iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
CEN

EN ISO 3657:2023

(Main)

Animal and vegetable fats and oils - Determination of saponification value (ISO 3657:2023)

Animal and vegetable fats and oils - Determination of saponification value (ISO 3657:2023)

This document specifies a method for the determination of the saponification value of animal and vegetable fats and oils. The saponification value is a measure of the free and esterified acids present in fats and fatty acids.
The method is applicable to refined and crude vegetable and animal fats.
If mineral acids are present, the results given by this method are not interpretable unless the mineral acids are determined separately.
The saponification value can also be calculated from fatty acid data obtained by gas chromatography analysis as given in Annex B. For this calculation, it is necessary to be sure that the sample does not contain major impurities or is thermally degraded.

Tierische und pflanzliche Fette und Öle - Bestimmung der Verseifungszahl (ISO 3657:2023)

Dieses Dokument legt ein Verfahren zur Bestimmung der Verseifungszahl von tierischen und pflanzlichen Fetten und Ölen fest. Die Verseifungszahl ist ein Maß für die Menge an freien und veresterten Säuren, die in Fetten und Fettsäuren vorhanden sind.
Das Verfahren ist für raffinierte und rohe pflanzliche und tierische Fette anwendbar.
Bei Vorhandensein von Mineralsäuren sind die nach diesem Verfahren erhaltenen Ergebnisse nicht auswertbar, es sei denn, die Mineralsäuren wurden getrennt bestimmt.
Die Verseifungszahl kann auch aus den Fettsäuredaten berechnet werden, die durch gaschromatographische Untersuchungen erhalten wurden, wie in Anhang B angegeben. Für diese Berechnung ist es notwendig, sich sicher zu sein, dass die Probe keine größeren Verunreinigungen enthält oder dass sie thermisch abgebaut wird.

Corps gras d'origines animale et végétale - Détermination de l'indice de saponification (ISO 3657:2023)

Le présent document spécifie une méthode de détermination de l'indice de saponification des corps gras d’origines animale et végétale. L'indice de saponification est une caractéristique des acides gras libres et estérifiés présents dans les corps gras et acides gras.
La méthode est applicable aux corps gras d'origines végétale et animale raffinés et bruts.
En présence d'acides minéraux, les résultats donnés par cette méthode ne sont plus interprétables si l'on ne dose pas séparément l'acidité minérale.
L’indice de saponification peut également être calculé à partir des données de composition en acides gras obtenues par chromatographie en phase gazeuse, selon l’Annexe B. Pour effectuer ce calcul, il est nécessaire de s’assurer que l’échantillon ne contient aucune impureté importante et qu’il n’est pas dégradé thermiquement.

Živalske in rastlinske maščobe ter olja - Določevanje števila umiljenja (ISO 3657:2023)

Ta dokument določa metodo za določevanje števila umiljenja živalskih in rastlinskih maščob ter olj. Umiljenje je meritev prostih in esterificiranih kislin, prisotnih v maščobah in maščobnih kislinah.
Metoda se uporablja za rafinirane in surove rastlinske in živalske maščobe.
Če so prisotne mineralne kisline, rezultatov, pridobljenih s to metodo, ni mogoče interpretirati, razen če se mineralne kisline določijo ločeno.
Umiljenje je mogoče izračunati tudi na podlagi podatkov o maščobnih kislinah, pridobljenih z analizo plinske kromatografije, kot je podana v Dodatku B. Za ta izračun je treba preveriti, da vzorec ne vsebuje večjih nečistoč in da ni termično razkrojen.

General Information

Status
Published
Publication Date
11-Jul-2023
ICS
67.200.10 - Animal and vegetable fats and oils
Technical Committee
CEN/TC 307 - Oilseeds, vegetables and animal fats and oils and their by-products - Methods of sampling and analys
Drafting Committee
CEN/TC 307 - Oilseeds, vegetables and animal fats and oils and their by-products - Methods of sampling and analys
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
12-Jul-2023
Completion Date
12-Jul-2023
Ref Project
SIST EN ISO 3657:2023 - Animal and vegetable fats and oils - Determination of saponification value (ISO 3657:2023)

Relations

Replaces
EN ISO 3657:2020 - Animal and vegetable fats and oils - Determination of saponification value (ISO 3657:2020)
Effective Date
15-Jun-2022

Buy Standard

EN ISO 3657:2023EN ISO 3657:2023
PreviousNext
Standard
EN ISO 3657:2023
English language
17 pages
sale 10% off
Preview
sale 10% off
Preview
e-Library read for
1 day

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 3657:2023
01-oktober-2023
Nadomešča:
SIST EN ISO 3657:2020
Živalske in rastlinske maščobe ter olja - Določevanje števila umiljenja (ISO
3657:2023)
Animal and vegetable fats and oils - Determination of saponification value (ISO
3657:2023)
Tierische und pflanzliche Fette und Öle - Bestimmung der Verseifungszahl (ISO
3657:2023)
Corps gras d'origines animale et végétale - Détermination de l'indice de saponification
(ISO 3657:2023)
Ta slovenski standard je istoveten z: EN ISO 3657:2023
ICS:
67.200.10 Rastlinske in živalske Animal and vegetable fats
maščobe in olja and oils
SIST EN ISO 3657:2023 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
SIST EN ISO 3657:2023

