Bitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method

This European Standard specifies a method for the determination of the breaking value of cationic bituminous emulsions.
WARNING  The use of this European Standard may involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 1: Bestimmung des Brechwertes kationischer Bitumenemulsionen, Verfahren mit Feinmineralstoff

Diese Europäische Norm legt ein Verfahren zur Bestimmung des Brechwertes kationischer Bitumen-emulsionen fest.
WARNUNG — Die Anwendung dieser Europäischen Norm kann die Anwendung gefährlicher Stoffe, Arbeitsgänge und Geräte mit sich bringen. Diese Europäische Norm beansprucht nicht, alle damit verbundenen Sicherheitsprobleme zu behandeln. Es liegt in der Verantwortung des Anwenders dieser Europäischen Norm, vor ihrer Anwendung geeignete Maßnahmen für die Sicherheit und den Gesundheitsschutz des Personals zu ergreifen, und dafür Sorge zu tragen, dass behördliche und gesetzliche Maßnahmen eingehalten werden.

Bitumes et liants bitumineux - Détermination du comportement à la rupture - Partie 1 : Détermination de l'indice de rupture des émulsions cationiques de bitume, méthode des fines minérales

La présente Norme européenne décrit une méthode de détermination de l’indice de rupture des émulsions cationiques de bitume.
AVERTISSEMENT — L’utilisation de la présente Norme européenne implique l'intervention de produits, d'opérations et d'équipements à caractère dangereux. La présente Norme européenne n'a pas la prétention d'aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Ugotavljanje stopnje stabilnosti - 1. del: Ugotavljanje hitrosti razpada kationskih bitumenskih emulzij, metoda z mineralnim polnilom

Ta evropski standard določa metodo za ugotavljanje hitrosti razpada kationskih bitumenskih emulzij.
OPOZORILO – pri uporabi tega standarda so lahko prisotni nevarni materiali, postopki in oprema. Ta evropski standard ne obravnava vseh varnostnih težav, ki se nanašajo na njegovo uporabo. Za vzpostavitev ustreznih varnostnih in zdravstvenih praks ter za določitev uporabnosti regulativnih omejitev pred uporabo je odgovoren uporabnik tega evropskega standarda. Zaradi okoljskih razlogov in za zmanjševanje emisij v zrak, vodo in zemljo, je priporočljivo omejiti uporabo izdelkov, topil in energije na minimum, potreben za veljavne rezultate preskusa.

General Information

Status
Published
Publication Date
08-Nov-2016
Withdrawal Date
30-May-2017
Current Stage
9092 - Decision on results of review/2YR ENQ - revise - Review Enquiry
Start Date
07-Dec-2022
Completion Date
14-Apr-2025

Relations

Overview

EN 13075-1:2016 - Bitumen and bituminous binders: Determination of breaking behaviour - Part 1 specifies a laboratory method (mineral filler method) to determine the breaking value of cationic bituminous emulsions. The breaking value (BV) is a dimensionless number that represents the mass of a reference filler (g) required to coagulate 100 g of emulsion. The standard covers both semi‑automatic and manual procedures, defines reference fillers, and gives requirements for apparatus, sample preparation and test conditions.

Keywords: EN 13075-1:2016, breaking value, cationic bituminous emulsions, mineral filler method, bitumen testing, bituminous binders, reference fillers.

Key topics and technical requirements

  • Scope & safety: Method applies to cationic bituminous emulsions; users must follow lab safety and regulatory limits (hazardous materials warning included).
  • Principle: A reference filler is added at a controlled rate to a stirred emulsion until the emulsion “breaks”; the mass of filler used gives the BV.
  • Sample size & conditioning: Typical test uses (100 ± 1) g of emulsion taken from a 250 g bottle conditioned at (25 ± 1) °C for ≥1.5 h.
  • Apparatus requirements:
    • Semi‑automatic: stirrer motor ≥25 W, stirrer speed (260 ± 60) r/min, metal can (≈500 ml), adjustable filler feeder.
    • Manual: dish (~20 cm dia.), spatula and steady mixing (≈1 r/s).
    • Common: oven at (110 ± 5) °C for drying fillers, balance to 0.1 g, timer accuracy 0.2 s.
  • Filler feed rate: Adjustable feeder calibrated to feed at (0.35 ± 0.10) g/s; actual feeding rate must be verified and reported.
  • Reference fillers: Forshammer, Sikaisol and Caolin Q92 are specified; results are converted to a “Forshammer equivalent” using factors given in Clause 9 (factors based on inter‑laboratory Round Robin data).
  • Precision & reporting: The standard includes repeatability and reproducibility guidance and a required test report content list.

