Petroleum products - Determination of distillation characteristics at atmospheric pressure (ISO 3405:2000)

Migrated from Progress Sheet (TC Comment) (2000-07-10): Decision of BT to submit this ISO document to UAP procedure. ++ Standard under revision in ISO ++ UAP procedure changed to parallel vote on revision, resolution BT C 123/1995?

Mineralölerzeugnisse - Bestimmung des Destillationsverlaufes bei Atmosphärendruck (ISO 3405:2000)

Produits pétroliers - Détermination des caractéristiques de distillation à pression atmosphérique (ISO 3405:2000)

La présente Norme internationale spécifie une méthode de laboratoire pour la détermination des caractéristiques de distillation des distillats pétroliers légers et moyens ayant un point initial de distillation supérieur à 0 °C et un point final inférieur à environ 400 °C, utilisant un équipement manuel ou automatisé, la méthode manuelle étant la procédure de référence, sauf accord contraire.NOTE : La méthode est applicable aux produits pétroliers contenant de petites quantités de composés non pétroliers.Toutefois, il est possible que dans certains cas les valeurs de fidélité ne s'appliquent pas.Les caractéristiques de distillation (volatilité) des hydrocarbures sont importantes en matière de sécurité et de performances, en particulier dans le cas des carburants et des solvants. L'intervalle de distillation donne des renseignements importants sur la composition et le comportement pendant le stockage et l'utilisation, et la vitesse d'évaporation est une caractéristique essentielle dans l'utilisation de nombreux solvants. La plupart des spécifications applicables aux distillats pétroliers fixent des valeurs limites pour certaines caractéristiques de distillation, afin de mieux maîtriser les performances en utilisation et pour contrôler la formation de vapeurs qui pourraient devenir explosives en présence d'air ou s'échapper dans l'atmosphère (COV).

Naftni proizvodi - Določevanje destilacijskih značilnosti pri tlačni atmosferi (ISO 3405:2000)

General Information

Status
Withdrawn
Publication Date
29-Feb-2000
Withdrawal Date
14-Jan-2011
Current Stage
9960 - Withdrawal effective - Withdrawal
Start Date
15-Jan-2011
Completion Date
15-Jan-2011

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SLOVENSKI STANDARD
01-julij-2000
1DIWQLSURL]YRGL'RORþHYDQMHGHVWLODFLMVNLK]QDþLOQRVWLSULWODþQLDWPRVIHUL ,62

Petroleum products - Determination of distillation characteristics at atmospheric pressure
(ISO 3405:2000)
Mineralölerzeugnisse - Bestimmung des Destillationsverlaufes bei Atmosphärendruck
(ISO 3405:2000)
Produits pétroliers - Détermination des caractéristiques de distillation a pression
atmosphérique (ISO 3405:2000)
Ta slovenski standard je istoveten z: EN ISO 3405:2000
ICS:
75.080 Naftni proizvodi na splošno Petroleum products in
general
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EUROPEAN STANDARD
EN ISO 3405
NORME EUROPÉENNE
EUROPÄISCHE NORM
March 2000
ICS 75.080
English version
Petroleum products - Determination of distillation characteristics
at atmospheric pressure (ISO 3405:2000)
Produits pétroliers - Détermination des caractéristiques de Mineralölerzeugnisse - Bestimmung des
distillation à pression atmosphérique (ISO 3405:2000) Destillationsverlaufes bei Atmosphärendruck (ISO
3405:2000)
This European Standard was approved by CEN on 1 March 2000.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official
versions.
CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,
Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2000 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 3405:2000 E
worldwide for CEN national Members.

Page 2
Foreword
Corrected 2001-05-09
The text of the International Standard ISO 3405:2000 has been prepared by Technical
Committee ISO/TC 28 "Petroleum products and lubricants" in collaboration with Technical
Committee CEN/TC 19 "Petroleum products, lubricants and related products", the secretariat
of which is held by NEN.
This European Standard shall be given the status of a national standard, either by publication
of an identical text or by endorsement, at the latest by September 2000, and conflicting
national standards shall be withdrawn at the latest by September 2000.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of
the following countries are bound to implement this European Standard: Austria, Belgium,
Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy,
Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United
Kingdom.
Endorsement notice
The text of the International Standard ISO 3405:2000 was approved by CEN as a European
Standard without any modification.
NOTE: Normative references to International Standards are listed in annex ZA (normative).