---------------------- Page: 2 ----------------------
SIST EN ISO 3657:2023


EN ISO 3657
EUROPEAN STANDARD

NORME EUROPÉENNE

July 2023
EUROPÄISCHE NORM
ICS 67.200.10 Supersedes EN ISO 3657:2020
English Version

Animal and vegetable fats and oils - Determination of
saponification value (ISO 3657:2023)
Corps gras d'origines animale et végétale - Tierische und pflanzliche Fette und Öle - Bestimmung
Détermination de l'indice de saponification (ISO der Verseifungszahl (ISO 3657:2023)
3657:2023)
This European Standard was approved by CEN on 12 May 2023.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 3657:2023 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
SIST EN ISO 3657:2023
EN ISO 3657:2023 (E)
Contents Page
European foreword . 3

2

---------------------- Page: 4 ----------------------
SIST EN ISO 3657:2023
EN ISO 3657:2023 (E)
European foreword
This document (EN ISO 3657:2023) has been prepared by Technical Committee ISO/TC 34 "Food
products" in collaboration with Technical Committee CEN/TC 307 “Oilseeds, vegetable and animal fats
and oils and their by-products - Methods of sampling and analysis” the secretariat of which is held by
AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by January 2024, and conflicting national standards shall
be withdrawn at the latest by January 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 3657:2020.
Any feedback and questions on this document should be directed to the users’ national standards
body/national committee. A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 3657:2023 has been approved by CEN as EN ISO 3657:2023 without any modification.

3

---------------------- Page: 5 ----------------------
SIST EN ISO 3657:2023

---------------------- Page: 6 ------
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

CEN
EN ISO 12872:2022(Main)
Olive oils and olive-pomace oils - Determination of the 2-glyceryl monopalmitate content (ISO 12872:2022)
SIST EN ISO 12872:2023

This document specifies a procedure for the determination of the content, as a percentage mass fraction, of 2-glyceryl monopalmitate in olive oils and olive-pomace oils that are liquid at ambient temperature (20 °C).
NOTE       This document is based on COI/T.20/Doc. No 23/Rev.1:2017[7].

  • Standard
    23 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 14111:2022(Main)
Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of iodine value
SIST EN 14111:2022

This document specifies a titrimetric method for the determination of iodine value in Fatty Acid Methyl Esters, hereinafter referred as FAME.
The precision statement of this test method was determined in a Round Robin exercise with iodine values in the range 111 g iodine/100 g to 129 g iodine/100 g.
The test method is also applicable for lower iodine values; however, the precision statement is not established for iodine values below 111 g iodine/100 g.
WARNING - The use of this document can involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this document to take appropriate measures to ensure the safety and health of personnel prior to the application of the document, and to determine the applicability of any other restrictions for this purpose.

  • Standard
    10 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO 18363-1:2021(Main)
Animal and vegetable fats and oils - Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 1: Method using fast alkaline transesterification and measurement for 3-MCPD and differential measurement for glycidol (ISO 18363-1:2015)
SIST EN ISO 18363-1:2022

ISO 18363-1:2015 describes a procedure for the indirect determination of 3-MCPD esters (bound 3-MCPD) and possible free 3-MCPD after alkaline catalysed ester cleavage and derivatization with phenylboronic acid (PBA). Furthermore, this part of ISO 18363 enables the indirect determination of glycidyl esters (bound glycidol) under the assumption that no other substances are present that react at room temperature with inorganic chloride to generate 3-MCPD.
ISO 18363-1:2015 is applicable to solid and liquid fats and oils. Milk and milk products (or fat coming from milk and milk products) are excluded from the scope of this part of ISO 18363.

  • Standard
    20 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO 18363-3:2021(Main)
Animal and vegetable fats and oils - Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol (ISO 18363-3:2017)
SIST EN ISO 18363-3:2022

ISO 18363-3:2017 specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2-MCPD), 3‐MCPD esters (bound 3‐MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC/MS analysis.
ISO 18363-3:2017 is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg.

  • Standard
    27 pages
    English language
    sale 10% off
    e-Library read for
    1 day
  • Draft
    24 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO 18363-4:2021(Main)
Animal and vegetable fats and oils - Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 4: Method using fast alkaline transesterification and measurement for 2-MCPD, 3-MCPD and glycidol by GC-MS/MS (ISO 18363-4:2021)
SIST EN ISO 18363-4:2021

This document specifies a rapid procedure for the simultaneous determination of 2-MCPD esters (bound 2-MCPD), 3‐MCPD esters (bound 3‐MCPD) and glycidyl esters (bound glycidol) in a single assay, based on alkaline catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC-MS/MS analysis. Glycidyl ester overestimation is corrected by addition of an isotopic labelled ester bound 3-MCPD which allows the quantification of 3-MCPD induced glycidol during the procedure.
This method is applicable to solid and liquid fats and oils. This document also applies to animal fats and used frying oils and fats, but these matrices were not included in the validation. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg.
Milk and milk products (or fat coming from milk and milk products), infant formulas, emulsifiers, free fatty acids and other fats- and oils-derived matrices are excluded from the scope of this document.

