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ASTM E1852-96(2001)

(Test Method)

Standard Test Method for Determination of Low Levels of Antimony in Carbon and Low-Alloy Steel by Electrothermal Atomic Absorption Spectrometry

Standard Test Method for Determination of Low Levels of Antimony in Carbon and Low-Alloy Steel by Electrothermal Atomic Absorption Spectrometry

SIGNIFICANCE AND USE
This test method is to be used for the determination of trace levels of antimony in carbon and low-alloy steel. It is assumed that the procedure will be performed by trained analysts capable of performing common laboratory practices skillfully and safely. It is expected that the work will be performed in a properly equipped laboratory and proper waste disposal procedures will be followed.
SCOPE
1.1 This test method covers the determination of antimony in carbon and low-alloy steel in the 0.0005 through 0,010% range.  
1.2 If this test method is used to test materials having contents less than 0.001% antimony, users of different laboratories will experience more than the usual 5% risk that their results will differ by more 50% relative error.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Dec-2000
ICS
71.040.50 - Physicochemical methods of analysis
Technical Committee
E01 - Analytical Chemistry for Metals, Ores, and Related Materials
Drafting Committee
E01.01 - Iron, Steel, and Ferroalloys
Current Stage
Ref Project

Relations

Replaces
ASTM E1852-96e1 - Standard Test Method for Determination of Low Levels of Antimony in Carbon and Low-Alloy Steel by Electrothermal Atomic Absorption Spectrometry
Effective Date
01-Jan-2001
Replaced By
ASTM E1852-08 - Standard Test Method for Determination of Low Levels of Antimony in Carbon and Low-Alloy Steel by Graphite Furnace Atomic Absorption Spectrometry
Effective Date
01-Mar-2008

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ASTM E1852-96(2001) - Standard Test Method for Determination of Low Levels of Antimony in Carbon and Low-Alloy Steel by Electrothermal Atomic Absorption SpectrometryASTM E1852-96(2001) - Standard Test Method for Determination of Low Levels of Antimony in Carbon and Low-Alloy Steel by Electrothermal Atomic Absorption Spectrometry
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ASTM E1852-96(2001) - Standard Test Method for Determination of Low Levels of Antimony in Carbon and Low-Alloy Steel by Electrothermal Atomic Absorption Spectrometry
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:E1852–96(Reapproved 2001)
Standard Test Method for
Determination of Low Levels of Antimony in Carbon and
Low-Alloy Steel by Electrothermal Atomic Absorption
1
Spectrometry
This standard is issued under the fixed designation E1852; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope ISO 5725 Precision of Test Methods—Determination of
Repeatability and Reproducibility for a Standard Test
1.1 This test method covers the determination of antimony
3
Method by Inter-Laboratory Tests
in carbon and low-alloy steel in the 0.0005 through 0.010%
ISO 10698 Steel—Determination of Antimony Content—
range.
Electrothermal Atomic Absorption Spectrometric
1.2 If this test method is used to test materials having
3
Method
contents less than 0.001% antimony, users of different labo-
ratories will experience more than the usual 5% risk that their
3. Summary of Test Method
results will differ by more than 50% relative error.
3.1 The sample is dissolved in hydrochloric and nitric acids
1.3 This standard does not purport to address all of the
and diluted to volume. An appropriate aliquot is injected into
safety concerns, if any, associated with its use. It is the
the electrothermal atomizer of an atomic absorption spectrom-
responsibility of the user of this standard to establish appro-
eter, which is equipped with a background correction. The
priate safety and health practices and determine the applica-
sample is dried, pyrolized, and atomized. The absorbance of
bility of regulatory limitations prior to use.
the radiation from the external light source is measured and
2. Referenced Documents compared to the absorbance of samples to which known
2
amounts of the sought element were added.
2.1 ASTM Standards:
E50 Practices forApparatus, Reagents, and Safety Consid-
NOTE 1—In general, the deuterium correction system should be able to
erations for Chemical Analysis of Metals, Ores, and correct for the broad-band background absorbance up to 0.5 to 0.6
absorbance units. Zeeman systems should compensate for background
Related Materials
levels as high as 1.0 to 1.5 absorbance units.
E 1184 Practice for Electrothermal (Graphite Furnace)
Atomic Absorption Analysis
4. Significance and Use
E1452 Practice for Preparation of Calibration Solutions for
4.1 This test method is to be used for the determination of
Spectrophotometric and for Spectroscopic Atomic Analy-
trace levels of antimony in carbon and low-alloy steel. It is
ses
assumed that the procedure will be performed by trained
E1601 Practice for Conducting an Interlaboratory Study to
analysts capable of performing common laboratory practices
Evaluate the Performance of an Analytical Method
skillfully and safely. It is expected that the work will be
E1770 Practice for Optimization of ElectrothermalAtomic
performed in a properly equipped laboratory and proper waste
Absorption Spectrometric Equipment
disposal procedures will be followed.
2.2 ISO Standards:
5. Apparatus
5.1 Atomic Absorption Spectrometer with Electrothermal
1
This test method is under the jurisdiction of ASTM Committee E01 on
Atomizer, equipped with background corrector and appropriate
Analytical Chemistry for Metals, Ores, and Related Materials and is the direct
signal output device, such as video display screen, digital
responsibility of Subcommittee E01.01 on Iron, Steel, and Ferroalloys.
Current edition approved Dec. 10, 1996. Published February 1997. computer, printer or strip chart recorder, and autosampler. It is
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on Available from American National Standards Institute, 11 West 42nd Street,
the ASTM website. 13th Floor, New York, NY 10036.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
E1852–96 (2001)
recommended that the instrument meet the following perfor- 7.3 The laboratory sample is normally in the form of
mance requirements after adjusting the instrument and opti- turnings, millings, or drillings. No further mechanical prepa-
mizing the furnace heating program as described in Practice ration of the sample is necessary.
E1770. 7.4 The laboratory sample shall be cleaned by first washing
in acetone and air drying.
5.1.1 The characteristic mass determined in accordance
7.5 If brazed alloy tools are used in the preparation of the
with Practice E1770
...

