ISO 13876:2013

Soil quality — Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)

ISO 13876:2013 specifies a method for quantitative determination of seven selected polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153, and PCB180) in sludge, treated biowaste, and soil using GC-MS and GC-ECD.

Qualité du sol — Détermination des polychlorobiphényles (PCB) par chromatographie en phase gazeuse avec détection sélective de masse (GC-MS) et chromatographie en phase gazeuse avec détection par capture d'électrons (GC-ECD)

Kakovost tal - Določevanje polikloriranih bifenilov (PCB) s plinsko kromatografijo z masno selektivnim detektorjem (GC-MS) ali s plinsko kromatografijo z detektorjem z zajetjem elektronov (GC-ECD)

Ta mednarodni standard določa metodo za kvantitativno določevanje sedmih izbranih polikloriranih bifenilov (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 in PCB180) v blatu,
obdelanih bioloških odpadkih in tleh z uporabo metod GC-MS in GC-ECD (glej preglednico 2).
Meja zaznavanja je odvisna od determinant, uporabljene opreme, kakovosti kemikalij, uporabljenih
za ekstrakcijo vzorca, in očiščenja ekstrakta.
Pod pogoji, določenimi v tem mednarodnem standardu, je mogoče doseči mejo uporabe 1 μg/kg (izraženo
kot suho snov).
Blato in obdelani biološki odpadki se lahko razlikujejo glede lastnosti, predvidenih stopenj onesnaženja s polikloriranimi bifenili ter prisotnosti motečih snovi. Zaradi teh razlik ni možen opis enotnega splošnega postopka. Ta mednarodni standard vključuje tabele odločanja, ki temeljijo na lastnostih vzorca, ter postopek za ekstrakcijo in očiščenje, ki ga je treba uporabiti.

General Information

• Status: Withdrawn
• Publication Date: 03-Nov-2013
• ICS: 13.080.10 - Chemical characteristics of soils
• Technical Committee: ISO/TC 190/SC 3 - Chemical and physical characterization
• Drafting Committee: ISO/TC 190/SC 3/WG 6 - Organic analysis
• Current Stage: 9599 - Withdrawal of International Standard
• Completion Date: 05-Oct-2023
• Ref Project: SIST ISO 13876:2019 - Soil quality - Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)

Relations

• Revised: ISO 18475:2023 - Environmental solid matrices — Determination of polychlorinated biphenyls (PCB) by gas chromatography - mass selective detection (GC-MS) or electron-capture detection (GC-ECD)
• Effective Date: 13-Aug-2022

Standards Content (Sample)

SLOVENSKI STANDARD
SIST ISO 13876:2019
01-oktober-2019
Kakovost tal - Določevanje polikloriranih bifenilov (PCB) s plinsko kromatografijo
z masno selektivnim detektorjem (GC-MS) ali s plinsko kromatografijo z
detektorjem z zajetjem elektronov (GC-ECD)
Soil quality - Determination of polychlorinated biphenyls (PCB) by gas chromatography
with mass selective detection (GC-MS) and gas chromatography with electron-capture
detection (GC-ECD)
Qualité du sol - Détermination des polychlorobiphényles (PCB) par chromatographie en
phase gazeuse avec détection sélective de masse (GC-MS) et chromatographie en
phase gazeuse avec détection par capture d'électrons (GC-ECD)
Ta slovenski standard je istoveten z: ISO 13876:2013
ICS:
13.080.10 Kemijske značilnosti tal Chemical characteristics of
soils
71.040.50 Fizikalnokemijske analitske Physicochemical methods of
metode analysis
SIST ISO 13876:2019 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST ISO 13876:2019

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SIST ISO 13876:2019
INTERNATIONAL ISO
STANDARD 13876
First edition
2013-11-15
Soil quality — Determination of
polychlorinated biphenyls (PCB)
by gas chromatography with mass
selective detection (GC-MS) and
gas chromatography with electron-
capture detection (GC-ECD)
Qualité du sol — Détermination des polychlorobiphényles (PCB) par
chromatographie en phase gazeuse avec détection sélective de masse
(GC-MS) et chromatographie en phase gazeuse avec détection par
capture d’électrons (GC-ECD)
Reference number
ISO 13876:2013(E)
©
ISO 2013

---------------------- Page: 3 ----------------------
SIST ISO 13876:2019
ISO 13876:2013(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2013
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail [e-mail]
Web www.iso.org
Published in Switzerland
ii © ISO 2013 – All rights reserved

---------------------- Page: 4 ----------------------
SIST ISO 13876:2019
ISO 13876:2013(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 2
4 Principle . 2
5 Interferences . 3
5.1 Interference with sampling and extraction . 3
5.2 Interference with GC . 3
6 Safety remarks . 3
7 Reagents . 4
7.1 General .
...

