EN 16801:2016

Foodstuffs - Determination of elements and their chemical species - Determination of methylmercury in foodstuffs of marine origin by isotope dilution GC-ICP-MS

This final draft European Standard describes a method for the determination of monomethylmercury (MMHg) in foodstuffs of marine origin. The method has been validated in an interlaboratory test on mussel tissue, squid muscle, crab claw muscle, dog fish liver, whale meat, cod muscle and Greenland halibut muscle (all freeze-dried) at levels from 0,04 mg/kg to 3,6 mg/kg dry weight according to ISO 5725 2 [1].
Laboratory experiences have shown that this method is also applicable on fresh samples [2].

Lebensmittel - Bestimmung von Elementen und ihren Verbindungen - Bestimmung von Methylquecksilber in Lebensmitteln marinen Ursprungs mit Isotopenverdünnung GC-ICP-MS

Diese Europäische Norm beschreibt ein Verfahren zur Bestimmung von Monomethylquecksilber (MMHg) in Lebensmitteln marinen Ursprungs. Das Verfahren wurde in einem Ringversuch an Muschelgewebe, Tintenfischgewebe, Scherenmuskulatur von Krabben, Dornhaileber, Walfleisch, Kabeljaumuskulatur und Muskulatur des Schwarzen Heilbutts (alle gefriergetrocknet) mit Massenanteilen von 0,04 mg/kg bis 3,6 mg/kg Trockenmasse nach ISO 5725-2 [1] validiert.
Laborversuche haben gezeigt, dass das Verfahren auch für frische Proben [2] anwendbar ist.

Produits alimentaires - Détermination des éléments et de leurs espèces chimiques - Détermination de la teneur en méthylmercure dans les produits alimentaires d'origine marine par dilution isotopique CG-ICP-SM

Le présent projet de Norme européenne spécifie une méthode de détermination de la teneur en monométhylmercure (MMHg) dans les produits alimentaires d’origine marine. La méthode a été validée dans le cadre d’un essai interlaboratoires réalisé sur du tissu de moule, du muscle de calamar, du muscle de pince de crabe, du foie d’anguille, de la chair de baleine, du muscle de morue et du muscle de flétan noir à des teneurs comprises entre 0,04 mg/kg et 3,6 mg/kg de matière sèche.

Živila - Določevanje elementov in njihovih kemijskih oblik - Določevanje metil živega srebra v živilih morskega izvora z izotopnim razredčenjem GC-ICP-MS

Ta osnutek evropskega standarda opisuje metodo za določevanje monometilnega živega srebra (MMHg) v živilih morskega izvora. Metoda je bila potrjena z medlaboratorijskim preskusom tkiva školjk, mišičnine lignjev, mišičnine v kleščah rakovic, jeter morskih psov, kitovega mesa, mišičnine polenovk in mišičnine grenlandskih morskih plošč v območju od 0,04 mg/kg do 3,6 mg/kg suhe mase (dw).

General Information

• Status: Published
• Publication Date: 29-Mar-2016
• Withdrawal Date: 29-Sep-2016
• ICS: 67.120.30 - Fish and fishery products
• Technical Committee: CEN/TC 275 - Food analysis - Horizontal methods
• Drafting Committee: CEN/TC 275/WG 10 - Trace elements (heavy metals)
• Current Stage: 9093 - Decision to confirm - Review Enquiry
• Completion Date: 03-Sep-2021
• Directive: 882/2004 - Regulation (EC) No 882/2004 of the European Parliament and of the Council of 29 April 2004 onofficial controls performed to ensure the verification of compliance with feed and food law, animal health and animal welfare rules
• Mandate: M/422 - Mandate for standardisation addressed to CEN in the field of methods of analysis for heavy metals and iodine in food
• Ref Project: SIST EN 16801:2016 - Foodstuffs - Determination of elements and their chemical species - Determination of methylmercury in foodstuffs of marine origin by isotope dilution GC-ICP-MS

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN 16801:2016
01-junij-2016
äLYLOD'RORþHYDQMHHOHPHQWRYLQQMLKRYLKNHPLMVNLKREOLN'RORþHYDQMHPHWLO
åLYHJDVUHEUDYåLYLOLKPRUVNHJDL]YRUD]L]RWRSQLPUD]UHGþHQMHP*&,&306
Foodstuffs - Determination of elements and their chemical species - Determination of
methylmercury in foodstuffs of marine origin by isotope dilution GC-ICP-MS
Lebensmittel - Bestimmung von Elementen und ihren Verbindungen - Bestimmung von
Methylquecksilber in Lebensmitteln marinen Ursprungs mit Isotopenverdünnung GC-ICP
-MS
Produits alimentaires - Détermination des éléments et de leurs espèces chimiques -
Détermination de la teneur en méthylmercure dans les produits alimentaires d'origine
marine par dilution isotopique CG-ICP-SM
Ta slovenski standard je istoveten z: EN 16801:2016
ICS:
67.120.30 Ribe in ribji proizvodi Fish and fishery products
SIST EN 16801:2016 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN 16801:2016

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SIST EN 16801:2016


EN 16801
EUROPEAN STANDARD

NORME EUROPÉENNE

March 2016
EUROPÄISCHE NORM
ICS 67.120.30
English Version

Foodstuffs - Determination of elements and their chemical
species - Determination of methylmercury in foodstuffs of
marine origin by isotope dilution GC-ICP-MS
Produits alimentaires - Détermination des éléments et Lebensmittel - Bestimmung von Elementen und ihren
de leurs espèces chimiques - Détermination de la Verbindungen - Bestimmung von Methylquecksilber in
teneur en méthylmercure dans les produits Lebensmitteln marinen Ursprungs mit
alimentaires d'origine marine par dilution isotopique Isotopenverdünnung GC-ICP-MS
CG-ICP-SM
This European Standard was approved by CEN on 8 February 2016.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

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© 2016 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 16801:2016 E
worldwide for CEN national Members.

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SIST EN 16801:2016
EN 16801:2016 (E)
Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Principle . 4
4 Reagents . 4
5 Apparatus and equipment . 6
6 Procedure. 7
7 Calculation . 10
8 Precision . 11
9 Test report .
...