Applications and users

  • Practical uses:
    • Characterising breaking (coagulation) behaviour of cationic emulsions for mix design, quality control and product development.
    • Assessing emulsion compatibility with mineral fillers used in road‑making and surface treatments.
  • Who uses it:
    • Pavement material laboratories, bitumen/emulsion manufacturers, road authorities, quality control personnel and researchers working with bituminous binders and cold‑mix processes.

Related standards

  • EN 58 - Sampling bituminous binders
  • EN 12594 - Preparation of test samples
  • EN 13075 Part 2 - Determination of fines mixing time of cationic bituminous emulsions

Use EN 13075-1:2016 when you need a repeatable, standardised laboratory method to quantify emulsion breaking performance and compare formulations or production batches under defined conditions.

Standard
EN 13075-1:2017
English language
16 pages
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Standards Content (Sample)


2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen in bitumenska veziva - Ugotavljanje stopnje stabilnosti - 1. del: Ugotavljanje hitrosti razpada kationskih bitumenskih emulzij, metoda z mineralnim polnilomBitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 1: Bestimmung des Brechwertes kationischer Bitumenemulsionen, Verfahren mit FeinmineralstoffBitumes et liants bitumineux - Détermination du comportement à la rupture - Partie 1 : Détermination de l'indice de rupture des émulsions cationiques de bitume, méthode des fines minéralesBitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 13075-1:2016SIST EN 13075-1:2017en,fr,de01-januar-2017SIST EN 13075-1:2017SLOVENSKI
STANDARDSIST EN 13075-1:20121DGRPHãþD

EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 13075-1
November
t r s x ICS
y wä s v râ
{ sä s r rä w r Supersedes EN
s u r y wæ sã t r r {English Version
Bitumen and bituminous binders æ Determination of breaking behaviour æ Part
sã Determination of breaking value of cationic bituminous emulsionsá mineral filler method Bitumes et liants bitumineux æ Détermination du comportement à la rupture æ Partie
s ã Détermination de l 5indice de rupture des émulsions cationiques de bitumeá méthode des fines minérales
Bitumen und bitumenhaltige Bindemittel æ Bestimmung des Brechverhaltens æ Teil
sã Bestimmung des Brechwertes kationischer Bitumenemulsionená Verfahren mit Feinmineralstoff This European Standard was approved by CEN on
t y August
t r s xä
egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey andUnited Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Avenue Marnix 17,
B-1000 Brussels
t r s x CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
s u r y wæ sã t r s x ESIST EN 13075-1:2017

Characteristics of the reference fillers . 12 A.1 Characteristics of the Forshammer filler . 12 A.2 Characteristics of the Sikaisol filler . 13 A.3 Characteristics of the Caolin Q92 filler . 14 Bibliography . 16
the three reference fillers. EN 13075 consists of the following parts under the general title “Bitumen and bituminous binders – Determination of breaking behaviour”: — Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method — Part 2: Determination of fines mixing time of cationic bituminous emulsions According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. SIST EN 13075-1:2017
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Frequently Asked Questions

EN 13075-1:2016 is a standard published by the European Committee for Standardization (CEN). Its full title is "Bitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method". This standard covers: This European Standard specifies a method for the determination of the breaking value of cationic bituminous emulsions. WARNING The use of this European Standard may involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

This European Standard specifies a method for the determination of the breaking value of cationic bituminous emulsions. WARNING The use of this European Standard may involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

EN 13075-1:2016 is classified under the following ICS (International Classification for Standards) categories: 75.140 - Waxes, bituminous materials and other petroleum products; 91.100.50 - Binders. Sealing materials. The ICS classification helps identify the subject area and facilitates finding related standards.

EN 13075-1:2016 has the following relationships with other standards: It is inter standard links to EN 13075-1:2009, EN 13075-1:2012. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

EN 13075-1:2016 is associated with the following European legislation: EU Directives/Regulations: 89/106/EEC; Standardization Mandates: M/124. When a standard is cited in the Official Journal of the European Union, products manufactured in conformity with it benefit from a presumption of conformity with the essential requirements of the corresponding EU directive or regulation.

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