INTERNATIONAL ISO
STANDARD 13876
First edition
2013-11-15
Soil quality — Determination of
polychlorinated biphenyls (PCB)
by gas chromatography with mass
selective detection (GC-MS) and
gas chromatography with electron-
capture detection (GC-ECD)
Qualité du sol — Détermination des polychlorobiphényles (PCB) par
chromatographie en phase gazeuse avec détection sélective de masse
(GC-MS) et chromatographie en phase gazeuse avec détection par
capture d’électrons (GC-ECD)
Reference number
ISO 13876:2013(E)
©
ISO 2013

---------------------- Page: 1 ----------------------
ISO 13876:2013(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2013
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail [e-mail]
Web www.iso.org
Published in Switzerland
ii © ISO 2013 – All rights reserved

---------------------- Page: 2 ----------------------
ISO 13876:2013(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 2
4 Principle . 2
5 Interferences . 3
5.1 Interference with sampling and extraction . 3
5.2 Interference with GC . 3
6 Safety remarks . 3
7 Reagents . 4
7.1 General . 4
7.2 Reagents for extraction . 4
7.3 Reagents for clean-up . 4
7.4 Gas chromatographic analysis . 7
7.5 Standards . 7
7.6 Preparation of standard solutions . 9
8 Apparatus .
...

SLOVENSKI STANDARD
oSIST ISO 13876:2019
01-junij-2019
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]PDVQRVHOHNWLYQLPGHWHNWRUMHP*&06DOLVSOLQVNRNURPDWRJUDILMR]
GHWHNWRUMHP]]DMHWMHPHOHNWURQRY*&(&'
Soil quality - Determination of polychlorinated biphenyls (PCB) by gas chromatography
with mass selective detection (GC-MS) and gas chromatography with electron-capture
detection (GC-ECD)
Qualité du sol - Détermination des polychlorobiphényles (PCB) par chromatographie en
phase gazeuse avec détection sélective de masse (GC-MS) et chromatographie en
phase gazeuse avec détection par capture d'électrons (GC-ECD)
Ta slovenski standard je istoveten z: ISO 13876:2013
ICS:
13.080.10 .HPLMVNH]QDþLOQRVWLWDO Chemical characteristics of
soils
71.040.50 Fizikalnokemijske analitske Physicochemical methods of
metode analysis
oSIST ISO 13876:2019 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------

oSIST ISO 13876:2019

---------------------- Page: 2 ----------------------

oSIST ISO 13876:2019
INTERNATIONAL ISO
STANDARD 13876
First edition
2013-11-15
Soil quality — Determination of
polychlorinated biphenyls (PCB)
by gas chromatography with mass
selective detection (GC-MS) and
gas chromatography with electron-
capture detection (GC-ECD)
Qualité du sol — Détermination des polychlorobiphényles (PCB) par
chromatographie en phase gazeuse avec détection sélective de masse
(GC-MS) et chromatographie en phase gazeuse avec détection par
capture d’électrons (GC-ECD)
Reference number
ISO 13876:2013(E)
©
ISO 2013

---------------------- Page: 3 ----------------------

oSIST ISO 13876:2019
ISO 13876:2013(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2013
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail [e-mail]
Web www.iso.org
Published in Switzerland
ii © ISO 2013 – All rights reserved

---------------------- Page: 4 ----------------------

oSIST ISO 13876:2019
ISO 13876:2013(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 2
4 Principle . 2
5 Interferences . 3
5.1 Interference with sampling and extraction . 3
5.2 Interference with GC . 3
6 Safety remarks . 3
7 Reagents . 4
7.1 General .
...