Bitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method

This European Standard specifies a method for the determination of the breaking value of cationic bituminous emulsions.
WARNING  The use of this European Standard may involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 1: Bestimmung des Brechwertes kationischer Bitumenemulsionen, Verfahren mit Feinmineralstoff

Diese Europäische Norm legt ein Verfahren zur Bestimmung des Brechwertes kationischer Bitumen-emulsionen fest.
WARNUNG — Die Anwendung dieser Europäischen Norm kann die Anwendung gefährlicher Stoffe, Arbeitsgänge und Geräte mit sich bringen. Diese Europäische Norm beansprucht nicht, alle damit verbundenen Sicherheitsprobleme zu behandeln. Es liegt in der Verantwortung des Anwenders dieser Europäischen Norm, vor ihrer Anwendung geeignete Maßnahmen für die Sicherheit und den Gesundheitsschutz des Personals zu ergreifen, und dafür Sorge zu tragen, dass behördliche und gesetzliche Maßnahmen eingehalten werden.

Bitumes et liants bitumineux - Détermination du comportement à la rupture - Partie 1 : Détermination de l'indice de rupture des émulsions cationiques de bitume, méthode des fines minérales

La présente Norme européenne décrit une méthode de détermination de l’indice de rupture des émulsions cationiques de bitume.
AVERTISSEMENT — L’utilisation de la présente Norme européenne implique l'intervention de produits, d'opérations et d'équipements à caractère dangereux. La présente Norme européenne n'a pas la prétention d'aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Ugotavljanje stopnje stabilnosti - 1. del: Ugotavljanje hitrosti razpada kationskih bitumenskih emulzij, metoda z mineralnim polnilom

Ta evropski standard določa metodo za ugotavljanje hitrosti razpada kationskih bitumenskih emulzij.
OPOZORILO – pri uporabi tega standarda so lahko prisotni nevarni materiali, postopki in oprema. Ta evropski standard ne obravnava vseh varnostnih težav, ki se nanašajo na njegovo uporabo. Za vzpostavitev ustreznih varnostnih in zdravstvenih praks ter za določitev uporabnosti regulativnih omejitev pred uporabo je odgovoren uporabnik tega evropskega standarda. Zaradi okoljskih razlogov in za zmanjševanje emisij v zrak, vodo in zemljo, je priporočljivo omejiti uporabo izdelkov, topil in energije na minimum, potreben za veljavne rezultate preskusa.

General Information

Status
Published
Publication Date
08-Nov-2016
Current Stage
9060 - Closure of 2 Year Review Enquiry - Review Enquiry
Due Date
04-Jun-2022
Completion Date
04-Jun-2022

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen in bitumenska veziva - Ugotavljanje stopnje stabilnosti - 1. del: Ugotavljanje hitrosti razpada kationskih bitumenskih emulzij, metoda z mineralnim polnilomBitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 1: Bestimmung des Brechwertes kationischer Bitumenemulsionen, Verfahren mit FeinmineralstoffBitumes et liants bitumineux - Détermination du comportement à la rupture - Partie 1 : Détermination de l'indice de rupture des émulsions cationiques de bitume, méthode des fines minéralesBitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 13075-1:2016SIST EN 13075-1:2017en,fr,de01-januar-2017SIST EN 13075-1:2017SLOVENSKI

STANDARDSIST EN 13075-1:20121DGRPHãþD
SIST EN 13075-1:2017
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 13075-1
November
t r s x ICS
y wä s v râ
{ sä s r rä w r Supersedes EN
s u r y wæ sã t r r {English Version
Bitumen and bituminous binders æ Determination of breaking behaviour æ Part

sã Determination of breaking value of cationic bituminous emulsionsá mineral filler method Bitumes et liants bitumineux æ Détermination du comportement à la rupture æ Partie

s ã Détermination de l 5indice de rupture des émulsions cationiques de bitumeá méthode des fines minérales