Page 3
Annex ZA (normative)
Normative references to international publications
with their relevant European publications
This European Standard incorporates by dated or undated reference, provisions from other
publications. These normative references are cited at the appropriate places in the text and the
publications are listed hereafter. For dated references, subsequent amendments to or revisions
of any of these publications apply to this European Standard only when incorporated in it by
amendment or revision. For undated references the latest edition of the publication referred to
applies (including amendments).
NOTE Where an International Publication has been modified by common modifications,
indicated by (mod.), the relevant EN/HD applies.
Publication Year Title EN Year
ISO 3170 1988 Petroleum liquids - Manual sampling EN ISO 3170 1998
(including Amendment 1:1998)
ISO 3171 1988 Petroleum liquids - Automatic pipeline EN ISO 3171 1999
sampling
INTERNATIONAL ISO
STANDARD 3405
Third edition
2000-03-01
Petroleum products — Determination of
distillation characteristics at atmospheric
pressure
Produits pétroliers — Détermination des caractéristiques de distillation à
pression atmosphérique
Reference number
ISO 3405:2000(E)
©
ISO 2000
ISO 3405:2000(E)
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ii © ISO 2000 – All rights reserved

ISO 3405:2000(E)
Contents Page
1 Scope .1
2 Normative references .1
3 Terms and definitions .2
4 Principle.3
5 Apparatus .3
5.1 General.3
5.2 Distillation flasks .3
5.3 Condenser tube and cooling bath.4
5.4 Metal shield or enclosure for flask (manual apparatus only).8
5.5 Heat source .8
5.6 Flask-support .8
5.7 Graduated cylinders .8
5.8 Temperature measurement system .9
5.9 Centring device.10
5.10 Barometer.10
6 Samples and sampling.11
7 Preparation of apparatus .12
8 Apparatus verification.14
8.1 Level follower.14
8.2 Electronic temperature-measurement devices.14
9 Procedure .15
10 Calculations.17
11 Expression of results .20
12 Precision.20
12.1 General.20
12.2 Repeatability.21
12.3 Reproducibility.21
12.4 Bias .23
13 Test report .23
Annex A (normative) Thermometer specifications.24
Annex B (normative) Determination of temperature-sensor lag times and specified distillation data.25
Annex C (informative) Examples of data calculations.27
Annex D (informative) Bias between manual and automated results.31
Annex E (informative) Emulation of emergent-stem errors .33
ISO 3405:2000(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO
member bodies). The work of preparing International Standards is normally carried out through ISO technical
committees. Each member body interested in a subject for which a technical committee has been established has
the right to be represented on that committee. International organizations, governmental and non-governmental, in
liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical
Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 3.
Draft International Standards adopted by the technical committees are circulated to the member bodies for voting.
Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this International Standard may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights.
International Standard ISO 3405 was prepared by Technical Committee ISO/TC 28, Petroleum products and
lubricants.
This third edition cancels and replaces the second edition (ISO 3405:1988), of which it constitutes a technically
revision.
Annexes A and B form a normative part of this International Standard. Annexes C, D and E are for information only.
iv © ISO 2000 – All rights reserved

INTERNATIONAL STANDARD ISO 3405:2000(E)
Petroleum products — Determination of distillation
characteristics at atmospheric pressure
WARNING — The use of this International Standard may involve hazardous materials, operations and
equipment. This International Standard does not purport to address all of the safety problems associated
with its use. It is the responsibility of the user of this International Standard to establish appropriate safety
and health practices and to determine the applicability of regulatory limitations prior to use.
1 Scope
This International Standard specifies a laboratory method for the determination of the distillation characteristics of
light and middle distillates derived from petroleum with initial boiling points above 0 �C and end-points below
approximately 400 �C, utilizing either manual or automated equipment, with the manual procedure being the
referee met
...

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