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ASTM E135-23a(Terminology)
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3.1 Definitions given in Section 4 are intended for use in all standards on analytical chemistry for metals, ores, and related materials. The definitions should be used uniformly and consistently. The purpose of these definitions is to promote clear understanding and interpretation of the standards in which the terms are used.
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4.1 This practice covers all aspects of sampling and preparing steel and iron for chemical analysis as defined in Test Methods, Practices, and Definitions A751 and Specification A48/A48M. Such subjects as sampling location and the sampling of lots are defined.  
4.2 This practice includes most requirements for sampling steel and iron for analysis. Standard test methods that reference this practice need contain only special modifications and exceptions.  
4.3 All who use these procedures should be trained samplers capable of performing common sampling operations skillfully and safely. Only proper sampling equipment should be used.
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1.1 This practice covers the sampling of all grades of steel, both cast and wrought, and all types (grades) of cast irons and blast furnace iron for chemical and spectrochemical determination of composition. This practice is similar to ISO 14284.  
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Sections  
Requirements for Sampling and Sample Preparation  
6  
General  
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Sample  
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General  
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Spoon Sampling  
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Probe Sampling  
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Preparation of a Sample for Analysis  
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Liquid Iron for Cast Iron Production  
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General  
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Spoon Sampling  
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8.4  
Sampling and Sample Preparation for the Determination of  
8.5  
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General  
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Probe Sampling  
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Sampling and Sample Preparation for the Determination  
9.6  
of Hydrogen  
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General  
10.1  
Increment Sampling  
10.2  
Preparation of a Sample for Analysis  
10.3  
Cast Iron Products  
11  
General  
11.1  
Sampling and Sample Preparation  
11.2  
Sections  
Steel Products  
12  
General  
12.1  
Selection of a Laboratory Sample or a Sample for  
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Analysis from a Cast Product  
Selection of a Laboratory Sample or a Sample for  
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Analysis from a Wrought Product  
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Sampling of Leaded Steel  
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Annexes  
Sampling Probes for Use with Liquid Iron and Steel  
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Standard Test Method for Analysis of Cast Iron by Spark Atomic Emission Spectrometry

SIGNIFICANCE AND USE
5.1 The chemical composition of cast iron alloys shall be determined accurately in order to ensure the desired metallurgical properties. This procedure is suitable for manufacturing control and inspection testing.
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1.1 This test method covers the analysis of cast iron by spark atomic emission spectrometry for the following elements in the ranges shown (Note 1):
Ranges, %  
Elements  
Applicable Range, %  
Quantitative Range, %A  
Carbon  
1.9 to 3.8  
1.90 to 3.8  
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0.02 to 2.0  
Phosphorus  
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0.15 to 2.5  
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5.1 X-ray fluorescence spectrometry can provide an accurate determination of metallic and many non-metallic elements in a wide variety of solid and liquid materials. This guide covers the information that should be included in an X-ray spectrometric analytical method and provides direction to the user for determining the optimum conditions needed to achieve acceptable accuracy.  
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5.1 This test method for the chemical analysis of titanium and titanium alloys is primarily intended to test material for compliance with specifications of chemical composition such as those under the jurisdiction of ASTM Committee B10. It may also be used to test compliance with other specifications that are compatible with the test method.  
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1.6 This international standard was developed in accordance with internationally recognized principle...

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SIGNIFICANCE AND USE
5.1 This test method is intended as a referee method for compliance with compositional specifications for impurity content. It is assumed that all who use this procedure will be trained analysts capable of performing common laboratory practices skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Follow appropriate quality control practices such as those described in Guide E882.
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1.1 This test method covers the determination of calcium and magnesium in iron ores, concentrates, and agglomerates in the mass fraction (%) range from 0.05 % to 5 % of calcium and 0.05 % to 3 % of magnesium.  
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1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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5.1 This test method is intended as a referee method for compliance with compositional specifications for impurity content. It is assumed that all who use this procedure will be trained analysts capable of performing common laboratory practices skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Follow appropriate quality control practices such as those described in Guide E882.
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4.1 This practice is intended for users who are attempting to establish GF-AAS procedures. It should be helpful for establishing a complete atomic absorption analysis program.
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1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
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1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Test Method for Determination of Gold in Copper Concentrates by Fire Assay Gravimetry

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5.1 In the metallurgical process used in the mining industries, gold is often carried along with copper during the flotation concentration process. Metallurgical accounting, process control, and concentrate evaluation procedures for this type of material depend on an accurate, precise measurement of the gold in the copper concentrate. This test method is intended to be a reference method for metallurgical laboratories and a referee method to settle disputes in commercial transactions. It is also a definitive method intended to test materials for compliance with compositional specifications and to provide data for certification of reference materials. It is essential that each performance of the method be validated by applying it to appropriate reference materials at the same time and in the same manner as it is applied to the unknowns.  
5.2 It is assumed that all who use this test method will be trained analysts capable of performing skillfully and safely. It is expected that the work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.
SCOPE
1.1 This test method is for the determination of gold in copper concentrates in the content range from 0.2 μg/g to 17 μg/g.
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