHz. Material velocity: 2.30 in./s × 105 in./s [5.85 cm/s × 105 cm/s].
FIG. 2 Solid Forgings
Note 1: Sensitivity multiplication factor such that a 10 % indication at the forging centerline surface will be equivalent to a 1/8 in. [3 mm] diameter flat bottom hole. Inspection frequency: 2.0 MHz or 2.25 MHz. Material velocity: 2.30 in./s × 105 in./s [5.85 cm/s × 105 cm/s].
FIG. 3 Conversion Factors to Be Used in Conjunction with Fig. 1 and Fig. 2 if a Change in the Reference Reflector Diameter is Required
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5.1 Often the most critical stress to which a sandwich panel core is subjected is shear. The effect of repeated shear stresses on the core material can be very important, particularly in terms of durability under various environmental conditions.  
5.2 This test method provides a standard method of obtaining the sandwich core shear fatigue response. Uses include screening candidate core materials for a specific application, developing a design-specific core shear cyclic stress limit, and core material research and development.
Note 3: This test method may be used as a guide to conduct spectrum loading. This information can be useful in the understanding of fatigue behavior of core under spectrum loading conditions, but is not covered in this standard.  
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This specification covers coated glass mat water-resistant gypsum backing panel designed for use on ceilings and walls in bath and shower areas as a base for the application of ceramic or plastic tile. Coated glass mat water-resistant gypsum backing panel shall consist of a noncombustible water-resistant gypsum core, surfaced with glass mat, partially or completely embedded in the core, and with a water-resistant coating on one surface. The specimens shall be tested for flexural strength, humidified deflection, core hardness, end hardness, edge hardness, nail pull resistance, water resistance, and surface water absorption. Coated glass mat water-resistant gypsum backing panel shall have surfaces true and free of imperfections that render the panel unfit for its designed use.
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1.1 This specification covers coated glass mat water-resistant gypsum backing panel designed for use on ceilings and walls in bath and shower areas as a base for the application of ceramic or plastic tile.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Within the text, the SI units are shown in brackets.  
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Standard Practice for Polarized Light Detection of Flaws in Aerospace Transparency Heating Elements

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4.1 This practice is useful as a screening basis for acceptance or rejection of transparencies during manufacturing so that units with identifiable flaws will not be carried to final inspection for rejection at that time.  
4.2 This practice may also be employed as a go-no go technique for acceptance or rejection of the finished product.  
4.3 This practice is simple, inexpensive, and effective. Flaws identified by this practice, as with other optical methods, are limited to those that produce temperature gradients when electrically powered. Any other type of flaw, such as minor scratches parallel to the direction of electrical flow, are not detectable.
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1.1 This practice covers a standard procedure for detecting flaws in the conductive coating (heater element) by the observation of polarized light patterns.  
1.2 This practice applies to coatings on surfaces of monolithic transparencies as well as to coatings imbedded in laminated structures.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 6.  
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ASTM C364/C364M-16(2024)(Test Method)
Standard Test Method for Edgewise Compressive Strength of Sandwich Constructions

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5.1 The edgewise compressive strength of short sandwich construction specimens provides a basis for judging the load-carrying capacity of the construction in terms of developed facing stress.  
5.2 This test method provides a standard method of obtaining sandwich edgewise compressive strengths for panel design properties, material specifications, research and development applications, and quality assurance.  
5.3 The reporting section requires items that tend to influence edgewise compressive strength to be reported; these include materials, fabrication method, facesheet lay-up orientation (if composite), core orientation, results of any nondestructive inspections, specimen preparation, test equipment details, specimen dimensions and associated measurement accuracy, environmental conditions, speed of testing, failure mode, and failure location.
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1.1 This test method covers the compressive properties of structural sandwich construction in a direction parallel to the sandwich facing plane. Permissible core material forms include those with continuous bonding surfaces (such as balsa wood and foams) as well as those with discontinuous bonding surfaces (such as honeycomb).  
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This specification covers austenitic steel castings for valves, flanges, fittings, and other pressure-containing parts. The steel shall be made by the electric furnace process with or without separate refining such as argon-oxygen decarburization. All castings shall receive heat treatment followed by quench in water or rapid cool by other means as noted. The steel shall conform to both chemical composition and tensile property requirements.
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1.2 A number of grades of austenitic steel castings are included in this specification. Since these grades possess varying degrees of suitability for service at high temperatures or in corrosive environments, it is the responsibility of the purchaser to determine which grade shall be furnished. Selection will depend on design and service conditions, mechanical properties, and high-temperature or corrosion-resistant characteristics, or both.  
1.2.1 Because of thermal instability, Grades CE20N, CF3A, CF3MA, and CF8A are not recommended for service at temperatures above 800 °F [425 °C].  
1.3 Supplementary requirements of an optional nature are provided for use at the option of the purchaser. The Supplementary requirements shall apply only when specified individually by the purchaser in the purchase order or contract.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.4.1 This specification is expressed in both inch-pound units and in SI units; however, unless the purchase order or contract specifies the applicable M-specification designation (SI units), the inch-pound units shall apply. Within the text, the SI units are shown in brackets or parentheses.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SCOPE
1.1 This specification covers asbestos-free asphalt roof coatings of brushing or spraying consistency.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.3 The following precautionary caveat pertains only to the test method portion, Section 8, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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