EN ISO 1183-3:1999

Plastics - Methods for determining the density of non-cellular plastics - Part 3: Gas pyknometer method (ISO 1183-3:1999)

This part of ISO 1183 specifies a method for the determination of the density or the specific volume of solid noncellular
plastics of any shape which do not contain closed pores.

Kunststoffe - Bestimmung der Dichte von nicht verschäumten Kunststoffen - Teil 3: Gas Pyknometer Verfahren (ISO 1183-3:1999)

Dieser Teil der ISO 1183 legt ein Prüfverfahren fest zur Bestimmung der Dichte oder des spezifischen Volumens fester, nicht verschäumter Kunststoffe, die einebeliebige Form aufweisen können und keine geschlossenen Poren enthalten.

Plastiques - Méthodes pour déterminer la masse volumique des plastiques non alvéolaires - Partie 3: Méthode du pycnomètre à gaz (ISO 1183-3:1999)

La présente partie de l'ISO 1183 spécifie une méthode d'essai pour déterminer la masse volumique ou le volume
spécifique des plastiques non alvéolaires solides de forme quelconque, mais exempts de cavités fermées.

Polimerni materiali - Metode za določanje gostote nepenjenih polimernih materialov - 3. del: Metoda s plinskim piknometrom (ISO 1183-3:1999)

General Information

• Status: Published
• Publication Date: 14-Sep-1999
• Withdrawal Date: 30-Mar-2000
• ICS: 83.080.10 - Thermosetting materials
• Technical Committee: CEN/TC 249 - Plastics
• Drafting Committee: CEN/TC 249 - Plastics
• Current Stage: 6060 - Definitive text made available (DAV) - Publishing
• Start Date: 15-Sep-1999
• Completion Date: 15-Sep-1999
• Ref Project: SIST EN ISO 1183-3:2000 - Plastics - Methods for determining the density of non-cellular plastics - Part 3: Gas pyknometer method (ISO 1183-3:1999)

Relations

• Parent: EN ISO 1183-1:2004 - Plastics - Methods for determining the density of non-cellular plastics - Part 1: Immersion method, liquid pyknometer method and titration method (ISO 1183-1:2004)
• Effective Date: 22-Dec-2008

Standards Content (Sample)

SLOVENSKI STANDARD
01-maj-2000
3ROLPHUQLPDWHULDOL0HWRGH]DGRORþDQMHJRVWRWHQHSHQMHQLKSROLPHUQLK
PDWHULDORYGHO0HWRGDVSOLQVNLPSLNQRPHWURP,62
Plastics - Methods for determining the density of non-cellular plastics - Part 3: Gas
pyknometer method (ISO 1183-3:1999)
Kunststoffe - Bestimmung der Dichte von nicht verschäumten Kunststoffen - Teil 3: Gas
Pyknometer Verfahren (ISO 1183-3:1999)
Plastiques - Méthodes pour déterminer la masse volumique des plastiques non
alvéolaires - Partie 3: Méthode du pycnometre a gaz (ISO 1183-3:1999)
Ta slovenski standard je istoveten z: EN ISO 1183-3:1999
ICS:
83.080.01 Polimerni materiali na Plastics in general
splošno
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

