prEN 12662-1
(Main)Liquid petroleum products - Determination of total contamination - Part 1: Middle distillates and diesel fuels
Liquid petroleum products - Determination of total contamination - Part 1: Middle distillates and diesel fuels
This document specifies a method for the determination of the content of undissolved substances, referred to as total contamination, in middle distillates, in diesel fuels containing up to 30 % (V/V) fatty acid methyl esters (FAME). The working range is from 12 mg/kg to 26 mg/kg and it was established in an interlaboratory study by applying EN ISO 4259-1 [1].
This document in general applies to products having a kinematic viscosity not exceeding 8 mm2/s at 20 °C, or 5 mm2/s at 40 °C, e.g. diesel fuel as specified in EN 590 [2].
This test method may be used for diesel fuels containing more than 30 % (V/V) FAME and for petroleum products having a kinematic viscosity exceeding 8 mm2/s at 20 °C, or 5 mm2/s at 40 °C, however in such cases the precision of the test method has not been defined.
NOTE For the purposes of this document, the term "% (V/V)" is used to represent the volume fraction, φ, of a material.
WARNING - Use of this test method may involve hazardous materials, operations and equipment. This method does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this method to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.
Flüssige Mineralölerzeugnisse - Bestimmung der Gesamtverschmutzung - Teil 1: Dieselkraftstoff
Dieses Dokument legt ein Prüfverfahren zur Bestimmung des Gehalts an ungelösten Stoffen, bezeichnet als Gesamtverschmutzung, in Mitteldestillaten, in Dieselkraftstoff mit einem Anteil von bis zu 30 % (V/V) Fettsäure-Methylester (FAME, en: fatty acid methyl ester) fest. Der zulässige Messbereich von 12 mg/kg bis 26 mg/kg wurde anhand von Ringversuchen unter Anwendung von EN ISO 4259-1 [1] festgelegt.
Dieses Dokument gilt im Allgemeinen für Erzeugnisse mit einer kinematischen Viskosität nicht über 8 mm2/s bei 20 °C bzw. 5 mm2/s bei 40 °C, z. B. Dieselkraftstoffe nach EN 590 [2].
Dieses Prüfverfahren kann ebenfalls für Dieselkraftstoffe mit mehr als 30 % (V/V) FAME sowie für Mineralölerzeugnisse mit einer kinematischen Viskosität oberhalb von 8 mm2/s bei 20 °C oder 5 mm2/s bei 40 °C eingesetzt werden. Für diese erweiterte Anwendung des Prüfverfahrens gibt es bisher allerdings keine Präzisionsangaben.
ANMERKUNG Für die Zwecke dieses Dokuments wird zur Angabe des Volumenanteils, φ, einer Substanz der Ausdruck "% (V/V)" verwendet.
WARNUNG - Die Anwendung dieses Prüfverfahrens kann den Einsatz gefährlicher Stoffe, Arbeitsgänge und Geräte mit sich bringen. Dieses Verfahren gibt nicht vor, alle mit seiner Anwendung verbundenen Sicherheitsprobleme anzusprechen. Der Anwender dieses Verfahrens ist dafür verantwortlich, vorher angemessene Maßnahmen hinsichtlich Sicherheit und Gesundheit zu ergreifen und die Anwendbarkeit einschränkender Vorschriften zu ermitteln.
Produits pétroliers liquides - Détermination de la contamination totale - Partie 1 : Distillats moyens et gazoles
Le présent document prescrit une méthode de détermination de la teneur en substances non dissoutes, référencée comme contamination totale, dans les distillats moyens, dans les gazoles contenant jusqu’à 30 % (V/V) d’esters méthyliques d’acides gras (EMAG). Le domaine d’application s’étend sur un intervalle de teneurs en contaminants allant de 12 mg/kg à 26 mg/kg ; celui-ci a été établi au moyen d’une étude interlaboratoires conformément à l’EN ISO 4259 1 [1].
Ce document s'applique généralement aux produits dont la viscosité cinématique ne dépasse pas 8 mm2/s à 20 C ou 5 mm2/s à 40 C, par exemple aux carburants pour moteurs diesel spécifiés dans la norme EN 590 [2].
Cette méthode d’essai peut être utilisée sur des carburants diesel contenant plus de 30 % (V/V) d’EMAG et sur des produits pétroliers dont la viscosité cinématique est supérieure à 8 mm2/s à 20 C ou 5 mm2/s à 40 C, cependant, dans de tels cas, les valeurs de fidélité concernant cette méthode n’ont pas été déterminées.