  • Standard
    32 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
CEN ISO/TS 22115:2021(Main)
Animal and vegetable fats and oils - Separation of lipid classes by capillary gas chromatography (fingerprint method) (ISO/TS 22115:2021)
SIST-TS CEN ISO/TS 22115:2021

This document specifies a method for the semi-quantitative analysis of oils, fats and oil/fat-related samples (deodistillates).
It is applicable to the screening of oils, fats and oil/fat-related samples to obtain main (e.g. triglycerides) and minor (e.g. sterols, sterol esters, tocopherols, wax esters, fatty alcohols, glycerol) component information in one single analysis. For a truly quantitative analysis of pre-identified compound classes, specific methods are more appropriate.
The method can also be used as a useful qualitative screening tool for the relative comparison of sample compositions.

  • Technical specification
    29 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN ISO 6321:2021(Main)
Animal and vegetable fats and oils - Determination of melting point in open capillary tubes - Slip point (ISO 6321:2021)
SIST EN ISO 6321:2021

This document specifies two methods for the determination of the melting point in open capillary tubes, commonly known as the slip melting point, of animal and vegetable fats and oils (referred to as fats hereinafter).
—    Method A is only applicable to animal and vegetable fats which are solid at ambient temperature and which do not exhibit pronounced polymorphism.
—    Method B is applicable to all animal and vegetable fats which are solid at ambient temperature and is the method to be used for fats whose polymorphic behaviour is unknown.
For the determination of the slip melting point of palm oil samples the method given in Annex A shall be used.
NOTE 1   If applied to fats with pronounced polymorphism, method A will give different and less satisfactory results than method B.
NOTE 2   Fats which exhibit pronounced polymorphism are principally cocoa butter and fats containing appreciable quantities of 2-unsaturated, 1,3-saturated triacylglycerols.

  • Standard
    18 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 14104:2021(Main)
Fat and oil derivates - Fatty acid methyl ester (FAME) - Determination of acid value
SIST EN 14104:2021

This document specifies a titrimetric method for the determination of acid value in light coloured Fatty Acid Methyl Esters, hereinafter referred as FAME.
It allows the determination of acid value within a range of 0,10 mg KOH/g to 1,00 mg KOH/g.
NOTE 1 For the purposes of this document, the terms "% (m/m)" and "% (V/V)" are used to represent respectively the mass fraction and the volume fraction.
NOTE 2 For oils and fats the determination of acid value is specified in EN ISO 660 [1].
WARNING - The use of this document can involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this document to take appropriate measures to ensure the safety and health of personnel prior to the application of the document, and to determine the applicability of any other restrictions for this purpose.

  • Standard
    10 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 14105:2020(Main)
Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of free and total glycerol and mono-, di-, triglyceride contents
SIST EN 14105:2021

This document specifies a method to determine the free glycerol and residual mono-, di- and triglyceride contents in fatty acid methyl esters (FAME). The total glycerol content is then calculated from the obtained results.
Under the conditions described, the quantification limits are 0,001 % (m/m) for free glycerol, 0,10 % (m/m) for all glycerides (mono-, di- and tri-). This method is suitable for FAME prepared from rapeseed, sunflower, soybean, palm, animal oils and fats and mixture of them. It is not suitable for FAME produced from or containing coconut and palm kernel oils derivatives because of overlapping of different glyceride peaks.
NOTE 1 For the purposes of this document, the term "% (m/m)" is used to represent the mass fraction.
NOTE 2 Under the common EN 14105 GC conditions squalene can coelute with alpha glycerol monostearate. If the presence of squalene is suspected, EN 17057 can be used to discriminate between squalene and glycerol monostearate.
WARNING - The use of this document can involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this document to take appropriate measures to ensure the safety and health of personnel prior to application of the standard, and fulfil statutory and regulatory requirements for this purpose.

  • Standard
    27 pages
    English language
    sale 10% off
    e-Library read for
    1 day
CEN
EN 14112:2020(Main)
Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of oxidation stability (accelerated oxidation test)
SIST EN 14112:2021

This document specifies a method for the determination of the oxidation stability of fatty acid methyl esters (FAME) at 110 °C, by means of measuring the induction period up to 48 h.
For induction periods higher than 8,5 h the precision is not covered by the precision statement of this method.
NOTE 1 EN 15751 [1] describes a similar test method for oxidation stability determination of pure fatty acid methyl esters and of blends of FAME with petroleum-based diesel containing 2 % (V/V) of FAME at minimum.
NOTE 2 Limited studies on EN 15751 with EHN (2-ethyl hexyl nitrate) on FAME blends indicated that the stability is reduced to an extent which is within the reproducibility of the test method. It is likely that the oxidation stability of pure FAMEs is also reduced in the presence of EHN when EN 14112 is used for testing.
NOTE 3 For the purposes of this document, the term ''% (V/V)'' is used to represent the volume fraction.

  • Standard
    18 pages
    English language
    sale 10% off
    e-Library read for
    1 day