INTERNATIONAL ISO
STANDARD 1183-3
First edition
1999-09-15
Plastics — Methods for determining the
density of non-cellular plastics —
Part 3:
Gas pyknometer method
Plastiques — Méthodes pour déterminer la masse volumique des
plastiques non alvéolaires —
Partie 3: Méthode utilisant un pycnomètre à gaz
A
Reference number
ISO 1183-3:1999(E)
ISO 1183-3:1999(E)
Contents
1 Scope .1
2 Terms, definitions, symbols, units and abbreviated terms .1
3 Principle.2
4 Apparatus and materials.3
5 Test specimens.3
6 Calibration .3
7 Procedure and calculation.4
8 Precision.4
9 Test report .4
Annex A (informative) Two-chamber pressure-measuring pyknometer.6
©  ISO 1999
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic
or mechanical, including photocopying and microfilm, without permission in writing from the publisher.
International Organization for Standardization
Case postale 56 • CH-1211 Genève 20 • Switzerland
Internet [e-mail]
Printed in Switzerland
ii
© ISO
ISO 1183-3:1999(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO
member bodies). The work of preparing International Standards is normally carried out through ISO technical
committees. Each member body interested in a subject for which a technical committee has been established has
the right to be represented on that committee. International organizations, governmental and non-governmental, in
liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical
Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 3.
Draft International Standards adopted by the technical committees are circulated to the member bodies for voting.
Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote.
International Standard ISO 1183-3 was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 5,
Physical-chemical properties. Together with the other parts (see below), it cancels and replaces ISO 1183:1987,
which has been technically revised.
ISO 1183 consists of the following parts under the general title, Plastics — Methods for determining the density of
non-cellular plastics:
 Part 1: Immersion method, pyknometer method and titration method
 Part 2: Density gradient column method
 Part 3: Gas pyknometer method
Annex A of this part of ISO 1183 is for information only.
iii
© ISO
ISO 1183-3:1999(E)
Introduction
This part of ISO 1183 is one of a series dealing with methods of measuring the density of solid non-cellular plastics.
The values obtained using this part of ISO 1183 are expected to be comparable to those obtained using the other
parts.
Density measurements may be used to investigate variations in the physical structure or the molecular order of
materials. Such measurements are widely used to determine the degree of crystallinity of polymers. In addition, they
may be used to determine the amount of filler present.
The density of a plastic material may depend on any conditioning or thermal treatment which the material has
undergone.
The physical structure of a polymer can change with time and temperature. Its volume is also a temperature-
dependent property. This means that the density may vary with time and/or temperature.
iv
INTERNATIONAL STANDARD  © ISO ISO 1183-3:1999(E)
Plastics — Methods for determining the density of non-cellular
plastics —
Part 3:
Gas pyknometer method
WARNING — The use of this part of ISO 1183 may involve hazardous materials, operations or equipment.
This part of ISO 1183 does not purport to address all of the safety problems, if any, associated with its use.
It is the responsibility of the user of this part of ISO 1183 to establish appropriate health and safety
practices and to determine the applicability of any regulatory limitations prior to use.
1 Scope
This part of ISO 1183 specifies a method for the determination of the density or the specific volume of solid non-
cellular plastics of any shape which do not contain closed pores.
2 Terms, definitions, symbols, units and abbreviated terms
For the purposes of this part of ISO 1183, the following terms, definitions, symbols, units and abbreviated terms
apply:
2.1
test material
material to be tested
2.2
test specimen
that part of the test material actually subjected to the test
2.3
mass
m
quantity of matter contained in a body
NOTE Mass is expressed in kilograms (kg) or grams (g).
2.4
weight
W
force produced by gravity acting on a mass
NOTE 1 Since gravity varies with location, so does weight.
NOTE 2 Weight is expressed in newtons (N).
© ISO
ISO 1183-3:1999(E)
2.5
apparent mass
m
app
mass of a body obtained by measuring its weight using an appropriately calibrated balance
NOTE Apparent mass is expressed in kilograms (kg) or grams (g).
2.6
volume
V
size of a body in three-dimensional space, excluding pores
NOTE 1 Due to thermal expansion, volume varies with temperature T.
3 3
NOTE 2 Volume is expressed in cubic metres (m ), litres (l), cubic centimetres (cm ) or millilitres (ml).
2.7
density
r
mass per unit volume of a material at a given temperature T
NOTE 1 Density is calculated using the equation
m
app
T
r =  at constant T (1)
V
3 3
NOTE 2 It is expressed in kilograms per cubic metre (kg/m ), kilograms per cubic decimetre (kg/dm ), grams per cubic
centimetre (g/cm ), kilograms per litre (kg/l) or grams per millilitre (g/ml).
2.8
specific volume
v
volume per unit mass of a material at a given temperature T
NOTE 1 Specific volume is calculated using the equation
T
T 1
V
v==  at constant T (2)
T
m
app
r
3 3
NOTE 2 It is expressed in cubic metres per kilogram (m /kg), cubic decimetres per kilogram (dm /kg), cubic centimetres per
gram (cm /g), litres per kilogram (l/kg) or millilitres per gram (ml/g).
NOTE 3 Density is to be distinguished from specific gravity, which is the ratio of the weight of a given volume of a material to
that of an equal volume of water at a stated temperature T.
3 Principle
3.1  The volume of a specimen of known apparent mass is determined by measuring the change of gas volume
within a pyknometer upon introducing the specimen. The volume change may be obtained either directly by means
of a movable piston or indirectly by measuring the change of the pressure within the pyknometer and calculating the
volume using the pressure-
...