iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
CEN

CR 13505:1999

(Main)

Food analysis - Biotoxins - Criteria of analytical methods of mycotoxins

Food analysis - Biotoxins - Criteria of analytical methods of mycotoxins

This CEN Report gives criteria for the selection of methods of analysis for mycotoxins. Criteria covered are the repeatability, reproducibility, recovery, extraction solvents, applicability and food types. Performance criteria are included for aflatoxin B1, total of aflatoxins B1, B2, G1 and G2, aflatoxin M1, ochratoxin A, patulin, fumonisin B1, fumonisin B2, deoxynivalenol, nivalenol, HT-2 toxin, T-2 toxin and zearalenone.

Lebensmittel - Biotoxine - Kriterien für Mycotoxin-Analyseverfahren

Produits alimentaires - Biotoxines - Critères des méthodes d'analyse des mycotoxines

Analize živil - Biotoksini - Kriteriji analiznih metod mikotoksinov

General Information

Status
Withdrawn
Publication Date
23-Feb-1999
Withdrawal Date
19-Nov-2019
ICS
67.050 - General methods of tests and analysis for food products
Technical Committee
CEN/TC 275 - Food analysis - Horizontal methods
Drafting Committee
CEN/TC 275/WG 5 - Biotoxins
Current Stage
9960 - Withdrawal effective - Withdrawal
Completion Date
20-Nov-2019
Ref Project
SIST CR 13505:2000 - Food analysis - Biotoxins - Criteria of analytical methods of mycotoxins

Relations

Revised
CEN/TR 16059:2010 - Food analysis - Performance criteria for single laboratory validated methods of analysis for the determination of mycotoxins
Effective Date
22-Dec-2008

Buy Standard

CR 13505:2000CR 13505:2000
PreviousNext
Standardization document
CR 13505:2000
English language
8 pages
sale 10% off
Preview
sale 10% off
Preview
e-Library read for
1 day

Standards Content (Sample)

SLOVENSKI STANDARD
SIST CR 13505:2000
01-maj-2000
Analize živil - Biotoksini - Kriteriji analiznih metod mikotoksinov
Food analysis - Biotoxins - Criteria of analytical methods of mycotoxins
Lebensmittel - Biotoxine - Kriterien für Mycotoxin-Analyseverfahren
Produits alimentaires - Biotoxines - Criteres des méthodes d'analyse des mycotoxines
Ta slovenski standard je istoveten z: CR 13505:1999
ICS:
67.050 Splošne preskusne in General methods of tests and
analizne metode za živilske analysis for food products
proizvode
SIST CR 13505:2000 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

CEN
EN 17851:2023(Main)
Foodstuffs - Determination of elements and their chemical species -Determination of Ag, As, Cd, Co, Cr, Cu, Mn, Mo, Ni, Pb, Se, Tl, U and Zn in foodstuffs by inductively coupled plasma mass spectrometry (ICP-MS) after pressure digestion
SIST EN 17851:2023

This document specifies a method for the determination of Ag, As, Cd, Co, Cr, Cu, Mn, Mo, Ni, Pb, Se, Tl, U and Zn in foodstuffs by ICP-MS after pressure digestion.
The following foodstuffs were analysed for the elements listed in Table 1 in an interlaboratory study: Banana (deep-frozen), Cocoa powder, Wheat noodle powder, Currant nectar (deep-frozen), Milk powder, Oyster (dried), Celery (dried), Dogfish liver (dried), Liver (deep-frozen), Kale (dried).
Table 1 - Rangea
....

  • Standard
    39 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO 22753:2022(Main)
Molecular biomarker analysis - Method for the statistical evaluation of analytical results obtained in testing sub-sampled groups of genetically modified seeds and grains - General requirements (ISO 22753:2021, Corrected version 2022-11)
SIST EN ISO 22753:2023

This document describes general requirements, procedures and performance criteria for evaluating the content of genetically modified (GM) seeds/grains in a lot by a group testing strategy that includes qualitative analysis of sub-sampled groups followed by statistical evaluation of the results.
This document is applicable to group testing strategy estimating the GM content on a percentage seed/grain basis for purity estimation, testing towards a given reject/accept criterion and for cases where seed/grain lots are carrying stacked events.
This document is not applicable to processed products.
NOTE       Description of the use of group testing strategy are available in References [1], [7], [8], [18], [19] and [20].

  • Standard
    34 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 17641:2022(Main)
Foodstuffs - Multimethod for the determination of aflatoxins, deoxynivalenol, fumonisins, ochratoxin A, T-2 toxin, HT-2 toxin and zearalenone by LC-MS/MS
SIST EN 17641:2022

This document describes a method using isotopically labelled standards for the quantitative determination of aflatoxins B1, B2, G1, G2 and M1 (AFB1, AFB2, AFG1, AFG2 and AFM1), ochratoxin A (OTA), deoxynivalenol (DON), zearalenone (ZEN), T-2 and HT-2 toxins (T-2 and HT-2) and fumonisins B1 and B2 (FB1 and FB2) in foods by liquid chromatography (LC) coupled with tandem mass spectrometry (MS/MS).
A specific immunoaffinity column (IAC) clean-up is needed for aflatoxins (AFs) and OTA in food intended for infants and young children (e.g. infant cereals, milk-based powders), in spices, in dried fruits and in nuts.
The method has been validated through an intercollaborative study on different commodity groups: cereals and cereal-based products including food for infant and young children, nuts, spices, dried fruits and milk powder. The measuring range of each mycotoxin in these naturally contaminated and/or spiked food samples were:
- AFB1: 0,085 7 µg/kg - 11,4 µg/kg;
- AFB2: 0,079 2 µg/kg - 12,5 µg/kg;
- AFG1: 0,062 8 µg/kg - 20,9 µg/kg;
- AFG2: 0,052 0 µg/kg - 15,0 µg/kg;
- AFM1: 0,034 2 µg/kg - 0,110 µg/kg;
- OTA: 0,448 µg/kg - 17,2 µg/kg;
- DON: 45,2 µg/kg - 743 µg/kg;
- ZEN: 9,57 µg/kg - 131 µg/kg;
- T-2: 10,3 µg/kg - 57,9 µg/kg;
- HT-2: 9,50 µg/kg - 81,8 µg/kg;
- FB1: 31,1 µg/kg - 4 260 µg/kg;
- FB2: 44,2 µg/kg - 1 300 µg/kg.
The measuring ranges of the method for each mycotoxin/matrix combination are given in Table 8.