NOTE Pour les besoins du présent document, l'expression « % (V/V) » est employée pour représenter la fraction volumique, φ, d’un produit.
AVERTISSEMENT — L'utilisation de la présente méthode d’essai implique l'intervention de produits, d'opérations et d'équipements à caractère dangereux. La présente méthode n'est pas censée aborder tous les problèmes de sécurité concernés par sa mise en œuvre. Il est de la responsabilité de l'utilisateur de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.
Tekoči naftni proizvodi - Določevanje vseh nečistoč - 1. del: Srednji destilati in dizelsko gorivo
General Information
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Standards Content (Sample)
SLOVENSKI STANDARD
oSIST prEN 12662-1:2023
01-januar-2023
Tekoči naftni proizvodi - Določevanje vseh nečistoč - 1. del: Srednji destilati in
dizelsko gorivo
Liquid petroleum products - Determination of total contamination - Part 1: Middle
distillates and diesel fuels
Flüssige Mineralölerzeugnisse - Bestimmung der Gesamtverschmutzung in
Mitteldestillaten, Dieselkraftstoff und Fettsäure-Methylestern
Produits pétroliers liquides - Détermination de la contamination totale des distillats
moyens, des gazoles et des esters méthyliques d'acides gras
Ta slovenski standard je istoveten z: prEN 12662-1
ICS:
75.160.20 Tekoča goriva Liquid fuels
oSIST prEN 12662-1:2023 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
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oSIST prEN 12662-1:2023
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oSIST prEN 12662-1:2023
DRAFT
EUROPEAN STANDARD
prEN 12662-1
NORME EUROPÉENNE
EUROPÄISCHE NORM
January 2023
ICS Will supersede EN 12662:2014
English Version
Liquid petroleum products - Determination of total
contamination - Part 1: Middle distillates and diesel fuels
Produits pétroliers liquides - Détermination de la Flüssige Mineralölerzeugnisse - Bestimmung der
contamination totale - Partie 1 : Distillats moyens et Verschmutzung - Teil 1: Mitteldestillate und
gazoles Dieselkraftstoffe
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 19.
If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.
This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.
Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 12662-1:2023 E
worldwide for CEN national Members.
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prEN 12662-1:2023 (E)
Contents Page
European foreword . 3
Introduction . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Principle . 6
5 Reagents and materials . 6
6 Equipment . 6
7 Cleansing of sample containers and filtration apparatus . 7
8 Sampling . 8
9 Preparation of the test portion . 8
9.1 General. 8
9.2 Middle distillates and diesel fuels . 9
2
9.3 Liquid petroleum products with a kinematic viscosity exceeding 8 mm /s at 20 °C, or
2
5 mm /s at 40 °C . 9
10 Preparation of the equipment . 9
10.1 Preparation of the filtration apparatus . 9
10.2 Preparation of the filter . 10
11 Procedure . 10
12 Calculation . 11
13 Expression of results . 11
14 Precision . 11
14.1 General. 11
14.2 Repeatability . 11
14.3 Reproducibility . 12
15 Test report . 12
Bibliography . 13
2
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prEN 12662-1:2023 (E)
European foreword
This document (prEN 12662-1:2023) has been prepared by Technical Committee CEN/TC 19 “Gaseous
and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin”, the
secretariat of which is held by NEN.
This document is currently submitted to the CEN Enquiry.
This document will supersede EN 12662:2014.
In comparison with the previous edition, the following technical modifications have been made:
— split of the scope of the previous edition in two parts, with Part 1 covering the middle distillates and
the diesel fuels containing up to 30 % (V/V) of fatty acid methyl ester (FAME) in this document and
with Part 2 covering the neat FAME in a separated document;
— update of the precision data following a new statistical analysis [4] of the interlaboratory tests data
available without the FAME samples according to EN ISO 4259-1 [1].
3
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Introduction
Excessive contamination in a fuel system can give rise to premature blocking of filters and/or hardware
failure, and is therefore undesirable. The determination of the content of undissolved substances,
referred to as total contamination, is a way to control this issue.
In the previous version of this method, the scope was covering middle distillates, diesel fuels containing
up to 30 % (V/V) of FAME and neat FAME. But, it was found that the method was not applicable for neat
FAME. It has been decided to split the scope in two parts: to include the previous version as Part 1 and to
develop a separate standard for neat FAME as Part 2.
