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ASTM D4317-98(2004)

(Specification)

Standard Specification for Polyvinyl Acetate-Based Emulsion Adhesives

Standard Specification for Polyvinyl Acetate-Based Emulsion Adhesives

ABSTRACT
This specification covers polyvinyl acetate or polyvinyl acetate copolymer resin emulsion adhesives suitable for use on wood, wood-based substrates, or plastic laminates. This does not cover the group of polyvinyl-based adhesives suitable for bonding flexible films. Adhesives are classified on the basis of water resistance at three performance levels, namely wet-use (Type 1), intermediate use (Type 2), and dry-use (Type 3). Adhesives shall conform to test requirements as performed under the following exposure conditions and treatments: dry shear at specified temperatures; two-cycle boil; 48-hour soak; humidity exposure; freeze-thaw stability; and storage life. Materials shall also adhere to physical properties such as density, nonvolatile matter, and pH.
SCOPE
1.1 This specification covers polyvinyl acetate or polyvinyl acetate copolymer resin emulsion adhesives suitable for use on wood, wood-based substrates, or plastic laminates. It does not cover the group of polyvinyl-based adhesives which are suitable for bonding flexible films.
1.2 The adhesives are classified at three performance levels in accordance with water-resistance as shown in and . See Section for a description of the expected exposure conditions for each class of adhesive. See for a classification of typical end products that are manufactured using adhesives at the three performance levels covered by this specification.
1.3 The following index is provided as a guide to the test methods portion of this specification:SectionTests for Physical PropertiesViscosityDensity NonvolatilespH Tests for Adhesive BondBlock Shear Strength, CompressionPlywood Shear Tests
1.4 The values stated in SI units are to be regarded as the standard. The values given in parenthesis are for information purposes only.
1.5 The following safety hazards caveat pertains only to the test method portion, Sections 9 and 10, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Mar-2004
Technical Committee
D14 - Adhesives
Drafting Committee
D14.30 - Wood Adhesives
Current Stage
Ref Project

Relations

Replaces
ASTM D4317-98 - Standard Specification for Polyvinyl Acetate-Based Emulsion Adhesives
Effective Date
01-Apr-2004
Replaced By
ASTM D4317-98(2011) - Standard Specification for Polyvinyl Acetate-Based Emulsion Adhesives
Effective Date
01-Jan-2011
Referred By
ASTM D907-15(2023) - Standard Terminology of Adhesives
Effective Date
01-Apr-2004
Referred By
ASTM D6465-99(2016) - Standard Guide for Selecting Aerospace and General Purpose Adhesives and Sealants
Effective Date
01-Apr-2004

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ASTM D4317-98(2004) - Standard Specification for Polyvinyl Acetate-Based Emulsion AdhesivesASTM D4317-98(2004) - Standard Specification for Polyvinyl Acetate-Based Emulsion Adhesives
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ASTM D4317-98(2004) - Standard Specification for Polyvinyl Acetate-Based Emulsion Adhesives
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D4317 – 98 (Reapproved 2004)
Standard Specification for
1
Polyvinyl Acetate-Based Emulsion Adhesives
This standard is issued under the fixed designation D4317; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
INTRODUCTION
This specification is a replacement for Federal Specification MMM-A-180C, Class B, August 6,
1979,Adhesive,VinylAcetate Resin Emulsion, which superseded MMM-A-193C, October 26, 1967.
Ithasbeenexpandedtoincludethemorewater-resistantpolyvinylacetate-basedadhesivesnowonthe
market, in addition to the less water-resistant ones formerly covered by the Federal Specification.
1. Scope This standard does not purport to address all of the safety
concerns, if any, associated with its use. It is the responsibility
1.1 This specification covers polyvinyl acetate or polyvinyl
of the user of this standard to establish appropriate safety and
acetatecopolymerresinemulsionadhesivessuitableforuseon
health practices and determine the applicability of regulatory
wood, wood-based substrates, or plastic laminates. It does not
limitations prior to use.
cover the group of polyvinyl-based adhesives which are
suitable for bonding flexible films.
2. Referenced Documents
1.2 The adhesives are classified at three performance levels
2
2.1 ASTM Standards:
in accordance with water-resistance as shown in Table 1 and
D905 Test Method for Strength Properties of Adhesive
Table 2. See Section 5 for a description of the expected
Bonds in Shear by Compression Loading
exposureconditionsforeachclassofadhesive.SeeTableX1.1
D906 Test Method for Strength Properties of Adhesives in
for a classification of typical end products that are manufac-
Plywood Type Construction in Shear by Tension Loading
tured using adhesives at the three performance levels covered
D907 Terminology of Adhesives
by this specification.
D1084 Test Methods for Viscosity of Adhesives
1.3 The following index is provided as a guide to the test
D1490 Test Method for Nonvolatile Content of Urea-
methods portion of this specification:
Formaldehyde Resin Solutions
Section
D1875 TestMethodforDensityofAdhesivesinFluidForm
Tests for Physical Properties 9
D2556 Test Method for Apparent Viscosity of Adhesives
Viscosity 9.1.1
Density 9.1.2 Having Shear-Rate-Dependent Flow Properties
Nonvolatiles 9.1.3
E4 Practices for Force Verification of Testing Machines
pH 9.1.4
E70 Test Method for pH of Aqueous Solutions With the
Tests for Adhesive Bond 10
Block Shear Strength, Compression 10.2 Glass Electrode
Plywood Shear Tests 10.3
2.2 Federal Standards:
3
Fed. Std. No. 123 Marking for Shipment (Civil Agencies)
1.4 The values stated in SI units are to be regarded as the
3
PPP-C-96 Cans, Metal, 28-Gauge and Lighter
standard. The values given in parenthesis are for information
3
PPP-D-723 Drums, Fiber
purposes only.
PPP-D-729 Drums,ShippingandStorage,Steel,55gal(208
1.5 The following safety hazards caveat pertains only to the
3
L)
test method portion, Sections 9 and 10, of this specification:
2
For referenced standards, visit the website, www.org, or contact Customer
1
ThisspecificationisunderthejurisdictionofCommitteeD14onAdhesivesand Service at service@.org. For Annual Book of Standards volume information, refer
is the direct responsibility of Subcommittee D14.30 on Wood Adhesives. to the standard’s Document Summary page on the website.
3
Current edition approved April 1, 2004. Published April 2004. Originally Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
approved in 1984. Last previous edition approved in 1998 as D4317–98. DOI: Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http://
10.1520/D4317-98R04. www.dodssp.daps.mil.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D4317 – 98 (2004)
TABLE 1 Test Requirements
Test Requirement, Required Tests
Test Section Number
min, psi (kPa)
Type 1 Type 2 Type 3
Block shear (compression) dry at 75°F (24°C) 10.2 2800 (19 306) X X X
Plywood (tension):
dry at 75°F (24°C) 10.3.3.1 400 (2 758) X X X
A
dry at 160°F (71.1°C) 10.3.3.2 or 10.3.3.3 250 (1 724) X X X
Two-cycle boil 10.3.3.4 see Table 2 X
48-h soak 10.3.3.5 250 (1 724) X X
A
Humidity exposure 10.3.3.6 250 (1 724) X
B B B B
Freeze-thaw stability 10.3.3.7 optional optional optional
C C C C
Storage life 10.3.3.8 X X X
A
Or 40 % of dry value at 75°F (24°C), whichever is larger.
B
Testing and certification for freeze-thaw stability is optional. To cla
...

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