  • Standard
    49 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 17644:2022(Main)
Foodstuffs - Detection of food allergens by liquid chromatography - mass spectrometry (LC-MS) methods - General considerations
SIST EN 17644:2022

This document establishes an overall framework covering qualitative and quantitative methods for the determination of food allergens and allergenic ingredients using mass spectrometry-based methods for the determination of specific peptides/proteins. This document provides general guidelines and performance criteria applicable to this methodology. Guidelines, minimum requirements and performance criteria laid down in this document are intended to ensure that comparable and reproducible results are obtained by different analysts, instrumentation and laboratories.

  • Standard
    20 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 1787:2022(Main)
Foodstuff - Detection of irradiated foodstuff containing cellulose by ESR spectroscopy
SIST EN 1787:2022

This document specifies a method for the detection of foodstuff containing cellulose which have been treated with ionizing radiation, by analysing the electron spin resonance (ESR) spectrum, also called electron paramagnetic resonance (EPR) spectrum, of the foodstuff, see [1] to [13].
Interlaboratory studies have been successfully carried out with pistachio nut shells, [14] to [18], paprika powder [19] and [20] and fresh strawberries [21]. However, it has been shown that chemical bleaching of nuts in shells can lead to comparable signals. For further information, see Clause 8 on limitations.

  • Standard
    16 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 13708:2022(Main)
Foodstuffs - Detection of irradiated foodstuff containing crystalline sugar by ESR spectroscopy
SIST EN 13708:2022

This document specifies a method for the detection of foodstuff containing crystalline sugars which have been treated with ionizing radiation, by analysing the electron spin resonance (ESR) spectrum, also called electron paramagnetic resonance (EPR) spectrum, of the foodstuff, see [1] to [7].
Interlaboratory studies have been successfully carried out on dried figs, dried mangoes, dried papayas and raisins, see [1] to [3].

  • Standard
    12 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
CEN/TS 17743:2022(Main)
Foodstuff - Determination of pesticide residues by ethyl acetate extraction using GC- and LC-MS/MS (SweEt)
SIST-TS CEN/TS 17743:2022

This document specifies a method for the analysis of pesticide residues in foods of plant and of animal origin by ethyl acetate extraction using GC- and LC-MS/MS (SweEt).

  • Technical specification
    17 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 17521:2021(Main)
Foodstuffs - Determination of Alternaria toxins in tomato, wheat and sunflower seeds by SPE clean-up and HPLC-MS/MS
SIST EN 17521:2021

This European Standard specifies a method for the determination of five Alternaria toxins in wheat, tomato juice and sunflower seed samples by liquid chromatography tandem mass spectrometry (LC-MS/MS). The method includes the analysis of Altenuene (ALT), Alternariol (AOH), Alternariol monomethyl ether (AME) in the range of 1 μg/kg to 100 μg/kg, and Tentoxin (TEN) in the range of 5 μg/kg to 500 μg/kg, and Tenuazonic acid (TEA) in the range of 10 μg/kg to 1000 μg/kg.

  • Standard
    37 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
CEN/TS 17329-1:2021(Main)
Foodstuffs - General guidelines for the validation of qualitative real-time PCR methods - Part 1: Single-laboratory validation
SIST-TS CEN/TS 17329-1:2021

This document describes the performance characteristics and minimum performance criteria for conducting a single-laboratory validation study for qualitative (binary) real-time polymerase chain reaction (PCR) methods applied for the detection of specific DNA sequences present in foods.
The protocol was developed for qualitative real-time PCR methods for the detection of DNA sequences derived from genetically modified foodstuffs. It is applicable also for single-laboratory validation of qualitative PCR methods used for analysis of other food materials, e.g. for species detection and identification.
The document does not cover the evaluation of the applicability and the practicability with respect to the specific scope of the PCR method.

  • Technical specification
    23 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 17203:2021(Main)
Foodstuffs - Determination of citrinin in food by HPLC-MS/MS
SIST EN 17203:2021

This document describes a procedure for the determination of the citrinin content in food (cereals, red yeast rice (RYR)), herbs and food supplements by liquid chromatography tandem mass spectrometry (LC-MS/MS).
This method has been validated for citrinin in red yeast rice and in the formulated food supplements in the range of 2,5 μg/kg to 3 000 μg/kg and in wheat flour in the range of 2,5 μg/kg to 100 μg/kg.
Laboratory experiences have shown that this method is also applicable to white rice, herbs such as a powder of ginkgo biloba leaves and the formulated food supplements in the range of 2,5 μg/kg to 50 μg/kg.

  • Standard
    23 pages
    English language
    sale 10% off
    e-Library read for
    1 day