EN 13466-2:2001

Fertilizers - Determination of water content (Karl Fischer methods) - Part 2: 2-propanol as extracting medium

This European standard specifies a Karl Fischer titrimetric method for the determination of the water content of fertilizers based on the use of 2-propanol as extracting medium.
The method is applicable to all solid mineral fertilizers. The result (KFP water) includes "free" water and extracted water of crystallization from the following components of fertilizers: calcium nitrate tetrahydrate (Ca(NO3)2·4H2O); magnesium sulfate heptahydrate (MgSO4·7H2O); potassium chloride magnesium chloride hexahydrate (Carnallite, KCl·MgCl2·6H2O); magnesium nitrate hexahydrate (Mg(NO3)2·6H2O).

Düngemittel - Bestimmung des Wassergehaltes (Karl-Fischer-Verfahren) - Teil 2: 2-Propanol als Extraktionsmittel

Diese Europäische Norm legt ein titrimetrisches Karl-Fischer-Verfahren für die maßanalytische Bestimmung des Wasser-ge-haltes von Düngemitteln fest, das auf der Verwendung von 2-Propanol als Extraktionsmittel basiert.
Das Verfahren gilt für alle festen mineralischen Düngemittel. Das Ergebnis (KFP-Wasser) umfasst ¿freies" Wasser sowie extrahiertes Kristallwasser der folgenden Düngemittelbestandteile: Calciumnitrattetrahydrat (Ca(NO3)2 · 4H2O); Magnesiumsulfatheptahydrat (MgSO4 · 7H2O); Kaliumchlorid-Magnesiumchloridhexahydrat (Carnallit, KCl · MgCl2 · 6H2O); Magnesiumnitrathexahy-drat (Mg(NO3)2 · 6H2O).

Engrais - Détermination de la teneur en eau (Méthodes Karl Fischer) - Partie 2: 2-propanol comme milieu d'extraction

La présente Norme européenne spécifie une méthode Karl Fischer de titrage de la teneur en eau des engrais, reposant sur l'utilisation de 2-propanol comme milieu d'extraction.
La méthode est applicable à tous les engrais solides. Le résultat (eau KFP) englobe l'eau "libre" et l'eau de cristallisation des éléments suivants des matières fertilisantes : nitrate de calcium tétrahydraté (Ca(NO3)2.4H2O), sulfate de magnésium heptahydraté (MgSO4.7H2O), chlorure de potassium et de magnésium hexahydraté (Carnallite, KCl.MgCl2.6H2O), nitrate de magnésium hexahydraté (Mg(NO3)2.6H2O).

Gnojila - Določevanje količine vode (Karl Fischerjeve metode) - 2. del: Ekstrakcija z 2-propanolom

General Information

• Status: Published
• Publication Date: 09-Oct-2001
• Withdrawal Date: 29-Apr-2002
• ICS: 65.080 - Fertilizers
• Technical Committee: CEN/TC 260 - Fertilizers and liming materials
• Drafting Committee: CEN/TC 260/WG 2 - Physical properties of fertilizers
• Current Stage: 9093 - Decision to confirm - Review Enquiry
• Completion Date: 08-Jul-2022
• Ref Project: SIST EN 13466-2:2002 - Fertilizers - Determination of water content (Karl Fischer methods) - Part 2: 2-propanol as extracting medium

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.SURSDQRORPDüngemittel - Bestimmung des Wassergehaltes (Karl-Fischer-Verfahren) - Teil 2: 2-Propanol als ExtraktionsmittelEngrais - Détermination de la teneur en eau (Méthodes Karl Fischer) - Partie 2: 2-propanol comme milieu d'extractionFertilizers - Determination of water content (Karl Fischer methods) - Part 2: 2-propanol as extracting medium65.080GnojilaFertilizersICS:Ta slovenski standard je istoveten z:EN 13466-2:2001SIST EN 13466-2:2002en01-november-2002SIST EN 13466-2:2002SLOVENSKI
STANDARD



SIST EN 13466-2:2002



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 13466-2October 2001ICS 65.080English versionFertilizers - Determination of water content (Karl Fischermethods) - Part 2: 2-propanol as extracting mediumEngrais - Détermination de la teneur en eau (Méthodes KarlFischer) - Partie 2: 2-propanol comme milieu d'extractionDüngemittel - Bestimmung des Wassergehaltes (Karl-Fischer-Verfahren) - Teil 2: 2-Propanol als ExtraktionsmittelThis European Standard was approved by CEN on 18 August 2001.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2001 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 13466-2:2001 ESIST EN 13466-2:2002



EN 13466-2:2001 (E)2ContentspageForeword.3Introduction.41Scope.52Normative references.53Principle.54Reagents.55Apparatus.56Installation and test of the Karl Fischer titrator.67Sampling.68Procedure.69Calculation and expression of results.810Precision.811Test report.8Bibliography.10SIST EN 13466-2:2002



EN 13466-2:2001 (E)3ForewordThis European Standard has been prepared by Technical Committee CEN/TC 260 "Fertilizers and limingmaterials", the secretariat of which is held by DIN.This European Standard shall be given the status of a national standard, either by publication of an identical text orby endorsement, at the latest by April 2002, and conflicting
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