4
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1 Scope
This document specifies a method for the determination of the content of undissolved substances,
referred to as total contamination, in middle distillates, in diesel fuels containing up to 30 % (V/V) fatty
acid methyl esters (FAME). The working range is from 12 mg/kg to 26 mg/kg and it was established in
an interlaboratory study by applying EN ISO 4259-1 [1].
2
This document in general applies to products having a kinematic viscosity not exceeding 8 mm /s at
2
20 °C, or 5 mm /s at 40 °C, e.g. diesel fuel as specified in EN 590 [2].
This test method may be used for diesel fuels containing more than 30 % (V/V) FAME and for petroleum
2 2
products having a kinematic viscosity exceeding 8 mm /s at 20 °C, or 5 mm /s at 40 °C, however in such
cases the precision of the test method has not been defined.
NOTE For the purposes of this document, the term “% (V/V)” is used to represent the volume fraction, φ, of a
material.
WARNING — Use of this test method may involve hazardous materials, operations and equipment. This
method does not purport to address all of the safety problems associated with its use. It is the
responsibility of the user of this method to establish appropriate safety and health practices and to
determine the applicability of regulatory limitations prior to use.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 14275, Automotive fuels — Assessment of petrol and diesel fuel quality — Sampling from retail site
pumps and commercial site fuel dispensers
EN ISO 3170, Petroleum liquids — Manual sampling (ISO 3170)
EN ISO 3171, Petroleum liquids — Automatic pipeline sampling (ISO 3171)
ISO 3819, Laboratory glassware — Beakers
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— IEC Electropedia: available at https://www.electropedia.org/
— ISO Online browsing platform: available at https://www.iso.org/obp/ui
3.1
total contamination
undissolved substances retained on a filter after filtration under test conditions
3.2
absolute pressure
pressure measured relative to zero pressure or a total vacuum
5
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4 Principle
A sample portion is weighed and filtered under vacuum through a pre-weighed filter. In the case of liquid
2 2
petroleum products having a kinematic viscosity exceeding 8 mm /s at 20 °C, or 5 mm /s at 40 °C, the
weighed sample portion is diluted with a solvent before filtration. The filter with the residue is washed,
dried and weighed. Contamination is calculated from the difference in mass of the filter and expressed
relative to the sample mass as mg/kg.
5 Reagents and materials
5.1 Heptane, with a purity no less than 99,0 % (V/V), filtered using a membrane filter (6.18).
NOTE Heptane used as a reference fuel in EN ISO 5164 [3] is suitable.
5.2 Propan-2-ol, with a purity no less than 99,0 % (V/V).
NOTE Propan-2-ol is used to dry glassware and the sample container after rinsing with water.
6 Equipment
All glassware and sample containers shall be carefully cleaned as described in Clause 7.
Usual laboratory apparatus and glassware, together with the following:
6.1 Filtration apparatus, suitable for a filter (6.2), as shown in Figure 1.
A different filtration apparatus may be used if it is suitable to take the filters given in 6.2.
6.2 Filters, of high retention glass fibre type, 47 mm in diameter and with a 0,7 μm mean pore size.
NOTE Glass fibre filters Whatman GF-F type have been found suitable for total contamination measurements.
This information is given for the convenience of users of this document and does not constitute an endorsement by
CEN of this product.
6.3 Beakers, tall form 0,5 l and 1 l, conforming with ISO 3819 or an equivalent national standard.
6.4 Cylinders, 500 ml and 1 000 ml graduated cylinders.
6.5 Glass bottles, 0,5 l and 1 l, with screw caps.
6.6 Oven, of the static type (without fan assisted circulation), explosion-proof, capable of heating to
(110 ± 5) °C.
6.7 Desiccator, containing freshly activated silica gel (or equivalent desiccant) with a moisture content
indicator.
6.8 Glass Petri dishes with covers, greater than 50 mm in diameter.
6.9 Analytical balance, capable of weighing to the nearest 0,1 mg.
6.10 Forceps, with round shaped tips for transferring the filter from the filter holder to the Petri dish
and from the latter on to the dish of the analytical balance.
6.11 Water bath or oven, capable of maintaining the following temperatures: (40 ± 1) °C and
(60 ± 1) °C.
6
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6.12 Wash bottle, fitted with spray nozzle, suitable for use with heptane (5.1).
6.13 Top load balance, capable of weighing 1 500 g to
...
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