Bitumen und bitumenhaltige Bindemittel æ Bestimmung des Brechverhaltens æ Teil

sã Bestimmung des Brechwertes kationischer Bitumenemulsionená Verfahren mit Feinmineralstoff This European Standard was approved by CEN on

t y August
t r s xä

egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä

translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä

CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey andUnited Kingdomä

EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre:
Avenue Marnix 17,
B-1000 Brussels

t r s x CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN

s u r y wæ sã t r s x ESIST EN 13075-1:2017

EN 13075-1:2016 (E) 2 Contents Page European foreword ....................................................................................................................................................... 3 1 Scope .................................................................................................................................................................... 4 2 Normative references .................................................................................................................................... 4 3 Terms and definitions ................................................................................................................................... 4 4 Principle ............................................................................................................................................................. 4 5 Reagents and materials ................................................................................................................................. 4 6 Apparatus ........................................................................................................................................................... 5 6.1 General ................................................................................................................................................................ 5 6.2 Equipment for semi-automatic procedure ............................................................................................ 5 6.3 Equipment for manual procedure............................................................................................................. 5 6.4 Equipment for both procedures ................................................................................................................ 5 7 Sampling ............................................................................................................................................................. 8 8 Procedure........................................................................................................................................................... 8 8.1 General ................................................................................................................................................................ 8 8.2 Semi-automatic procedure .......................................................................................................................... 9 8.3 Manual procedure ........................................................................................................................................... 9 9 Calculation ...................................................................................................................................................... 10 10 Expression of results ................................................................................................................................... 10 11 Precision .......................................................................................................................................................... 10 11.1 Repeatability, r .............................................................................................................................................. 10 11.2 Reproducibility, R ........................................................................................................................................ 11 12 Test report ...................................................................................................................................................... 11 Annex A (normative)

Characteristics of the reference fillers ................................................................... 12 A.1 Characteristics of the Forshammer filler ............................................................................................ 12 A.2 Characteristics of the Sikaisol filler ....................................................................................................... 13 A.3 Characteristics of the Caolin Q92 filler ................................................................................................. 14 Bibliography ................................................................................................................................................................. 16

SIST EN 13075-1:2017

EN 13075-1:2016 (E) 3 European foreword This document (EN 13075-1:2016) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2017, and conflicting national standards shall be withdrawn at the latest by May 2017. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 13075-1:2009. In comparison with EN 13075-1:2009, the following significant changes have been made: — Clause 5 : three reference fillers (Forshammer, Sikaisol and Caolin Q92) may be used; — Subclauses 6.4.3 and 6.4.4: calibration range of the filler feeder and accuracy requirements for the timer are extended so as to cover the case of slow breaking emulsions; — Subclause 6.4.8 is discarded since this clause is not called by the test procedure (Clause 8) and since requirements on temperature control are already stated in 6.4.1 (oven) and 6.4.6 (temperature bath or climatic chamber); — Subclauses 8.2 and 8.3: more accurate and more complete description of the test procedure. Calculation and reporting (Clause 12) of the actual filler feeding rate; — Clause 9: New factors for the conversion of measured breaking values into “Forshammer equivalents”. The conversion factors for Sikaisol and Caolin Q92 have been established from an extensive Round Robin test program conducted by TC336/WG2 in 2014 (see bibliographic reference N°2); — Subclause 11.2: A value for Reproducibility is now stated, as an outcome of the TC336/WG2 Round Robin; — Annex A: more complete (e.g. particle size distribution envelopes) and more homogeneous description of

the three reference fillers. EN 13075 consists of the following parts under the general title “Bitumen and bituminous binders – Determination of breaking behaviour”: — Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method — Part 2: Determination of fines mixing time of cationic bituminous emulsions According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. SIST EN 13075-1:2017

EN 13075-1:2016 (E) 4 1 Scope This European Standard specifies a method for the determination of the breaking value of cationic bituminous emulsions. WARNING — The use of this European Standard may involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders - Sampling bituminous binders EN 12594, Bitumen and bituminous binders - Preparation of test samples 3 Terms and definitions For the purposes of this document, the following term and definition applies. 3.1 breaking value “BV” dimensionless number corresponding to the mass of reference filler, in grams, needed to coagulate 100 g of bitumen emulsion 4 Principle A reference filler is added at a uniform rate to a specified quantity of stirred cationic bitumen emulsion. When the emulsion has broken completely, the mass of added filler is determined by weighing. The mass of filler (in grams) multiplied by 100 and divided by the mass of emulsion (in grams) is the breaking value. NOTE The cationic or anionic nature of an emulsion can be determined with EN 1430 [1]. 5 Reagents and materials 5.1 Reference fillers. The Forshammer filler1), the Sikaisol filler1) or the Caolin Q92 filler1) shall be used as reference fillers while applying the conversion factors given in Clause 9. The characteristics of these fillers are given in Annex A. In the event of dispute, the same filler and the same procedure (manual or semi-automatic) shall be used by the testing laborat

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