ASTM D1754/D1754M-09
(Test Method)Standard Test Method for Effect of Heat and Air on Asphaltic Materials (Thin-Film Oven Test)
Standard Test Method for Effect of Heat and Air on Asphaltic Materials (Thin-Film Oven Test)
SIGNIFICANCE AND USE
This method indicates approximate change in properties of asphalt during conventional hot-mixing at about 150°C [302°F] as indicated by viscosity, penetration, or ductility measurements. It yields a residue which approximates the asphalt condition as incorporated in the pavement. If the mixing temperature differs appreciably from the 150°C [302°F] level, more or less effect on properties will occur.
Note 1—The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D 3666 are generally considered capable of competent and objective testing and sampling.
SCOPE
1.1 This test method covers the determination of the effects of heat and air on a film of semisolid asphaltic materials. The effects of this treatment are determined from measurements of selected asphalt properties before and after the test.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/index.htm—for additional information. Users should be aware that selling mercury and/or mercury containing products into your state may be prohibited by state law.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D1754/D1754M − 09
StandardTest Method for
Effects of Heat and Air on Asphaltic Materials (Thin-Film
1
Oven Test)
This standard is issued under the fixed designation D1754/D1754M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D2170 Test Method for Kinematic Viscosity of Asphalts
(Bitumens)
1.1 This test method covers the determination of the effects
D2171 Test Method for Viscosity of Asphalts by Vacuum
of heat and air on a film of semisolid asphaltic materials. The
Capillary Viscometer
effects of this treatment are determined from measurements of
D3666 Specification for Minimum Requirements for Agen-
selected asphalt properties before and after the test.
cies Testing and Inspecting Road and Paving Materials
1.2 The values stated in either SI units or inch-pound units
D4753 Guide for Evaluating, Selecting, and Specifying Bal-
are to be regarded separately as standard. The values stated in
ances and Standard Masses for Use in Soil, Rock, and
each system may not be exact equivalents; therefore, each
Construction Materials Testing
system shall be used independently of the other. Combining
E1 Specification for ASTM Liquid-in-Glass Thermometers
values from the two systems may result in non-conformance
E145 Specification for Gravity-Convection and Forced-
with the standard.
Ventilation Ovens
1.3 Warning—Mercury has been designated by the United E1137/E1137M Specification for Industrial Platinum Resis-
tance Thermometers
States Environmental ProtectionAgency and many state agen-
cies as a hazardous material that can cause central nervous
3. Summary of Test Method
system,kidneyandliverdamage.Mercury,oritsvapor,maybe
hazardous to health and corrosive to materials. Caution should
3.1 Afilm of asphaltic material is heated in an oven for 5 h
be taken when handling mercury and mercury containing
at 163°C [325°F]. The effects of heat and air are determined
products. See the applicable Material Safety Data Sheet
from changes incurred in physical properties measured before
(MSDS) for details and EPA’s website—http://www.epa.gov/
andaftertheoventreatment.Anoptionalprocedureisprovided
mercury/index.htm—for additional information. Users should
for determining the change in sample mass.
be aware that selling mercury and/or mercury containing
3.2 Precisionvaluesforthemethodhavebeendevelopedfor
products into your state may be prohibited by state law.
viscosity, viscosity change, penetration change, mass change,
1.4 This standard does not purport to address all of the
and ductility.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
4. Significance and Use
priate safety and health practices and determine the applica-
4.1 This method indicates approximate change in properties
bility of regulatory limitations prior to use.
of asphalt during conventional hot-mixing at about 150°C
[302°F] as indicated by viscosity, penetration, or ductility
2. Referenced Documents
measurements. It yields a residue which approximates the
2
2.1 ASTM Standards:
asphalt condition as incorporated in the pavement. If the
D5 Test Method for Penetration of Bituminous Materials
mixing temperature differs appreciably from the 150°C
D113 Test Method for Ductility of Bituminous Materials
[302°F] level, more or less effect on properties will occur.
NOTE 1—The quality of the results produced by this standard are
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
dependent on the competence of the personnel performing the procedure
and Paving Materials and is the direct responsibility of Subcommittee D04.46 on
and the capability, calibration, and maintenance of the equipment used.
Durability and Distillation Tests.
Agencies that meet the criteria of Specification D3666 are generally
Current edition approved July 1, 2009. Published July 2009. Originally approved
considered capable of competent and objective testing and sampling.
in 1960. Last previous edition approved in 2002 as D1754 – 97 (2002). DOI:
10.1520/D1754_D1754M-09.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 5. Apparatus
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
5.1 Oven—The oven shall be electrically heated and shall
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. conform to the performance requirements of Specification
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D1754–97 (Reapproved 2002) Designation:D1754/D1754M–09
Standard Test Method for
Effects of Heat and Air on Asphaltic Materials (Thin-Film
1
Oven Test)
This standard is issued under the fixed designation D 1754/D 1754M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the determination of the effects of heat and air on a film of semisolid asphaltic materials.The effects
of this treatment are determined from measurements of selected asphalt properties before and after the test.
1.2The values stated in SI units are to be regarded as the standard.
1.3
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each
system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the
two systems may result in non-conformance with the standard.
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies
as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous
to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the
applicable Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/index.htm—for
additional information. Users should be aware that selling mercury and/or mercury containing products into your state may be
prohibited by state law.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D5 Test Method for Penetration of Bituminous Materials
D5Test Method for Penetration of Bituminous Materials
2
D113 Test Method for Ductility of Bituminous Materials
2
D2170Test Method for Kinematic Viscosity of Asphalts (Bitumens)
2
D2171Test Method for Viscosity of Asphalts by Vacuum Capillary Viscometer Test Method for Ductility of Bituminous
Materials
D 2170 Test Method for Kinematic Viscosity of Asphalts (Bitumens)
D 2171 Test Method for Viscosity of Asphalts by Vacuum Capillary Viscometer
D 3666 Specification for Minimum Requirements for Agencies Testing and Inspecting Road and Paving Materials
D 4753 Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction
Materials Testing
E1 Specification for ASTM Liquid-in-Glass Thermometers
E 145 Specification for Gravity-Convection and Forced-Ventilation Ovens Specification for Gravity-Convection and Forced-
Ventilation Ovens
E 1137/E 1137M Specification for Industrial Platinum Resistance Thermometers
3. Summary of Test Method
3.1 Afilm of asphaltic material is heated in an oven for5hat 163°C (325°F).[325°F].The effects of heat and air are determined
1
This test method is under the jurisdiction ofASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.46 on Durability
and Distillation Test.
Current edition approved Aug. 10, 1997. Published February 1998. Originally published as D1754–60 T. Last previous edition D1754–94.on Durability and Distillation
Tests.
Current edition approved July 1, 2009. Published July 2009. Originally approved in 1960. Last previous edition approved in 2002 as D 1754 – 97 (2002).
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
, Vol 04.03.volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
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D1754/D1754M–09
from changes incurred in physical properties measured before and after the oven treatment.An optional procedure is provided for
determining the change in sample mass.
3.2 Precision values for the method have been developed for viscosity, viscosity change, penetration change, mass change, and
...
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